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US181499A - Improvement in processes and apparatus for manufacturing gas - Google Patents

Improvement in processes and apparatus for manufacturing gas Download PDF

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US181499A
US181499A US181499DA US181499A US 181499 A US181499 A US 181499A US 181499D A US181499D A US 181499DA US 181499 A US181499 A US 181499A
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retort
gas
pipe
charge
coke
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10JPRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J3/00Production of combustible gases containing carbon monoxide from solid carbonaceous fuels
    • C10J3/02Fixed-bed gasification of lump fuel
    • C10J3/06Continuous processes
    • C10J3/08Continuous processes with ash-removal in liquid state

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  • FIG. 2 is a detached view of a basket used in connection with the retort.
  • the method commonly practiced in the manufacture of coal-gas is to first heat the retorts to the requisite degree, and then introduce the charge, and permit distillation to take place for four or five hours, or until the charge is exhausted, after which the retorts are drawn and recharged.
  • the stand -pipe is located near the mouth of the retort, and the gases are drawn directly from the retort, an exhaust being usually employed for that purpose.
  • A indicates a retort, which may be the only one employed, according to v the amount of gas to be produced, or one of a bench or series.
  • the rear third or fourth part v of the retort is occupied by what I'term a basket, as it may be made of metal and detachable, but is preferably built of brick or tile, in the form of an arch platform or false bottom, a, which will support coke or like substance placed thereon, and form a channel or conduit for the entrance of gas beneath.
  • This platform or false bottom a is perforated
  • a partition-wall a vi the rear wall a terminating just below the top of the retort, or perforated, if preferred, to permit the escape of gas to the exitpipe c.
  • a barrier, b Directly in front of partition (1. is a barrier, b, which prevents the charge from closing the conduit beneath the platform a. a
  • Exitpipe 0 is an exit-pipe, (or 'downtake,) provided with a steam-jet, d, and, directly below the same, a water-jet or spray pipe, 0, by means of which the exhaust may be controlled, and the gas freed from any light carbonaceous matter, thus keeping the exit pipe clean.
  • This pipe may proceed from side or top.
  • Exitpipe 0 communicates directly with a sprayor similar washer, B, interposed between the exit-pipe and the usual stand-pipe G.
  • Bis a washer 9r condenser provided above with a spray-pipe, f, and below with a trap-pipe, g.
  • Saidwasher receives the gas on its way to the stand-pipe, and washes out all pitchy or carbonaceous particles not previously removed by the first or exit pipe, spray, and condenser, thus preventing anything but fixed gas passing to the stand-pipe O, and preventing clog- No scrubber is shown in the drawing; but it'is understood, of course, that the usual or any approved scrubber and condenser may be employed.
  • the operation of these devices is as follows:
  • the retort being filled, the first charge may be worked off in the usual manner, (the steam-jet being regulated to the required exhaust,) after which the resulting coke is pushed back or charged onto platform a, and a fresh charge of coal introduced into the front part of the retort.
  • the first gas or product of slow distillation, in its passage through and over the red-hot coke on platform a, has its oily and tarry matters arrested and decomposed within the retort.
  • the exhaust located near the connection of the exit-pipe and retort induces and controls the flow of gas, and the spray-condenser immediately below the steam-jet assists the exhaust,and at the same time washes out any pitchy matters that might otherwise become attached to and clog the exit-pipe.
  • a The same body of coke placed on platform a a. may be frequently used without being changed.
  • the size of the body of coke will depend to some extent on the coal used, a richer coal requiring a greater body of coke than a poor gas-producin g coal.
  • the charge'of coke in the rear of the retort must be adapted to the coal or .body distilled. N 0 tar, but simply a heavy pitch and carbonaceous matter is produced.
  • the gas product will be increased from ten per cent. to thirty per cent. without being deteriorated.
  • At moment of charging the retort by increasing the through or over abody of coke located in said retort between the charge and exit pipe, and subsequently subjecting the gas thus produced to the action of a water jet or spray before its escape from the exit-pipe of the retort, substantially as herein specified.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Coke Industry (AREA)

Description

UNITED STATES PATENT OFFIGE.
HERBERT W. C. TWEDDLE, OF PITTSBURG, PENNSYLVANIA.
IMPROVEMENT IN PROCESSES AND APPARATUS FOR MANUFACTURING GAS.
Specification forming part of Letters Patent No. 181,499, dated August 22, 1876; application filed 4 March 13, 1876.
' ing out my invention. Fig. 2 is a detached view of a basket used in connection with the retort. v v
Like letters refer to like parts wherever they My invention relates to processes and apparatus for the manufacture of gas from coal.
The method commonly practiced in the manufacture of coal-gas is to first heat the retorts to the requisite degree, and then introduce the charge, and permit distillation to take place for four or five hours, or until the charge is exhausted, after which the retorts are drawn and recharged. The stand -pipe is located near the mouth of the retort, and the gases are drawn directly from the retort, an exhaust being usually employed for that purpose. By such a method the best results are not attainable, for the reason that when the charge is introduced it rapidly absorbs the heat of the retort, reducing the temperature so low as to produce a slow distillation inimical to the production of gas, but favorable to the formation of tar. As a consequence, the gas that first passes over is surcharged with tarry and oily matters, which clog the stand-pipe and condense in the hydraulic main. As the distillation is continued thegas becomes poorer and poorer, for the reason that the slow distillation which first took place to a greatextent exhausted without utilizing the gas-producing elements.
Recognizing these objections to the common method, various modifications have been suggested and tried-as, for instance, dividing up the retort into sections by partitions, which prolonged the travel of the gas, and caused it to pass consecutively through the several quantities or divisions of the charge, and retained it in the retort for a longer period; 2
the use of outer and inner retorts to obtain uniform distribution, perfect circulation, and
intimate contact of the gases with the hot sarfaces of the retorts-but such methods increased the pressure in the retort, and are ob- I .viously objectionable. It has likewise been suggested to introduce the charge in successive divided quantities to re-enforce, as it were,
the exhausted portions of the charge but it is v evident that what results in the common practice will likewise occur under this modification, though perhaps in a less degree. a Finally, thepassing of the gas from a bench of retorts through a superheating-retort filled method is, so far as I am aware, the nearest approach to the present invention; but, by such a method, each retort does not work off its own charge, and produce a rich uniformwith coke, brick, and various substances has been suggested and applied, and this latte gas; it simply transfers to a common retort or reservoir the tarry and oily matters of the first part. or slow distillation. This latter method results in the formation of carbon in the superh'eating-retort and stand-pipes, and I method of producing coal-gas is still the method .universally followed.
I will how proceed to describe the devices employed by me, and in connection therewith my process, so that others skilled in the art to which it appertains may apply my inven- 7 tion. In the drawing, A indicates a retort, which may be the only one employed, according to v the amount of gas to be produced, or one of a bench or series. The rear third or fourth part v of the retort is occupied by what I'term a basket, as it may be made of metal and detachable, but is preferably built of brick or tile, in the form of an arch platform or false bottom, a, which will support coke or like substance placed thereon, and form a channel or conduit for the entrance of gas beneath. This platform or false bottom a is perforated,
as shown, and bounded at each end by a partition-wall, a vi the rear wall a terminating just below the top of the retort, or perforated, if preferred, to permit the escape of gas to the exitpipe c. Directly in front of partition (1. is a barrier, b, which prevents the charge from closing the conduit beneath the platform a. a
0 is an exit-pipe, (or 'downtake,) provided with a steam-jet, d, and, directly below the same, a water-jet or spray pipe, 0, by means of which the exhaust may be controlled, and the gas freed from any light carbonaceous matter, thus keeping the exit pipe clean. This pipe may proceed from side or top. Exitpipe 0 communicates directly with a sprayor similar washer, B, interposed between the exit-pipe and the usual stand-pipe G. Bis a washer 9r condenser, provided above with a spray-pipe, f, and below with a trap-pipe, g. Saidwasher receives the gas on its way to the stand-pipe, and washes out all pitchy or carbonaceous particles not previously removed by the first or exit pipe, spray, and condenser, thus preventing anything but fixed gas passing to the stand-pipe O, and preventing clog- No scrubber is shown in the drawing; but it'is understood, of course, that the usual or any approved scrubber and condenser may be employed.
'The operation of these devices is as follows: The retort being filled, the first charge may be worked off in the usual manner, (the steam-jet being regulated to the required exhaust,) after which the resulting coke is pushed back or charged onto platform a, and a fresh charge of coal introduced into the front part of the retort. The first gas or product of slow distillation, in its passage through and over the red-hot coke on platform a, has its oily and tarry matters arrested and decomposed within the retort. The exhaust located near the connection of the exit-pipe and retort induces and controls the flow of gas, and the spray-condenser immediately below the steam-jet assists the exhaust,and at the same time washes out any pitchy matters that might otherwise become attached to and clog the exit-pipe.
By thus retaining the tarry products of the distillation within the retort, and subjecting them to the action of the red-hot coke, it will be found that a greater quantity of illuminating-gas is obtained, depending upon the quality of the coal, or other matter employed.
I have thus far described my process in connection with the apparatus shown but it is evident other devices may be substituted for those shown, (and preferred,) and that some specified may be dispensed with entirelyas for instance, the basket may be omitted, and the first charge, when coked, be
pushed directly back. In the process the rear of the retort may be charged with coke, be-
fore the first charge is introduced,if preferred. a The same body of coke placed on platform a a. may be frequently used without being changed. The size of the body of coke will depend to some extent on the coal used, a richer coal requiring a greater body of coke than a poor gas-producin g coal.
If petroleum, benzole, or petroleum resid uum, or other rich bodies are used, the body of coke in the rear end of retort must be made larger and more compact. are used that do not yield much tar, passing over the coke is only necessary. In any event,
the charge'of coke in the rear of the retort must be adapted to the coal or .body distilled. N 0 tar, but simply a heavy pitch and carbonaceous matter is produced. The gas product will be increased from ten per cent. to thirty per cent. without being deteriorated. At moment of charging the retort by increasing the through or over abody of coke located in said retort between the charge and exit pipe, and subsequently subjecting the gas thus produced to the action of a water jet or spray before its escape from the exit-pipe of the retort, substantially as herein specified.
2. In combination with a retort of the ordinary form, the perforated basket a. a a, and the barrier b, interposed between the charging orifice and the gas-exit, substantially as and for the purpose specified.
3. In combination with a gas-retort, having the basket 0 a a interposed between the charging-orifice and the gas-exit, the exit-pipe 0, provided with the steam-jet d, and the water-jet e, substantially as and for the purpose specified.
In testimony thereof I, the said HERBERT W. G. TWEDDLE, have hereunto set my hand.
HERBERT W. G. TWEDDLE.
Witnesses: JAMES I. KAY,
L. G. FITTER.
Where poor coals
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