CN105670828A - Polyvinyl acetate-plant mixed cleaner and preparation method thereof - Google Patents
Polyvinyl acetate-plant mixed cleaner and preparation method thereof Download PDFInfo
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- CN105670828A CN105670828A CN201610111111.9A CN201610111111A CN105670828A CN 105670828 A CN105670828 A CN 105670828A CN 201610111111 A CN201610111111 A CN 201610111111A CN 105670828 A CN105670828 A CN 105670828A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 229920002554 vinyl polymer Polymers 0.000 title claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 37
- AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Chemical compound OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 claims abstract description 16
- -1 alkyl phenol Chemical compound 0.000 claims abstract description 15
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims abstract description 10
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 150000003863 ammonium salts Chemical class 0.000 claims abstract description 8
- 239000012153 distilled water Substances 0.000 claims abstract description 8
- 239000000463 material Substances 0.000 claims abstract description 8
- VYQNWZOUAUKGHI-UHFFFAOYSA-N monobenzone Chemical compound C1=CC(O)=CC=C1OCC1=CC=CC=C1 VYQNWZOUAUKGHI-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 8
- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical compound [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 claims abstract description 8
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims abstract description 5
- 238000002156 mixing Methods 0.000 claims description 15
- 241001122767 Theaceae Species 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- 239000002253 acid Substances 0.000 claims description 10
- 229910052708 sodium Inorganic materials 0.000 claims description 9
- 239000011734 sodium Substances 0.000 claims description 9
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 7
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 7
- 229960004275 glycolic acid Drugs 0.000 claims description 7
- 229920001206 natural gum Polymers 0.000 claims description 7
- 235000019394 potassium persulphate Nutrition 0.000 claims description 7
- 210000000582 semen Anatomy 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 6
- 239000011259 mixed solution Substances 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 5
- 102000004160 Phosphoric Monoester Hydrolases Human genes 0.000 claims description 3
- 108090000608 Phosphoric Monoester Hydrolases Proteins 0.000 claims description 3
- 238000010025 steaming Methods 0.000 claims description 3
- 229920002689 polyvinyl acetate Polymers 0.000 claims 1
- 239000011118 polyvinyl acetate Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 5
- 238000005516 engineering process Methods 0.000 abstract description 4
- 238000000034 method Methods 0.000 abstract description 3
- 241000196324 Embryophyta Species 0.000 abstract description 2
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 238000004140 cleaning Methods 0.000 abstract description 2
- 230000003472 neutralizing effect Effects 0.000 abstract description 2
- 244000037364 Cinnamomum aromaticum Species 0.000 abstract 1
- 235000014489 Cinnamomum aromaticum Nutrition 0.000 abstract 1
- 241000693687 Draba nemorosa Species 0.000 abstract 1
- 241000218671 Ephedra Species 0.000 abstract 1
- IMROMDMJAWUWLK-UHFFFAOYSA-N Ethenol Chemical compound OC=C IMROMDMJAWUWLK-UHFFFAOYSA-N 0.000 abstract 1
- 241000935235 Fritillaria meleagris Species 0.000 abstract 1
- 244000303040 Glycyrrhiza glabra Species 0.000 abstract 1
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 abstract 1
- 235000017443 Hedysarum boreale Nutrition 0.000 abstract 1
- 235000007858 Hedysarum occidentale Nutrition 0.000 abstract 1
- 241001522232 Pinellia ternata Species 0.000 abstract 1
- 240000006079 Schisandra chinensis Species 0.000 abstract 1
- 244000269722 Thea sinensis Species 0.000 abstract 1
- 238000005202 decontamination Methods 0.000 abstract 1
- 230000003588 decontaminative effect Effects 0.000 abstract 1
- 235000013399 edible fruits Nutrition 0.000 abstract 1
- ZOOODBUHSVUZEM-UHFFFAOYSA-N ethoxymethanedithioic acid Chemical compound CCOC(S)=S ZOOODBUHSVUZEM-UHFFFAOYSA-N 0.000 abstract 1
- 239000001947 glycyrrhiza glabra rhizome/root Substances 0.000 abstract 1
- 238000006386 neutralization reaction Methods 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 159000000000 sodium salts Chemical class 0.000 abstract 1
- 239000012991 xanthate Substances 0.000 abstract 1
- 239000003599 detergent Substances 0.000 description 4
- 239000013042 solid detergent Substances 0.000 description 4
- 239000012752 auxiliary agent Substances 0.000 description 2
- 239000011324 bead Substances 0.000 description 2
- 238000001694 spray drying Methods 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 230000002159 abnormal effect Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229940077388 benzenesulfonate Drugs 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 235000019832 sodium triphosphate Nutrition 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000271 synthetic detergent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/042—Acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2082—Polycarboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2093—Esters; Carbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3753—Polyvinylalcohol; Ethers or esters thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
- C11D1/721—End blocked ethers
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Inorganic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a polyvinyl acetate-plant mixed cleaner and a preparation method thereof. The polyvinyl acetate-plant mixed cleaner is prepared from the following materials in percentage by weight: 18-22 parts of phosphoric acid, 16-19 parts of glycolic acid, 11-14 parts of oxethyl ammonium salt of alkyl phenol, 11-12 parts of ethenyl tetraaceticacid tetrasodium, 11-13 parts of xanthate gum, 6-8 parts of vinol, 7-12 parts of OP-10, 12-15 parts of dodecyl-benzenesulfonic aci sodium salt, 12-15 parts of potassium peroxodisulfate, 50-55 parts of distilled water, 3-6 parts of vinyl acetate, 4-5 parts of Draba nemorosa L., 10-12 parts of cassia twig, 10-12 parts of radix paeoniae alba, 10-12 parts of rhizoma zingiberis, 8-10 parts of herba ephedra, 8-10 parts of pinellia ternata, 5-8 parts of thunberg fritillary bulb, 3-5 parts of herba asari, 10-15 parts of the fruit of Chinese magnoliavine, 8-10 parts of licorice root and 4-5 scented tea particles. The polyvinyl acetate-plant mixed cleaner has the beneficial effects that the prepared cleaner is simple and convenient in preparation technology, and is not pungent in a cleaning process, plant components in the formula are used for neutralizing, environment friendliness is realized, pollution is avoided, in the application of the cleaner, places contaminated by petrol and the like are cleaned as key points, and compared with a common cleaner, the cleaner is good in decontamination effect, strong in neutralization capability and obvious in use effect.
Description
Technical field:
The present invention relates to industrial chemicals preparing technical field, concrete one relates to polyvinyl acetate-plant mixing abluent and preparation method thereof.
Background technology:
Abluent is configured to by surfactant (such as sodium alkyl benzene sulfonate, sodium alkyl sulfate) and various auxiliary agent (such as sodium tripolyphosphate), adjuvant, during dirt on washings surface, the surface tension of aqueous solution can be reduced, improve the material of clean effect. It is divided into solid detergent, liquid detergent by product appearance form. Solid detergent yield is maximum, claims detergent traditionally, including fine-powdered, graininess and hollow bead shape etc. Also has detergent paste therebetween, also referred to as washing cream. All kinds of synthetic detergents have different production technologies, wherein complicated with solid detergent. Countries in the world generally produce hollow bead shape solid detergent, adopt high tower spray drying method, and its master operation has Pulp preparation, spray drying, wind to send aging and packaging. Liquid detergent manufactures simplicity, only need to by surfactant, auxiliary agent and other additives, and treated water, sending into mixer to carry out mixing, existing abluent abnormal smells from the patient is pungent, containing a large amount of pollution elements in abluent, flow in subsoil water and river, cause serious environmental pollution.
Summary of the invention:
The technical problem to be solved is in that to overcome the defect of prior art, it is provided that one relates to polyvinyl acetate-plant mixing abluent and preparation method thereof.
The technical problem to be solved realizes by the following technical solutions.
Polyvinyl acetate-plant mixing abluent, it is characterized in that: including percentage by weight is, phosphatase 11 8-22 part, hydroxyacetic acid 16-19 part, ethyoxyl ammonium salt 11-14 part of alkyl phenol, ethylidine tetraacethyl four sodium 11-12 part, xanthic acid natural gum 11-13 part, polyvinyl alcohol 6-8 part, 7-12 part OP-10, pelopon A 12-15 part, potassium peroxydisulfate 12-15 part, distilled water 50-55 part, vinyl acetate 3-6 part, Semen Lepidii 4-5 part, Ramulus Cinnamomi 10-12 part, Radix Paeoniae Alba 10-12 part, Rhizoma Zingiberis 10-12 part, Herba Ephedrae 8-10 part, Rhizoma Pinelliae 8-10 part, Bulbus Fritillariae Thunbergii 5-8 part, Herba Asari 3-5 part, Fructus Schisandrae Chinensis 10-15 part, Radix Glycyrrhizae 8-10 part, scented tea 4-5 grain.
Preparation process is: polyvinyl alcohol, OP-10, pelopon A, potassium peroxydisulfate is added in agitator, stirs 10 minutes, obtains stirring mixed solution; Being poured into by distilled water in agitator tank, heat, temperature controls at 60-70 DEG C, 10-20 minute, is completely dissolved to water with stirring mixed solution; Again heating, temperature controls at 70-80 DEG C, heats 30 minutes; Add vinyl acetate, maintain reaction 4 hours of heating, obtain intermixture;
By the Semen Lepidii in constitutive material, Ramulus Cinnamomi, the Radix Paeoniae Alba, Rhizoma Zingiberis, Herba Ephedrae, the Rhizoma Pinelliae, Bulbus Fritillariae Thunbergii, Herba Asari, Fructus Schisandrae Chinensis and Radix Glycyrrhizae, putting in alembic, add the clear water of 5 times, steaming and decocting, the water to alembic is evaporated, and collects steam, and steam liquefies again; Being put into by scented tea in boiled water simultaneously and soak, the water yield is 300ml, soaks 5-8 minute, crosses drainage, obtains scented tea water; Again the steam collected is mixed with scented tea water, take out foreign material, obtain mixed liquor;
First time takes the intermixture of 5% and the mixed liquor mix and blend of 8%, second time takes the intermixture of 9% and the mixed liquor mixing of 3% again, third time takes the intermixture of 2% and the mixed liquor mix and blend of 6%, three times are mixed gained liquid and adds in acid-resistant tank, add a certain amount of water, stirring adds a certain amount of phosphoric acid, add a certain amount of hydroxyacetic acid, add the ethyoxyl ammonium salt of a certain amount of alkyl phenol, add a certain amount of ethylidine tetraacethyl four sodium, it is eventually adding a certain amount of xanthic acid natural gum, add the water mixing of surplus, it is stirred for 20 minutes, obtain abluent.
The invention has the beneficial effects as follows: the abluent of preparation in the present invention, it has preparation technology simple and convenient, cleaning process is not pungent, formula passes through in plant component with environment friendly and pollution-free, in the application, emphasis cleans oil etc. and pollutes, good relative to common abluent clean effect simultaneously, neutralising capacity is strong, and result of use is obvious.
Detailed description of the invention:
For the technological means making the present invention realize, creation characteristic, reach purpose and effect and be easy to understand, below in conjunction with specific embodiment, the present invention is expanded on further.
Specific embodiment 1: polyvinyl acetate-plant mixing abluent, including percentage by weight be, phosphatase 11 8 parts, hydroxyacetic acid 16 parts, the ethyoxyl ammonium salt of alkyl phenol 11 parts, 11 parts of ethylidine tetraacethyl four sodium, xanthic acid natural gum 11 parts, polyvinyl alcohol 6 parts, 7 parts of OP-10, pelopon A 12 parts, potassium peroxydisulfate 12 parts, distilled water 50 parts, vinyl acetate 3 parts, Semen Lepidii 4 parts, Ramulus Cinnamomi 10 parts, the Radix Paeoniae Alba 10 parts, Rhizoma Zingiberis 10 parts, Herba Ephedrae 8-10 part, the Rhizoma Pinelliae 8 parts, Bulbus Fritillariae Thunbergii 5 parts, Herba Asari 3 parts, Fructus Schisandrae Chinensis 10 parts, 8 parts of Radix Glycyrrhizae, scented tea 4.
Specific embodiment 2: polyvinyl acetate-plant mixing abluent, including percentage by weight be, phosphoric acid 22 parts, hydroxyacetic acid 19 parts, the ethyoxyl ammonium salt of alkyl phenol 14 parts, 12 parts of ethylidine tetraacethyl four sodium, xanthic acid natural gum 13 parts, polyvinyl alcohol 8 parts, 12 parts of OP-10, pelopon A 15 parts, potassium peroxydisulfate 15 parts, distilled water 55 parts, vinyl acetate 6 parts, Semen Lepidii 5 parts, Ramulus Cinnamomi 12 parts, the Radix Paeoniae Alba 12 parts, Rhizoma Zingiberis 12 parts, 10 parts of Herba Ephedrae, the Rhizoma Pinelliae 10 parts, Bulbus Fritillariae Thunbergii 8 parts, Herba Asari 5 parts, Fructus Schisandrae Chinensis 15 parts, 10 parts of Radix Glycyrrhizae, scented tea 5.
Preparation process is: polyvinyl alcohol, OP-10, pelopon A, potassium peroxydisulfate is added in agitator, stirs 10 minutes, obtains stirring mixed solution;Being poured into by distilled water in agitator tank, heat, temperature controls at 60-70 DEG C, 10-20 minute, is completely dissolved to water with stirring mixed solution; Again heating, temperature controls at 70-80 DEG C, heats 30 minutes; Add vinyl acetate, maintain reaction 4 hours of heating, obtain intermixture;
By the Semen Lepidii in constitutive material, Ramulus Cinnamomi, the Radix Paeoniae Alba, Rhizoma Zingiberis, Herba Ephedrae, the Rhizoma Pinelliae, Bulbus Fritillariae Thunbergii, Herba Asari, Fructus Schisandrae Chinensis and Radix Glycyrrhizae, putting in alembic, add the clear water of 5 times, steaming and decocting, the water to alembic is evaporated, and collects steam, and steam liquefies again; Being put into by scented tea in boiled water simultaneously and soak, the water yield is 300ml, soaks 5-8 minute, crosses drainage, obtains scented tea water; Again the steam collected is mixed with scented tea water, take out foreign material, obtain mixed liquor;
First time takes the intermixture of 5% and the mixed liquor mix and blend of 8%, second time takes the intermixture of 9% and the mixed liquor mixing of 3% again, third time takes the intermixture of 2% and the mixed liquor mix and blend of 6%, three times are mixed gained liquid and adds in acid-resistant tank, add a certain amount of water, stirring adds a certain amount of phosphoric acid, add a certain amount of hydroxyacetic acid, add the ethyoxyl ammonium salt of a certain amount of alkyl phenol, add a certain amount of ethylidine tetraacethyl four sodium, it is eventually adding a certain amount of xanthic acid natural gum, add the water mixing of surplus, it is stirred for 20 minutes, obtain abluent.
The ultimate principle of the present invention, principal character and advantages of the present invention have more than been shown and described. Skilled person will appreciate that of the industry; the present invention is not restricted to the described embodiments; described in above-described embodiment and description is that principles of the invention is described; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements both fall within the claimed scope of the invention. Claimed scope is defined by appending claims and equivalent thereof.
Claims (2)
1. polyvinyl acetate-plant mixing abluent, it is characterized in that: including percentage by weight is, phosphatase 11 8-22 part, hydroxyacetic acid 16-19 part, ethyoxyl ammonium salt 11-14 part of alkyl phenol, ethylidine tetraacethyl four sodium 11-12 part, xanthic acid natural gum 11-13 part, polyvinyl alcohol 6-8 part, 7-12 part OP-10, pelopon A 12-15 part, potassium peroxydisulfate 12-15 part, distilled water 50-55 part, vinyl acetate 3-6 part, Semen Lepidii 4-5g, Ramulus Cinnamomi 10-12g, Radix Paeoniae Alba 10-12g, Rhizoma Zingiberis 10-12g, Herba Ephedrae 8-10g, Rhizoma Pinelliae 8-10g, Bulbus Fritillariae Thunbergii 5-8g, Herba Asari 3-5g, Fructus Schisandrae Chinensis 10-15g, Radix Glycyrrhizae 8-10g, scented tea 4-5 grain.
2. polyvinyl acetate according to claim 1-plant mixing abluent, it is characterised in that: preparation process is:
Polyvinyl alcohol, OP-10, pelopon A, potassium peroxydisulfate are added in agitator, stirs 10 minutes, obtain stirring mixed solution; Being poured into by distilled water in agitator tank, heat, temperature controls at 60-70 DEG C, 10-20 minute, is completely dissolved to water with stirring mixed solution; Again heating, temperature controls at 70-80 DEG C, heats 30 minutes; Add vinyl acetate, maintain reaction 4 hours of heating, obtain intermixture;
By the Semen Lepidii in constitutive material, Ramulus Cinnamomi, the Radix Paeoniae Alba, Rhizoma Zingiberis, Herba Ephedrae, the Rhizoma Pinelliae, Bulbus Fritillariae Thunbergii, Herba Asari, Fructus Schisandrae Chinensis and Radix Glycyrrhizae, putting in alembic, add the clear water of 5 times, steaming and decocting, the water to alembic is evaporated, and collects steam, and steam liquefies again;Being put into by scented tea in boiled water simultaneously and soak, the water yield is 300ml, soaks 5-8 minute, crosses drainage, obtains scented tea water; Again the steam collected is mixed with scented tea water, take out foreign material, obtain mixed liquor;
First time takes the intermixture of 5% and the mixed liquor mix and blend of 8%, second time takes the intermixture of 9% and the mixed liquor mixing of 3% again, third time takes the intermixture of 2% and the mixed liquor mix and blend of 6%, three times are mixed gained liquid and adds in acid-resistant tank, add a certain amount of water, stirring adds a certain amount of phosphoric acid, add a certain amount of hydroxyacetic acid, add the ethyoxyl ammonium salt of a certain amount of alkyl phenol, add a certain amount of ethylidine tetraacethyl four sodium, it is eventually adding a certain amount of xanthic acid natural gum, add the water mixing of surplus, it is stirred for 20 minutes, obtain abluent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610111111.9A CN105670828A (en) | 2016-02-29 | 2016-02-29 | Polyvinyl acetate-plant mixed cleaner and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610111111.9A CN105670828A (en) | 2016-02-29 | 2016-02-29 | Polyvinyl acetate-plant mixed cleaner and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105670828A true CN105670828A (en) | 2016-06-15 |
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| CN201610111111.9A Pending CN105670828A (en) | 2016-02-29 | 2016-02-29 | Polyvinyl acetate-plant mixed cleaner and preparation method thereof |
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| CN106753909A (en) * | 2016-12-10 | 2017-05-31 | 钦州学院 | A kind of plant cleaning agent and preparation method thereof |
| CN106861774A (en) * | 2017-03-14 | 2017-06-20 | 安徽海德石油化工有限公司 | The method that the selection hydrogenation acetylene removal catalyst of carbon four is prepared using useless palladium-based catalyst |
| CN106947618A (en) * | 2017-03-14 | 2017-07-14 | 安徽海德石油化工有限公司 | Waste Sulfuric Acid pyrolysis recycle device spent sulfuric acid spray gun cleaning agent |
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| CN101165152A (en) * | 2006-10-16 | 2008-04-23 | 吴江市远东清洗剂厂 | Ceramic tile cleaning agent |
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| CN106753909A (en) * | 2016-12-10 | 2017-05-31 | 钦州学院 | A kind of plant cleaning agent and preparation method thereof |
| CN106861774A (en) * | 2017-03-14 | 2017-06-20 | 安徽海德石油化工有限公司 | The method that the selection hydrogenation acetylene removal catalyst of carbon four is prepared using useless palladium-based catalyst |
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