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CN101500700B - 将氧化汞转化成单质汞的方法及装置 - Google Patents

将氧化汞转化成单质汞的方法及装置 Download PDF

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Publication number
CN101500700B
CN101500700B CN2006800238846A CN200680023884A CN101500700B CN 101500700 B CN101500700 B CN 101500700B CN 2006800238846 A CN2006800238846 A CN 2006800238846A CN 200680023884 A CN200680023884 A CN 200680023884A CN 101500700 B CN101500700 B CN 101500700B
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mercury
fluid sample
room
pressure
converter
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Chinese (zh)
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CN101500700A (zh
Inventor
詹姆斯·H·格拉西
戴特尔·基塔
杰弗里·索查
德克·阿佩尔
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Thermo Fisher Scientific Inc
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Thermo Electron Corp
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Priority claimed from US11/120,317 external-priority patent/US7354553B2/en
Priority claimed from US11/120,182 external-priority patent/US7454952B2/en
Priority claimed from US11/120,316 external-priority patent/US20060245974A1/en
Priority claimed from US11/120,315 external-priority patent/US20060243096A1/en
Application filed by Thermo Electron Corp filed Critical Thermo Electron Corp
Publication of CN101500700A publication Critical patent/CN101500700A/zh
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/46Removing components of defined structure
    • B01D53/64Heavy metals or compounds thereof, e.g. mercury
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/30Controlling by gas-analysis apparatus
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/346Controlling the process
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B43/00Obtaining mercury
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B7/00Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
    • C22B7/001Dry processes
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B7/00Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
    • C22B7/02Working-up flue dust
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0009General constructional details of gas analysers, e.g. portable test equipment
    • G01N33/0011Sample conditioning
    • G01N33/0013Sample conditioning by a chemical reaction
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0009General constructional details of gas analysers, e.g. portable test equipment
    • G01N33/0027General constructional details of gas analysers, e.g. portable test equipment concerning the detector
    • G01N33/0036General constructional details of gas analysers, e.g. portable test equipment concerning the detector specially adapted to detect a particular component
    • G01N33/0045Hg
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/60Heavy metals or heavy metal compounds
    • B01D2257/602Mercury or mercury compounds
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/62Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
    • G01N21/63Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
    • G01N21/64Fluorescence; Phosphorescence
    • G01N21/6402Atomic fluorescence; Laser induced fluorescence
    • G01N21/6404Atomic fluorescence
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Environmental & Geological Engineering (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Metallurgy (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Biomedical Technology (AREA)
  • Physics & Mathematics (AREA)
  • Geology (AREA)
  • Pathology (AREA)
  • Immunology (AREA)
  • General Physics & Mathematics (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Food Science & Technology (AREA)
  • Biochemistry (AREA)
  • Combustion & Propulsion (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
  • Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Treating Waste Gases (AREA)
CN2006800238846A 2005-05-02 2006-05-02 将氧化汞转化成单质汞的方法及装置 Active CN101500700B (zh)

Applications Claiming Priority (9)

Application Number Priority Date Filing Date Title
US11/120,317 2005-05-02
US11/120,317 US7354553B2 (en) 2005-05-02 2005-05-02 Method and apparatus for detecting the presence of elemental mercury in a gas sample
US11/120,182 US7454952B2 (en) 2005-05-02 2005-05-02 Method and apparatus for monitoring mercury in a gas sample
US11/120,316 US20060245974A1 (en) 2005-05-02 2005-05-02 Method and apparatus for generating oxidized mercury having a measurable concentration
US11/120,316 2005-05-02
US11/120,182 2005-05-02
US11/120,315 2005-05-02
US11/120,315 US20060243096A1 (en) 2005-05-02 2005-05-02 Method and apparatus for converting oxidized mercury into elemental mercury
PCT/US2006/016854 WO2006119298A2 (fr) 2005-05-02 2006-05-02 Procede et appareil de conversion de mercure oxyde en mercure elementaire

Publications (2)

Publication Number Publication Date
CN101500700A CN101500700A (zh) 2009-08-05
CN101500700B true CN101500700B (zh) 2012-05-16

Family

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Family Applications (2)

Application Number Title Priority Date Filing Date
CN2006800234205A Active CN101287987B (zh) 2005-05-02 2006-05-02 监测气体样品中的汞的方法及装置
CN2006800238846A Active CN101500700B (zh) 2005-05-02 2006-05-02 将氧化汞转化成单质汞的方法及装置

Family Applications Before (1)

Application Number Title Priority Date Filing Date
CN2006800234205A Active CN101287987B (zh) 2005-05-02 2006-05-02 监测气体样品中的汞的方法及装置

Country Status (8)

Country Link
US (1) US7454945B1 (fr)
EP (3) EP1877776A4 (fr)
JP (2) JP2009503438A (fr)
CN (2) CN101287987B (fr)
CA (2) CA2606720C (fr)
FI (1) FI3514533T3 (fr)
PL (1) PL1877770T3 (fr)
WO (4) WO2006119298A2 (fr)

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US8443648B2 (en) * 2007-06-29 2013-05-21 Babcock & Wilcox Power Generation Group, Inc. Controlled humidification calibration checking of continuous emissions monitoring system
JP2009019886A (ja) * 2007-07-10 2009-01-29 Nippon Instrument Kk 水銀原子蛍光分析装置
US8069703B1 (en) * 2007-11-30 2011-12-06 The United States Of America As Represented By The United States Department Of Energy Semi-continuous detection of mercury in gases
FR2938916B1 (fr) * 2008-11-24 2012-10-19 Ap2E Dispositif d'echantillonnage de gaz.
US8351035B2 (en) * 2009-05-12 2013-01-08 Thermo Fisher Scientific Inc. Particulate detection and calibration of sensors
US8646306B2 (en) * 2009-12-14 2014-02-11 Ngk Insulators, Ltd. Method for manufacturing sensor element for gas sensor
EP2482057B1 (fr) * 2011-01-27 2013-03-20 Sick Ag Analyseur de gaz destiné à la mesure de la teneur en mercure d'un gaz et procédé de calibration
CN102564986B (zh) * 2011-12-30 2014-08-27 北京雪迪龙科技股份有限公司 一种烟气汞排放监测系统和方法
US20150096349A1 (en) * 2012-05-14 2015-04-09 Pen Inc. Optimize analyte dynamic range in gas chromatography
CN102698657B (zh) * 2012-06-19 2015-04-01 北京雪迪龙科技股份有限公司 一种汞的催化反应装置
WO2014032615A1 (fr) * 2012-08-31 2014-03-06 Bao Diana Détecteur d'ions métalliques portatif
CN103134718B (zh) * 2012-12-29 2015-06-10 聚光科技(杭州)股份有限公司 烟气中气态总汞的监测系统及方法
CN104155249A (zh) * 2014-07-17 2014-11-19 中国科学院过程工程研究所 一种同时测定零价汞和二价汞的监测装置及监测方法
US10012622B2 (en) 2014-07-29 2018-07-03 Utah State University Gaseous mercury detection systems, calibration systems, and related methods
CN104330374B (zh) * 2014-11-19 2017-01-04 清华大学 一种煤中汞含量测量装置
WO2016136714A1 (fr) * 2015-02-24 2016-09-01 日立造船株式会社 Appareil pour traiter des gaz de fumée
CN105955217A (zh) * 2016-05-24 2016-09-21 曹国东 一种火力发电厂燃料采样及化验信息化管理方法及装置
US10712242B2 (en) 2017-02-28 2020-07-14 Process Hg Group Holdings, Llc Mercury-in-gas sampling system
CN107238527A (zh) * 2017-04-28 2017-10-10 东南大学 一种高温裂解式气相汞形态转化装置及方法
CN109239009A (zh) * 2018-09-03 2019-01-18 杭州电子科技大学 基于环形谐振腔倍频结构的气态汞浓度检测装置及方法
CN109211816B (zh) * 2018-11-13 2024-01-05 南京工程学院 烟气中含Hg浓度的抗干扰检测方法和检测装置
JP7552220B2 (ja) * 2020-10-08 2024-09-18 株式会社Ihi 排ガス処理装置
CN112473345B (zh) * 2020-10-23 2021-08-24 三河市清源绿创环境技术股份有限公司 一种气体发生系统
CN113959792A (zh) * 2021-10-25 2022-01-21 西安热工研究院有限公司 一种基于低温等离子体热解的烟气中汞测量装置及方法
CN113884649B (zh) * 2021-11-05 2025-07-25 中国科学院地球化学研究所 一种用于分析气态总汞的自动分析装置

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US3844719A (en) * 1972-06-01 1974-10-29 Ppg Industries Inc Mercury metal analyzer
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Also Published As

Publication number Publication date
EP3514533B1 (fr) 2023-06-28
WO2006119193A1 (fr) 2006-11-09
CN101500700A (zh) 2009-08-05
WO2006119298A3 (fr) 2009-04-23
WO2006119424A3 (fr) 2007-06-28
EP1877776A4 (fr) 2014-08-13
PL1877770T3 (pl) 2019-02-28
FI3514533T3 (fi) 2023-09-14
WO2006119192A2 (fr) 2006-11-09
WO2006119424A2 (fr) 2006-11-09
JP2009503437A (ja) 2009-01-29
CA2606733C (fr) 2010-11-09
EP1877776A2 (fr) 2008-01-16
WO2006119298A2 (fr) 2006-11-09
EP1877770A2 (fr) 2008-01-16
CN101287987B (zh) 2011-03-30
CN101287987A (zh) 2008-10-15
EP1877770B1 (fr) 2018-09-12
CA2606720C (fr) 2013-09-10
CA2606733A1 (fr) 2006-11-09
EP3514533A2 (fr) 2019-07-24
CA2606720A1 (fr) 2006-11-09
US7454945B1 (en) 2008-11-25
EP3514533A3 (fr) 2019-11-27
EP1877770A4 (fr) 2014-08-13
JP2009503438A (ja) 2009-01-29
WO2006119192A3 (fr) 2007-09-27

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