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CN104475663A - Stearic acid wax material recovering processing technology - Google Patents

Stearic acid wax material recovering processing technology Download PDF

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Publication number
CN104475663A
CN104475663A CN201410646328.0A CN201410646328A CN104475663A CN 104475663 A CN104475663 A CN 104475663A CN 201410646328 A CN201410646328 A CN 201410646328A CN 104475663 A CN104475663 A CN 104475663A
Authority
CN
China
Prior art keywords
wax material
wax
water
stearic acid
value
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410646328.0A
Other languages
Chinese (zh)
Inventor
何拥军
何嘉圣
何嘉贤
赖卫华
伍斌华
杨学
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
LIUZHOU JINTE MACHINERY Co Ltd
Original Assignee
LIUZHOU JINTE MACHINERY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by LIUZHOU JINTE MACHINERY Co Ltd filed Critical LIUZHOU JINTE MACHINERY Co Ltd
Priority to CN201410646328.0A priority Critical patent/CN104475663A/en
Publication of CN104475663A publication Critical patent/CN104475663A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22CFOUNDRY MOULDING
    • B22C1/00Compositions of refractory mould or core materials; Grain structures thereof; Chemical or physical features in the formation or manufacture of moulds
    • B22C1/16Compositions of refractory mould or core materials; Grain structures thereof; Chemical or physical features in the formation or manufacture of moulds characterised by the use of binding agents; Mixtures of binding agents
    • B22C1/18Compositions of refractory mould or core materials; Grain structures thereof; Chemical or physical features in the formation or manufacture of moulds characterised by the use of binding agents; Mixtures of binding agents of inorganic agents

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

The invention discloses a stearic acid wax material recovering processing technology. The technology comprises the following steps: checking whether a processing tank has water leakage and wax leakage phenomena or not, burdening water and a wax material, adding the obtained mixture to the processing tank, heating, adding hydrochloric acid or sulfuric acid when the wax material is boiling, discarding acid water, and detecting the pH value of the obtained wax liquid to obtain a qualified wax liquid. The processing technology can be used to well recover the wax liquid and process the qualified wax liquid to a brown or yellow transparent wax liquid.

Description

A kind of stearic acid wax material recovery processing technique
Technical field
The invention belongs to casting waterglass technical field, particularly a kind of stearic acid wax material recovery processing technique.
Background technology
In casting waterglass process, can relate to a lot of waste material, cause great waste, improve production cost, waste resource, existing recovery method can not thoroughly be recycled, and utilization rate is not high.
Summary of the invention
The invention provides a kind of stearic acid wax material recovery processing technique.
Technical scheme of the present invention is: a kind of stearic acid wax material recovery processing technique, is characterized in that, comprise the following steps:
(1) whether check processing groove leaks, leaks wax;
(2) water to be processed and wax material are prepared respectively and add in treatment trough, be heated to boiling, keep fluidized state 45-60 minute, temperature controls at 95-105 DEG C, and wherein, the ratio of wax material and water is 3:1;
(3) under wax material fluidized state, slowly add hydrochloric acid or sulfuric acid, continue 45-90 minute;
(4) open after treatment trough valve bleeds off sour water, add appropriate water and be heated to the 10-15 minute that seethes with excitement again, 2-3 time repeatedly, the pH value of measurement sour water, makes pH value be 6-7;
(5) wax liquid qualified after, through being furnished with being pumped in stationary tub of screen pack.
Preferably, hydrochloric acid is added in wax material in described step (three).
Preferably, described step (four) if in when the pH value of sour water is less than 6-7 after 2-3 time repeatedly, in treatment trough, add industrial Na (OH), then survey pH value.
Preferably, in described step (five), qualified wax liquid just can enter next process in static more than 2 hours in stationary tub.
Beneficial effect of the present invention: processing method energy of the present invention well recycling wax liquid, processing qualified wax liquid is brown or yellow transparent shape.
Detailed description of the invention
Embodiment provided by the invention is described in further detail:
A kind of stearic acid wax material recovery processing technique, comprises the following steps:
(1) whether check processing groove leaks, leaks wax, has problem to process in time;
(2) water to be processed and wax material are prepared respectively and add in treatment trough, be heated to boiling, keep fluidized state 45-60 minute, temperature controls at 95-105 DEG C, and wherein, the ratio of wax material and water is 3:1;
(3) under wax material fluidized state, slowly add hydrochloric acid or sulfuric acid, continue 45-90 minute;
(4) open after treatment trough valve bleeds off sour water, add appropriate water and be heated to the 10-15 minute that seethes with excitement again, 2-3 time repeatedly, measure the pH value of sour water, pH value is made to be 6-7, if when the pH value of 2-3 rear sour water is less than 6-7 repeatedly, adds industrial Na (OH) in treatment trough, then survey pH value;
(5) wax liquid qualified after, through being furnished with being pumped in stationary tub of screen pack.
Preferably, hydrochloric acid is added in wax material in described step (three).
Preferably, in described step (five), qualified wax liquid just can enter next process in static more than 2 hours in stationary tub.
In this description, the present invention is described with reference to its specific embodiment.But, still can make various amendment and conversion obviously and not deviate from the spirit and scope of the present invention.Therefore, description is regarded in an illustrative, rather than a restrictive.

Claims (4)

1. a stearic acid wax material recovery processing technique, is characterized in that, comprises the following steps:
(1) whether check processing groove leaks, leaks wax;
(2) water to be processed and wax material are prepared respectively and add in treatment trough, be heated to boiling, keep fluidized state 45-60 minute, temperature controls at 95-105 DEG C, and wherein, the ratio of wax material and water is 3:1;
(3) under wax material fluidized state, slowly add hydrochloric acid or sulfuric acid, continue 45-90 minute;
(4) open after treatment trough valve bleeds off sour water, add appropriate water and be heated to the 10-15 minute that seethes with excitement again, 2-3 time repeatedly, the pH value of measurement sour water, makes pH value be 6-7;
(5) wax liquid qualified after, through being furnished with being pumped in stationary tub of screen pack.
2. stearic acid wax material recovery processing technique according to claim 1, is characterized in that, adds hydrochloric acid in described step (three) in wax material.
3. stearic acid wax material recovery processing technique according to claim 1, is characterized in that, described step (four) if in when the pH value of sour water is less than 6-7 after 2-3 time repeatedly, in treatment trough, add industrial Na (OH), then survey pH value.
4. stearic acid wax material recovery processing technique according to claim 1, is characterized in that, in described step (five), qualified wax liquid just can enter next process in static more than 2 hours in stationary tub.
CN201410646328.0A 2014-11-15 2014-11-15 Stearic acid wax material recovering processing technology Pending CN104475663A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410646328.0A CN104475663A (en) 2014-11-15 2014-11-15 Stearic acid wax material recovering processing technology

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410646328.0A CN104475663A (en) 2014-11-15 2014-11-15 Stearic acid wax material recovering processing technology

Publications (1)

Publication Number Publication Date
CN104475663A true CN104475663A (en) 2015-04-01

Family

ID=52750340

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410646328.0A Pending CN104475663A (en) 2014-11-15 2014-11-15 Stearic acid wax material recovering processing technology

Country Status (1)

Country Link
CN (1) CN104475663A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107262669A (en) * 2017-07-05 2017-10-20 天长市兴宇铸造有限公司 A kind of pretreating process that casting wax is carried out based on sedimentation

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1084776A1 (en) * 1999-09-14 2001-03-21 Kawasaki Steel Techno-Research Corporation Method of recovering and refining filler from a lost wax composition
CN1796518A (en) * 2004-12-22 2006-07-05 洪静升 Treatment method of recovered wax
CN102615244A (en) * 2012-03-31 2012-08-01 四川德力铁道科技有限公司 Technology for recycling paraffin-resin mold material
CN103614242A (en) * 2013-11-20 2014-03-05 江苏江旭铸造集团有限公司 Lost foam wax material recycling method
CN104130865A (en) * 2014-07-31 2014-11-05 梁福柳 Recovering method for wax

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1084776A1 (en) * 1999-09-14 2001-03-21 Kawasaki Steel Techno-Research Corporation Method of recovering and refining filler from a lost wax composition
CN1796518A (en) * 2004-12-22 2006-07-05 洪静升 Treatment method of recovered wax
CN102615244A (en) * 2012-03-31 2012-08-01 四川德力铁道科技有限公司 Technology for recycling paraffin-resin mold material
CN103614242A (en) * 2013-11-20 2014-03-05 江苏江旭铸造集团有限公司 Lost foam wax material recycling method
CN104130865A (en) * 2014-07-31 2014-11-05 梁福柳 Recovering method for wax

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
九连砂陈鹏: "精密铸造水玻璃工艺:石蜡—硬脂酸蜡料回收处理", 《新浪博客》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107262669A (en) * 2017-07-05 2017-10-20 天长市兴宇铸造有限公司 A kind of pretreating process that casting wax is carried out based on sedimentation

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Application publication date: 20150401

RJ01 Rejection of invention patent application after publication