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CN104913886B - Method for leakage detection of Freon valve - Google Patents

Method for leakage detection of Freon valve Download PDF

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Publication number
CN104913886B
CN104913886B CN201510184162.XA CN201510184162A CN104913886B CN 104913886 B CN104913886 B CN 104913886B CN 201510184162 A CN201510184162 A CN 201510184162A CN 104913886 B CN104913886 B CN 104913886B
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freon
gas
valve
temperature
liquid separation
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CN104913886A (en
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金樟民
沈志斌
张奇
张博
李敏
张海
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Special Equipment Detect Delay Institute Of Wenzhou City
Dalian University of Technology
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Special Equipment Detect Delay Institute Of Wenzhou City
Dalian University of Technology
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Abstract

The invention provides a new method for leakage detection of a Freon valve, and belongs to the technical field of valve supervision and inspection. Freon is input via a Freon control vale firstly, high-temperature high-voltage water vapor is input via a high-temperature high-voltage stream control valve then, a mixed gas of the high-temperature high-voltage water vapor and the Freon enters a checked valve, multipoint step-by-step air extraction is performed on the checked valve by using an air extracting device, the extracted mixed gas is cooled in an air cooling device firstly, gas-liquid separation is performed in a gas-liquid separation device subsequently, and, finally, a halogen detector performs detection at air outlet of the gas-liquid separation device. The usage amount of the Freon is reduced, and serious pollution caused by that total fluoride as a working medium performs detection is reduced; a leakage point is accurately located through detection for the tracer gas Freon, and the leakage grade is determined through the number of lit alarm indicating lamps; and the cooling and gas-liquid separation devices are increased, an influence of too high stream temperature is prevented, and inspection precision is improved.

Description

氟利昂阀门检漏方法Freon valve leak detection method

技术领域technical field

本发明属于阀门监检技术领域,尤其是利用氟利昂作为示踪气体来检测阀门漏点和确定泄漏等级。The invention belongs to the technical field of valve supervision and inspection, and in particular uses freon as a tracer gas to detect valve leakage points and determine leakage levels.

背景技术Background technique

目前,阀门检漏方法主要有:气泡渗漏检测法、卤素检漏法、压力下降泄漏检测法、传感器流量检测法、氦气光谱分析检测法以及超声波检漏法。传统气泡渗漏检测法虽可以检测到泄漏,但无法测量泄漏量,由此改进的集气法虽可以测量泄漏量,但精度不够,且实施局限性很大。压力下降泄漏检测法可以间接计算出泄漏率,但由于检测以及精度的原因难以检测出微量泄漏,在一般工业现场实现起来效率较低。传感器流量检测法可以直接检测出泄漏率,但对于微泄漏测量所需的仪器精度要求非常高,从而造成检测成本高,在一般工业现场难以实现。氦气光谱分析检测法主要对微泄漏进行检测,检漏灵敏度高,但需要营造真空环境,整个检测过程时间较长,而且氦气价格昂贵,检测成本高,在阀门企业中使用率较低。超声波检漏法可以快速定位漏点,耗时短,检漏精度高,但超声波检漏设备开发技术难度大,目前国内外的超声波检漏仪都只能进行定性判断,不能进行泄漏量的计算。传统的卤素检测法使用大量的氟利昂,易对环境造成很大污染。At present, the valve leak detection methods mainly include: bubble leak detection method, halogen leak detection method, pressure drop leak detection method, sensor flow detection method, helium gas spectral analysis detection method and ultrasonic leak detection method. Although the traditional air bubble leak detection method can detect the leakage, it cannot measure the leakage amount. Although the improved gas collection method can measure the leakage amount, the accuracy is not enough, and the implementation limitations are very large. The pressure drop leak detection method can indirectly calculate the leakage rate, but it is difficult to detect small leaks due to detection and accuracy reasons, and the implementation efficiency in general industrial sites is low. The sensor flow detection method can directly detect the leakage rate, but the accuracy of the instrument required for micro-leakage measurement is very high, resulting in high detection costs, which is difficult to achieve in general industrial sites. The helium spectroscopic analysis detection method is mainly used to detect micro-leakage. The leak detection sensitivity is high, but it needs to create a vacuum environment, and the entire detection process takes a long time. Moreover, helium is expensive, and the detection cost is high, so the utilization rate in valve enterprises is low. The ultrasonic leak detection method can quickly locate the leak point, takes a short time, and has high leak detection accuracy. However, the development of ultrasonic leak detection equipment is difficult. At present, ultrasonic leak detectors at home and abroad can only make qualitative judgments and cannot calculate the amount of leakage. . The traditional halogen detection method uses a large amount of freon, which is easy to cause great pollution to the environment.

发明内容Contents of the invention

本发明的目的是对传统全氟检漏方式进行改进,降低卤素使用量的同时,降低传统卤素检测法对环境造成的严重污染,精确检测微泄漏点的同时确定泄漏等级,提高在工业现场的阀门气密性检漏效率。The purpose of the present invention is to improve the traditional perfluorinated leak detection method, while reducing the amount of halogen used, reduce the serious pollution of the environment caused by the traditional halogen detection method, accurately detect the micro-leakage point and determine the leakage level, and improve the safety of the industrial site. Valve air tightness leak detection efficiency.

本发明的技术方案:Technical scheme of the present invention:

氟利昂阀门检漏新方法,该方法所用的检测系统包括受检阀门、高温高压蒸汽控制阀1、氟利昂储存容器2、氟利昂控制阀3、排蒸汽阀4、抽气装置5、空气冷却装置6、冷凝水控制阀7、气液分离装置8和卤素检测仪9;高温高压蒸汽管道进口处安装高温高压蒸汽控制阀1,进高温高压蒸汽管道的中部与氟利昂储存容器2连接,氟利昂储存容器2出口处安装氟利昂控制阀3,受检阀门与进高温高压蒸汽管道、排蒸汽管道相连接,连接方式由受检阀门的结构决定,排蒸汽阀4安装在排蒸汽管道上靠近受检阀门位置,抽气装置5前端距离受检阀门表面检测点的距离不大于3mm,空气冷却装置6与抽气装置5一体化连接,空气流过空气冷却装置6,将抽气装置5中抽到的气体充分冷却,气液分离装置8安装在抽气装置5的末端,气液分离装置8的底部安装冷凝水控制阀7,卤素检测仪9的探头贴近气液分离装置8出气口的下沿,探头与出气口的水平距离为不大于3mm。A new method for leak detection of freon valves. The detection system used in this method includes the inspected valve, high temperature and high pressure steam control valve 1, freon storage container 2, freon control valve 3, steam exhaust valve 4, air extraction device 5, air cooling device 6, Condensed water control valve 7, gas-liquid separation device 8 and halogen detector 9; high-temperature and high-pressure steam control valve 1 is installed at the inlet of the high-temperature and high-pressure steam pipeline, and the middle part of the high-temperature and high-pressure steam pipeline is connected with Freon storage container 2, and the outlet of Freon storage container 2 Freon control valve 3 is installed at the place where the inspected valve is connected with the high-temperature and high-pressure steam inlet pipe and the exhaust steam pipe. The connection mode is determined by the structure of the inspected valve. The distance between the front end of the gas device 5 and the detection point on the surface of the tested valve is not more than 3mm, and the air cooling device 6 is integrated with the air extraction device 5, and the air flows through the air cooling device 6 to fully cool the gas pumped by the air extraction device 5 , the gas-liquid separation device 8 is installed at the end of the air extraction device 5, the condensate control valve 7 is installed at the bottom of the gas-liquid separation device 8, the probe of the halogen detector 9 is close to the lower edge of the gas outlet of the gas-liquid separation device 8, and the probe is connected to the outlet The horizontal distance of the gas port is not more than 3mm.

氟利昂阀门检漏新方法,在传统检测工质全部为氟利昂的基础上,提出了高温高压水蒸汽携带氟利昂作为工质的检测新方法,氟利昂与高温高压水蒸汽浓度比为1:10,该方法增大了检验工质的压力,减少了对环境的污染,精确检测受检阀门微泄漏点,为受检阀门泄漏量定级,在传统检测工质全部为氟利昂的基础上,增加了空气冷却装置6和气液分离装置8。利用氟利昂可作为示踪粒子的原理,先由氟利昂控制阀3通入氟利昂,再由高温高压蒸汽控制阀1通入高温高压水蒸汽,氟利昂与高温高压水蒸汽浓度比为1:10,高温高压水蒸汽与氟利昂的混合气体进入受检阀门,使用抽气装置5对受检阀门表面进行多点分步抽气,抽取的混合气体进入空气冷却装置6中冷却,混合气体中水蒸汽冷凝成液态水,随后液态水和氟利昂进入气液分离装置8,其中液态水经冷凝水控制阀7排出,卤素检测仪9在气液分离装置8出气口处进行最后定性检测以及确 定泄漏等级。A new method for leak detection of Freon valves. On the basis of the traditional detection of all Freon working fluids, a new detection method is proposed in which high-temperature and high-pressure water vapor carries Freon as a working medium. The concentration ratio of Freon to high-temperature and high-pressure water vapor is 1:10. Increase the pressure of the inspection medium, reduce the pollution to the environment, accurately detect the micro-leakage point of the inspected valve, and grade the leakage of the inspected valve. Device 6 and gas-liquid separation device 8. Utilizing the principle that freon can be used as tracer particles, freon is first introduced into freon through freon control valve 3, and then high-temperature and high-pressure steam is introduced through high-temperature and high-pressure steam control valve 1. The concentration ratio of freon to high-temperature and high-pressure water vapor is 1:10. The mixed gas of water vapor and freon enters the valve under test, and the surface of the valve under test is pumped at multiple points by using the air extraction device 5, and the extracted mixed gas enters the air cooling device 6 for cooling, and the water vapor in the mixed gas condenses into a liquid state Water, then liquid water and freon enter the gas-liquid separation device 8, wherein the liquid water is discharged through the condensate control valve 7, and the halogen detector 9 conducts final qualitative detection at the gas outlet of the gas-liquid separation device 8 and determines the leakage level.

本发明的效果和益处是:采用高温高压水蒸汽携带氟利昂示踪气体的模式,氟利昂与高温高压水蒸汽浓度比为1:10,增大了检验工质的压力,能够检测出更加微小的漏点;对阀门表面进行了三维多点分步抽气,确保了检测精度;减少了氟利昂较以往全氟检测的使用量,降低了因全部使用氟利昂气体进行检测造成的严重污染;通过对示踪气体氟利昂的检测来精确定位泄漏点的同时,研究示踪气体浓度与阀门泄漏等级之间的关系,进而确定泄漏等级;增加了冷却装置与气液分离装置,避免了因蒸汽温度过高对检测仪检测精度造成的影响。The effects and benefits of the present invention are: the mode of using high-temperature and high-pressure water vapor to carry Freon tracer gas, the concentration ratio of Freon to high-temperature and high-pressure water vapor is 1:10, which increases the pressure of the inspection working medium and can detect smaller leaks points; three-dimensional multi-point step-by-step pumping is carried out on the surface of the valve to ensure the detection accuracy; the use of freon is reduced compared with the previous perfluorinated detection, and the serious pollution caused by the use of freon gas for detection is reduced; through the tracer While detecting the gas freon to accurately locate the leak point, study the relationship between the tracer gas concentration and the valve leakage level, and then determine the leakage level; increase the cooling device and the gas-liquid separation device to avoid the detection due to excessive steam temperature The impact of the instrument detection accuracy.

附图说明Description of drawings

附图1是本发明氟利昂阀门检漏新方法的整体检测过程示意图。Accompanying drawing 1 is a schematic diagram of the overall detection process of the new method for leak detection of Freon valves of the present invention.

图1中:1高温高压蒸汽控制阀;2氟利昂储存容器;3氟利昂控制阀;4排蒸汽阀;5抽气装置;6空气冷却装置;7冷凝水控制阀;8气液分离装置;9卤素检测仪。In Fig. 1: 1 high temperature and high pressure steam control valve; 2 freon storage container; 3 freon control valve; 4 steam exhaust valve; 5 air extraction device; 6 air cooling device; 7 condensate water control valve; Detector.

具体实施方式detailed description

以下结合技术方案和附图详细叙述本发明的具体实施方式。The specific embodiments of the present invention will be described in detail below in conjunction with the technical solutions and accompanying drawings.

本发明工作过程如下:按装置示意图布置,将卤素检测仪9的探头对准气液分离装置8的出口,由于氟利昂气体密度比空气大,所以卤素检测仪9的探头要贴近气液分离装置8出气口的下沿,卤素检测仪9的探头与气液分离装置8出气口的水平距离为不大于3mm。打开高温高压蒸汽控制阀1、排蒸汽阀4和受检阀门,同时关闭氟利昂控制阀3,向进高温高压蒸汽管道通入高温高压水蒸汽排尽装置内的空气。随后关闭高温高压蒸汽控制阀1,待装置内压力恢复正常后,关闭受检阀门和排蒸汽阀4,打开氟利昂控制阀3,通入氟利昂后,关闭氟利昂控制阀3。随后,打开高温高压蒸汽控制阀1,通入高温高压水蒸汽,氟利昂与 高温高压水蒸汽浓度比为1:10,待氟利昂和高温高压水蒸汽混合均匀后打开受检阀门,同时使用抽气装置5对受检阀门表面进行多点分步抽气,抽气装置5前端不得马上移开,停留3秒后缓慢移动,且距离受检阀门的表面检测点的距离不大于3mm。如果受检阀门泄漏,那么抽取的气体为高温水蒸汽、氟利昂混合气体。随后,混合气体在空气冷却装置6中被流通空气冷却,其中水蒸汽冷凝为液态水,随后液态水和氟利昂进入气液分离装置8中,液态水由冷凝水控制阀7排出,从气液分离装置8出气口排出的氟利昂被抽入到卤素检测仪9中进行检测,卤素检测仪9发出蜂鸣声,根据卤素检测仪9报警指示灯亮的个数将泄漏量定级,以ITE-5650A-FP型号的卤素检漏仪为例,共划分为一到七级,即报警指示灯亮七个则泄漏量最多,定义为七级泄漏。如果受检阀门并未泄漏,则卤素检漏仪9报警指示灯按原频率闪烁,将不会发出蜂鸣声。The working process of the present invention is as follows: arrange according to the schematic diagram of the device, align the probe of the halogen detector 9 with the outlet of the gas-liquid separation device 8, and because the gas density of Freon is higher than that of air, the probe of the halogen detector 9 should be close to the gas-liquid separation device 8 The lower edge of the gas outlet, the horizontal distance between the probe of the halogen detector 9 and the gas outlet of the gas-liquid separation device 8 is not more than 3mm. Open the high-temperature and high-pressure steam control valve 1, the exhaust steam valve 4 and the inspected valve, and close the Freon control valve 3 at the same time, and pass the high-temperature and high-pressure steam into the high-temperature and high-pressure steam pipeline to exhaust the air in the device. Then close the high-temperature and high-pressure steam control valve 1. After the pressure in the device returns to normal, close the tested valve and the steam exhaust valve 4, open the Freon control valve 3, and close the Freon control valve 3 after the Freon is introduced. Then, open the high-temperature and high-pressure steam control valve 1, and introduce high-temperature and high-pressure steam. The concentration ratio of Freon and high-temperature and high-pressure steam is 1:10. 5. Perform multi-point and step-by-step pumping on the surface of the tested valve. The front end of the pumping device 5 must not be removed immediately. After staying for 3 seconds, move slowly, and the distance from the surface detection point of the tested valve is not greater than 3mm. If the valve under test leaks, the extracted gas is a mixture of high-temperature water vapor and Freon. Subsequently, the mixed gas is cooled by circulating air in the air cooling device 6, in which the water vapor is condensed into liquid water, and then the liquid water and Freon enter the gas-liquid separation device 8, and the liquid water is discharged by the condensate control valve 7, from the gas-liquid separation The freon discharged from the outlet of the device 8 is pumped into the halogen detector 9 for detection, the halogen detector 9 beeps, and the leakage is rated according to the number of the alarm indicators on the halogen detector 9, and the ITE-5650A- Taking the FP type halogen leak detector as an example, it is divided into one to seven levels, that is, the leakage amount is the most when the alarm indicator light is on seven, which is defined as seven levels of leakage. If the tested valve does not leak, the alarm indicator light of the halogen leak detector 9 will flash at the original frequency, and the buzzer will not sound.

Claims (1)

1.一种氟利昂阀门检漏方法,其特征在于,该方法所用的检测系统包括受检阀门、高温高压蒸汽控制阀、氟利昂储存容器、氟利昂控制阀、排蒸汽阀、抽气装置、空气冷却装置、冷凝水控制阀、气液分离装置和卤素检测仪;高温高压蒸汽管道进口处安装高温高压蒸汽控制阀,进高温高压蒸汽管道的中部与氟利昂储存容器连接,氟利昂储存容器出口处安装氟利昂控制阀,受检阀门与进高温高压蒸汽管道、排蒸汽管道相连接,连接方式由受检阀门的结构决定,排蒸汽阀安装在排蒸汽管道上靠近受检阀门位置,抽气装置前端距离受检阀门表面检测点的距离不大于3mm,空气冷却装置与抽气装置一体化连接,空气流过空气冷却装置,将抽气装置中抽到的气体充分冷却,气液分离装置安装在抽气装置的末端,气液分离装置的底部安装冷凝水控制阀,卤素检测仪的探头贴近气液分离装置出气口的下沿,探头与出气口的水平距离为不大于3mm;所述的氟利昂为高温化学性质稳定的氟利昂,具体方法如下:1. A Freon valve leak detection method, characterized in that the detection system used in the method comprises a valve under inspection, a high temperature and high pressure steam control valve, a Freon storage container, a Freon control valve, a steam exhaust valve, an air extraction device, and an air cooling device , condensed water control valve, gas-liquid separation device and halogen detector; install a high-temperature and high-pressure steam control valve at the inlet of the high-temperature and high-pressure steam pipeline, connect the middle part of the high-temperature and high-pressure steam pipeline with the Freon storage container, and install a Freon control valve at the outlet of the Freon storage container , the inspected valve is connected with the high-temperature and high-pressure steam inlet pipe and the steam exhaust pipe. The connection method is determined by the structure of the inspected valve. The distance between the surface detection points is not more than 3mm. The air cooling device is integrated with the air extraction device. The air flows through the air cooling device to fully cool the gas pumped in the air extraction device. The gas-liquid separation device is installed at the end of the air extraction device. , a condensate control valve is installed at the bottom of the gas-liquid separation device, the probe of the halogen detector is close to the lower edge of the gas outlet of the gas-liquid separation device, and the horizontal distance between the probe and the gas outlet is not more than 3mm; the Freon is high-temperature chemically stable Freon, the specific method is as follows: 利用氟利昂作为示踪粒子,先由氟利昂控制阀通入氟利昂,再由高温高压蒸汽控制阀通入高温高压水蒸汽,氟利昂与高温高压水蒸汽浓度比为1:10,高温高压水蒸汽与氟利昂的混合气体进入受检阀门,使用抽气装置对受检阀门表面进行多点分步抽气,抽取的混合气体进入空气冷却装置中冷却,混合气体中水蒸汽冷凝成液态水,随后液态水和氟利昂进入气液分离装置,其中液态水经冷凝水控制阀排出,卤素检测仪在气液分离装置出气口处进行最后定性检测以及确定泄漏等级。Using Freon as a tracer particle, the Freon control valve is first introduced into Freon, and then the high-temperature and high-pressure steam control valve is introduced into high-temperature and high-pressure steam. The mixed gas enters the tested valve, and the surface of the tested valve is pumped at multiple points by using the pumping device. The extracted mixed gas enters the air cooling device for cooling. The water vapor in the mixed gas condenses into liquid water, and then the liquid water and Freon Enter the gas-liquid separation device, where the liquid water is discharged through the condensate control valve, and the halogen detector performs the final qualitative detection at the gas outlet of the gas-liquid separation device to determine the leakage level.
CN201510184162.XA 2015-04-17 2015-04-17 Method for leakage detection of Freon valve Active CN104913886B (en)

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