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CN104928082A - Preparing method for composite type gentle and moistening soap base - Google Patents

Preparing method for composite type gentle and moistening soap base Download PDF

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Publication number
CN104928082A
CN104928082A CN201510340825.2A CN201510340825A CN104928082A CN 104928082 A CN104928082 A CN 104928082A CN 201510340825 A CN201510340825 A CN 201510340825A CN 104928082 A CN104928082 A CN 104928082A
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ratio
soap base
compound
soap
preparation
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CN201510340825.2A
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Chinese (zh)
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罗晓安
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Abstract

The invention provides a preparing method for a composite type gentle and moistening soap base. The preparing method for the composite type gentle and moistening soap base comprises the steps that saponification reaction is carried out on fatty acid with the proportion ranging from 8% to 30%, polyhydric alcohol with the proportion ranging from 20% to 52%, cane sugar with the proportion ranging from 8% to 27.5%, purified water with the proportion ranging from 3% to 22%, a surface active agent with the proportion ranging from 1% to 18% through sodium hydroxide with the proportion ranging from 3% to 7.5%. The method has the advantages that repeated dissolution can be achieved, the utilization rate can be increased, polyhydric alcohol moisture components are added in the production process, the skin irritant of the soap is lowered, and the moisture degree on the skin is improved. Wastes are not produced in the producing process, big-scaled devices and middle-scaled devices are not needed, a producing device is simple, and minimum conditions and factory mass production conditions exist. In addition, the repeated utilization rate of the soap base is high, redissolution can be carried out on the soap with the mass production due to the inaccurate statistical quantity during producing, the soap with other types can be manufactured, and the resource wastes cannot be caused.

Description

A kind of compound gentleness moistens the preparation method of soap base
Technical field
The present invention relates to the technical field of soap, refer more particularly to the preparation method that a kind of compound gentleness moistens soap base.
Background technology
Traditional perfumed soap (representative has comfortable good perfumed soap, vertical white perfumed soap etc.) mainly manufactures raw material: soap base (perfumed soap hereafter mentioned makes raw material and all refers to soap base) can only rely on heavy-duty machines equipment vegetables oil or animal oil, recovery wet goods by following sodium hydroxide to carry out and saponification reaction obtain soap base, water and glycerine, extrude shaping after soap base is carried out vacuum-drying and become neat soap, byproduct glycerine and effluent part, the method is relatively traditional, there is certain waste water to produce, the place of certain area need be possessed and buy expensive equipment and technician.
If this soap base occurs that in production link mishandle will cause this batch all to be scrapped, cauldron can not be thrown back for regenerative ratio, cause the waste of resource.
This soap base has taken out the glycerin components with moisturizing effect in production final tache, residue major part is fatty dry soda soap, if wash for the production of middle and high ends such as the clean facial soaps of makeup and protect product and non-optimal, pungency is large, alkalescence (pH value) is high, and cleaning capacity easily allows by force people do not feel like oneself.
The traditional perfumed soap adopting this soap base to make also needs the using area of corresponding big-and-middle-sized equipment and certain area, machine energy consumption is large, conflict with energy-saving and emission-reduction, production process is many, from feeding intake → be uniformly mixed → grinding chips → extrude shaping → punching press printing → final product, is also not suitable for little Wei enterprise that current government encourage develops and electric commercial business industry.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, providing the preparation method that a kind of compound gentleness moistens soap base.
The present invention is realized by above technical scheme:
The invention provides the preparation method that a kind of compound gentleness moistens soap base, the preparation method that this compound gentleness moistens soap base is: by the pure water of the sucrose of the polyvalent alcohol of the lipid acid of 8% ~ 30% ratio, 20% ~ 52% ratio, 8% ~ 27.5% ratio, 3% ~ 22% ratio, the tensio-active agent of 1% ~ 18% ratio by carrying out saponification reaction with the sodium hydroxide of 3% ~ 7.5% ratio.
Preferably, the titanium dioxide also comprising interpolation 0.05% ~ 0.12% ratio carries out saponification reaction.
Preferably, described the pure water of the sucrose of the polyvalent alcohol of the lipid acid of 8% ~ 30% ratio, 20% ~ 52% ratio, 8% ~ 27.5% ratio, 3% ~ 22% ratio, the tensio-active agent of 1% ~ 18% ratio to be specially by carrying out saponification reaction with the sodium hydroxide of 3% ~ 7.5% ratio:
The lipid acid of 8% ~ 30% ratio is heated until dissolve completely in heating cylinder;
Add the polyvalent alcohol of 20% ~ 52% ratio fully to mix with lipid acid, and with the speed of per minute 36 turns at the uniform velocity dispersed with stirring 8 ~ 20 minutes;
The tensio-active agent adding 1% ~ 18% ratio continues stirring 5 ~ 20 minutes;
The sodium hydroxide of the pure water and 3% ~ 7.5% ratio that add 3% ~ 22% ratio continues stirring allows each composition fully carry out saponification reaction for 10 ~ 20 minutes;
Stop heating after the sucrose adding 8% ~ 27.5% ratio stirs and stir;
Leave standstill to allow for 2 ~ 10 minutes and obtain compound gentleness after the removal of foam and moisten soap base.
Preferably, described the fatty acids of 8% ~ 30% ratio to be heated until consoluet temperature controls between 70 ~ 90 degree in heating cylinder.
Preferably, described lipid acid is the higher fatty acid that vegetables oil obtains after High Temperature High Pressure continuous hydrolysis.
Preferably, described vegetables oil is plam oil, palm-kernel oil or Oleum Cocois.
Preferably, described lipid acid is lauric acid, tetradecanoic acid, palmitinic acid or stearic acid.
Preferably, described polyvalent alcohol is propylene glycol, glycerol, Xylitol or sorbyl alcohol.
The invention has the beneficial effects as follows: have repeatedly to melt and increase operation rate, production link is added with polyvalent alcohol moisturizing composition, the pungency reducing soap improves the moist degree to skin simultaneously.And do not produce waste material (byproduct), waste water, waste gas in production link, all adding materials are all fully saponified, to environment and ecological pollution-free.Adopt plurality of raw materials by accurate compound proportioning, in raw material, major part is all pharmaceutical grade or food grade materials.And in process of production, this soap base is adopted to make finished product soap without the need to big-and-middle-sized equipment, production unit is simple, minimal condition can be had to follow factory's volume production condition: minimal condition, only needs a beaker or high temperature resistant utensil, a heating installation, a mould, can complete the process making finished product soap from soap base, need not the machine knowledge of complicated specialty, without the need to excessive place, 10 square meter ~ 20 square meters just can solve place problem.Factory's volume production condition: the place of 70 square meters, a stainless steel heating cylinder, Zhang Gong's station, some moulds, 2 ~ 4 workmans can operate volume production.
In addition, this soap base repeating utilization factor is high, for the soap that the output that production causes because statistical magnitude is inaccurate is too much, can be made into the soap of other type, can not cause the waste in resource after dissolving again.
Accompanying drawing explanation
Fig. 1 is the schema that compound gentleness that the embodiment of the present invention provides moistens the preparation method of soap base.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with drawings and Examples, the present invention is further elaborated.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not intended to limit the present invention.
Embodiments provide the preparation method that a kind of compound gentleness moistens soap base, the preparation method that this compound gentleness moistens soap base is:
By the pure water of the sucrose of the polyvalent alcohol of the lipid acid of 8% ~ 30% ratio, 20% ~ 52% ratio, 8% ~ 27.5% ratio, 3% ~ 22% ratio, the tensio-active agent of 1% ~ 18% ratio by carrying out saponification reaction with the sodium hydroxide of 3% ~ 7.5% ratio.
In the above-mentioned methods, can be found out by each composition, the preparation method of the soap base provided in present method has repeatedly to melt and increases operation rate, and production link is added with in polyvalent alcohol has moisturizing composition, and the pungency reducing soap improves the moist degree to skin simultaneously.Do not produce waste material (byproduct), waste water, waste gas in production link, all adding materials are all fully saponified, to environment and ecological pollution-free.Adopt plurality of raw materials by accurate compound proportioning, in raw material, major part is all pharmaceutical grade or food grade materials.In concrete production process, this soap base is adopted to make finished product soap without the need to big-and-middle-sized equipment, minimal condition can be had to follow factory's volume production condition: minimal condition, only need a beaker or high temperature resistant utensil, a heating installation, a mould, the process making finished product soap from soap base can be completed, need not the machine knowledge of complicated specialty, without the need to excessive place, 10 square meter ~ 20 square meters just can solve place problem.Factory's volume production condition: places more than 70 square meters, a stainless steel heating cylinder, Zhang Gong's station, some moulds, 2 ~ 4 workmans can operate volume production.
In addition, this soap base repeating utilization factor is high, for the soap that the output that production causes because statistical magnitude is inaccurate is too much, can be made into the soap of other type, can not cause the waste in resource after dissolving again.
In addition, when the soap base needing preparation oyster white opaque, titanium dioxide can be added, concrete, in mentioned component, add the titanium dioxide of 0.05% ~ 0.12% ratio, after saponification reaction, form the opaque soap base of oyster white.
In order to the making method of the soap base that the detailed understanding embodiment of the present invention provides, below in conjunction with accompanying drawing 1, its production stage is described in detail.
Step 001: the lipid acid of 8% ~ 30% ratio is heated until dissolve completely in heating cylinder;
Concrete, the lipid acid that the present embodiment adopts is the higher fatty acid that vegetables oil obtains after High Temperature High Pressure continuous hydrolysis.Be specially: lauric acid, tetradecanoic acid, palmitinic acid or stearic acid.The vegetables oil adopted when preparing higher fatty acid can be plam oil, palm-kernel oil or Oleum Cocois.In addition, when heating for dissolving, temperature controls between 70 ~ 90 degree.As: the temperature arbitrarily between 70 ~ 90 degree such as 70 degree, 75 degree, 80 degree, 85 degree, 90 degree.
Step 002, add the polyvalent alcohol of 20% ~ 52% ratio and fully mix with lipid acid, and with the speed of per minute 36 turns at the uniform velocity dispersed with stirring 8 ~ 20 minutes;
In concrete whipping process, the time length can be 8 minutes, 10 minutes, 15 minutes, 20 minutes etc. arbitrarily between the time of 8 ~ 20 minutes, and fully to mix between polyvalent alcohol with lipid acid after ensureing to stir.This well-mixed standard is get the liquid of the unit volume of different positions, and in different unit liquid, the error of the ratio shared by both is in the scope of setting.
Polyvalent alcohol wherein can adopt different polyvalent alcohols, as propylene glycol, glycerol, Xylitol or sorbyl alcohol.
The tensio-active agent of step 003, interpolation 1% ~ 18% ratio continues stirring 5 ~ 20 minutes;
The sodium hydroxide of step 004, the pure water adding 3% ~ 22% ratio and 3% ~ 7.5% ratio continues stirring allows each composition fully carry out saponification reaction for 10 ~ 20 minutes;
Stop heating after step 005, the sucrose adding 8% ~ 27.5% ratio stir and stir;
Step 006, leave standstill to allow for 2 ~ 10 minutes and obtain compound gentleness after the removal of foam and moisten soap base.
In above-mentioned concrete preparation method, heterogeneity can adopt different ratios, the proportional range of each composition when preparing soap base is given in above-mentioned concrete preparation method, when specifically using, can select according to the proportional range in above-mentioned each composition, enumerate below several specifically prepare soap base time composition.
Embodiment 1
By the pure water of the sucrose of the polyvalent alcohol of the lipid acid of 8% ratio, 20% ratio, 25% ratio, 22% ratio, the tensio-active agent of 18% ratio by carrying out saponification reaction with sodium hydroxide 7%.
Embodiment 2
By the pure water of the sucrose of the polyvalent alcohol of the lipid acid of 30% ratio, 20% ratio, 22% ratio, 3% ratio, the tensio-active agent of 18% ratio by carrying out saponification reaction with sodium hydroxide 7%.
Embodiment 3
By the tensio-active agent of the pure water of the sucrose of the polyvalent alcohol of the lipid acid of 20% ratio, 30% ratio, 20% ratio, 15% ratio, 9.95% ratio, 0.05% titanium dioxide by carrying out saponification reaction with sodium hydroxide 5%.
Embodiment 4
By the pure water of the sucrose of the polyvalent alcohol of lipid acid 40% ratio of 20% ratio, 10% ratio, 15% ratio, the tensio-active agent of 11.9% ratio, the titanium dioxide of 0.1% ratio by carrying out saponification reaction with sodium hydroxide 3%.
Embodiment 5
By the pure water of the sucrose of the polyvalent alcohol of the lipid acid of 15% ratio, 52% ratio, 26% ratio, 3% ratio, the tensio-active agent of 1% ratio by carrying out saponification reaction with sodium hydroxide 3%.
Can be found out by above-mentioned specific embodiment, the preparation method of the soap base that the present embodiment provides can select according to the proportional range of each composition provided, thus the required soap base of system.
These are only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.

Claims (8)

1. a compound gentleness moistens the preparation method of soap base, it is characterized in that, by the pure water of the sucrose of the polyvalent alcohol of the lipid acid of 8% ~ 30% ratio, 20% ~ 52% ratio, 8% ~ 27.5% ratio, 3% ~ 22% ratio, the tensio-active agent of 1% ~ 18% ratio by carrying out saponification reaction with the sodium hydroxide of 3% ~ 7.5% ratio.
2. compound gentleness according to claim 1 moistens the preparation method of soap base, it is characterized in that, the titanium dioxide also comprising interpolation 0.05% ~ 0.12% ratio carries out saponification reaction.
3. compound gentleness according to claim 2 moistens the preparation method of soap base, it is characterized in that, described the pure water of the sucrose of the polyvalent alcohol of the lipid acid of 8% ~ 30% ratio, 20% ~ 52% ratio, 8% ~ 27.5% ratio, 3% ~ 22% ratio, the tensio-active agent of 1% ~ 18% ratio to be specially by carrying out saponification reaction with the sodium hydroxide of 3% ~ 7.5% ratio:
The lipid acid of 8% ~ 30% ratio is heated until dissolve completely in heating cylinder;
Add the polyvalent alcohol of 20% ~ 52% ratio fully to mix with lipid acid, and with the speed of per minute 36 turns at the uniform velocity dispersed with stirring 8 ~ 20 minutes;
The tensio-active agent adding 1% ~ 18% ratio continues stirring 5 ~ 20 minutes;
The sodium hydroxide of the pure water and 3% ~ 7.5% ratio that add 3% ~ 22% ratio continues stirring allows each composition fully carry out saponification reaction for 10 ~ 20 minutes;
Stop heating after the sucrose adding 8% ~ 27.5% ratio stirs and stir;
Leave standstill to allow for 2 ~ 10 minutes and obtain compound gentleness after the removal of foam and moisten soap base.
4. compound gentleness according to claim 3 moistens the preparation method of soap base, it is characterized in that, describedly in heating cylinder, heats the fatty acids of 8% ~ 30% ratio until consoluet temperature controls between 70 ~ 90 degree.
5. compound gentleness according to claim 1 moistens the preparation method of soap base, it is characterized in that, described lipid acid is the higher fatty acid that vegetables oil obtains after High Temperature High Pressure continuous hydrolysis.
6. compound gentleness according to claim 5 moistens the preparation method of soap base, it is characterized in that, described vegetables oil is plam oil, palm-kernel oil or Oleum Cocois.
7. compound gentleness according to claim 5 moistens the preparation method of soap base, it is characterized in that, described lipid acid is lauric acid, tetradecanoic acid, palmitinic acid or stearic acid.
8. compound gentleness according to claim 1 moistens the preparation method of soap base, it is characterized in that, described polyvalent alcohol is propylene glycol, glycerol, Xylitol or sorbyl alcohol.
CN201510340825.2A 2015-06-18 2015-06-18 Preparing method for composite type gentle and moistening soap base Pending CN104928082A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106883959A (en) * 2017-02-24 2017-06-23 浙江如美日化有限公司 A kind of Chinese torreya essential oil soap
CN106978288A (en) * 2017-05-05 2017-07-25 陈磊 A kind of handmade soap containing Composition of Meteorite and preparation method thereof
CN109179745A (en) * 2018-08-29 2019-01-11 杭州轩辉环境设备有限公司 A kind for the treatment of process for the waste water producing fatty acid generation

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1535310A (en) * 2001-07-23 2004-10-06 Improved detergent bar and process for making same
CN101341242A (en) * 2005-12-21 2009-01-07 高露洁-棕榄公司 Soap composition with capsules
CN103013715A (en) * 2012-12-20 2013-04-03 广东鹏锦实业有限公司 Transparent soap
CN101445773B (en) * 2008-12-20 2013-05-29 汕头市大千高新科技研究中心有限公司 Method for preparing fancy soap
CN103232910A (en) * 2013-04-28 2013-08-07 广州丹奇日用化工厂有限公司 Transparent handmade soap and preparation method thereof
WO2013131307A1 (en) * 2012-03-07 2013-09-12 南京华狮化工有限公司 Transparent beauty soap composition

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1535310A (en) * 2001-07-23 2004-10-06 Improved detergent bar and process for making same
CN101341242A (en) * 2005-12-21 2009-01-07 高露洁-棕榄公司 Soap composition with capsules
CN101445773B (en) * 2008-12-20 2013-05-29 汕头市大千高新科技研究中心有限公司 Method for preparing fancy soap
WO2013131307A1 (en) * 2012-03-07 2013-09-12 南京华狮化工有限公司 Transparent beauty soap composition
CN103013715A (en) * 2012-12-20 2013-04-03 广东鹏锦实业有限公司 Transparent soap
CN103232910A (en) * 2013-04-28 2013-08-07 广州丹奇日用化工厂有限公司 Transparent handmade soap and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106883959A (en) * 2017-02-24 2017-06-23 浙江如美日化有限公司 A kind of Chinese torreya essential oil soap
CN106978288A (en) * 2017-05-05 2017-07-25 陈磊 A kind of handmade soap containing Composition of Meteorite and preparation method thereof
CN109179745A (en) * 2018-08-29 2019-01-11 杭州轩辉环境设备有限公司 A kind for the treatment of process for the waste water producing fatty acid generation

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Effective date of registration: 20160419

Address after: 518000 Guangdong province Shenzhen city Longhua District Guanlan Fumin Street community size lion Road No. 13 outside industrial park building B 3

Applicant after: Shenzhen Zhuo wild commodity Limited company

Address before: 518000 Guangdong province Shenzhen city Longhua District Guanlan Fumin Street Community Road No. 13 by Lion Industrial Park B building 3 floor

Applicant before: Luo Xiaoan

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RJ01 Rejection of invention patent application after publication

Application publication date: 20150923