CN107156897B - A kind of device and method preparing tobacco tar - Google Patents
A kind of device and method preparing tobacco tar Download PDFInfo
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- CN107156897B CN107156897B CN201710551397.7A CN201710551397A CN107156897B CN 107156897 B CN107156897 B CN 107156897B CN 201710551397 A CN201710551397 A CN 201710551397A CN 107156897 B CN107156897 B CN 107156897B
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- pyrolysis
- flue gas
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- 241000208125 Nicotiana Species 0.000 title claims abstract description 66
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 66
- 238000000034 method Methods 0.000 title claims description 23
- 238000000197 pyrolysis Methods 0.000 claims abstract description 69
- 238000010438 heat treatment Methods 0.000 claims abstract description 65
- 238000010521 absorption reaction Methods 0.000 claims abstract description 61
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims abstract description 34
- 239000003546 flue gas Substances 0.000 claims abstract description 34
- 239000007788 liquid Substances 0.000 claims abstract description 19
- 239000000779 smoke Substances 0.000 claims description 71
- 230000005540 biological transmission Effects 0.000 claims description 33
- 239000007789 gas Substances 0.000 claims description 22
- 108090000790 Enzymes Proteins 0.000 claims description 17
- 102000004190 Enzymes Human genes 0.000 claims description 17
- 229940088598 enzyme Drugs 0.000 claims description 17
- 239000003517 fume Substances 0.000 claims description 13
- 108010059892 Cellulase Proteins 0.000 claims description 9
- 229940106157 cellulase Drugs 0.000 claims description 9
- 239000000796 flavoring agent Substances 0.000 claims description 5
- 235000019634 flavors Nutrition 0.000 claims description 5
- 238000011282 treatment Methods 0.000 claims description 4
- 108010059820 Polygalacturonase Proteins 0.000 claims 2
- 108010093305 exopolygalacturonase Proteins 0.000 claims 2
- 235000019504 cigarettes Nutrition 0.000 abstract description 30
- 238000004519 manufacturing process Methods 0.000 abstract description 7
- 230000001953 sensory effect Effects 0.000 abstract 1
- 230000009102 absorption Effects 0.000 description 53
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 42
- 241000196324 Embryophyta Species 0.000 description 27
- 238000009434 installation Methods 0.000 description 25
- 239000003205 fragrance Substances 0.000 description 22
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 21
- 235000019441 ethanol Nutrition 0.000 description 17
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 16
- 239000002904 solvent Substances 0.000 description 13
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 12
- 239000003571 electronic cigarette Substances 0.000 description 11
- 239000000126 substance Substances 0.000 description 10
- 238000002360 preparation method Methods 0.000 description 8
- 235000011187 glycerol Nutrition 0.000 description 7
- 239000000463 material Substances 0.000 description 7
- 239000002304 perfume Substances 0.000 description 7
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 6
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 6
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 6
- 230000008569 process Effects 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 4
- 238000005267 amalgamation Methods 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 235000019505 tobacco product Nutrition 0.000 description 4
- MDYZKJNTKZIUSK-UHFFFAOYSA-N tyloxapol Chemical compound O=C.C1CO1.CC(C)(C)CC(C)(C)C1=CC=C(O)C=C1 MDYZKJNTKZIUSK-UHFFFAOYSA-N 0.000 description 4
- 230000002255 enzymatic effect Effects 0.000 description 3
- 230000007071 enzymatic hydrolysis Effects 0.000 description 3
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 description 3
- 125000004836 hexamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000003208 petroleum Substances 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000010923 batch production Methods 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005485 electric heating Methods 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 2
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 2
- LHGVFZTZFXWLCP-UHFFFAOYSA-N guaiacol Chemical compound COC1=CC=CC=C1O LHGVFZTZFXWLCP-UHFFFAOYSA-N 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 150000002429 hydrazines Chemical class 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- RUVINXPYWBROJD-ONEGZZNKSA-N trans-anethole Chemical compound COC1=CC=C(\C=C\C)C=C1 RUVINXPYWBROJD-ONEGZZNKSA-N 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- IEMMBWWQXVXBEU-UHFFFAOYSA-N 2-acetylfuran Chemical compound CC(=O)C1=CC=CO1 IEMMBWWQXVXBEU-UHFFFAOYSA-N 0.000 description 1
- NOEGNKMFWQHSLB-UHFFFAOYSA-N 5-hydroxymethylfurfural Chemical compound OCC1=CC=C(C=O)O1 NOEGNKMFWQHSLB-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 229930013930 alkaloid Natural products 0.000 description 1
- 150000003797 alkaloid derivatives Chemical class 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229940011037 anethole Drugs 0.000 description 1
- 230000002738 anti-smoking effect Effects 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- VIHAEDVKXSOUAT-UHFFFAOYSA-N but-2-en-4-olide Chemical class O=C1OCC=C1 VIHAEDVKXSOUAT-UHFFFAOYSA-N 0.000 description 1
- 239000012159 carrier gas Substances 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010894 electron beam technology Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000005755 formation reaction Methods 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 229960001867 guaiacol Drugs 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- RJGBSYZFOCAGQY-UHFFFAOYSA-N hydroxymethylfurfural Natural products COC1=CC=C(C=O)O1 RJGBSYZFOCAGQY-UHFFFAOYSA-N 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000001819 mass spectrum Methods 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- RUVINXPYWBROJD-UHFFFAOYSA-N para-methoxyphenyl Natural products COC1=CC=C(C=CC)C=C1 RUVINXPYWBROJD-UHFFFAOYSA-N 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- AXFBAIOSECPASO-UHFFFAOYSA-N pentacyclo[6.6.2.02,7.04,16.011,15]hexadeca-1(14),2(7),3,5,8(16),9,11(15),12-octaene Chemical compound C1=C(C=C23)C4=C5C3=CC=CC5=CC=C4C2=C1 AXFBAIOSECPASO-UHFFFAOYSA-N 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000003303 reheating Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 238000004227 thermal cracking Methods 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
本发明提供了一种制备烟油的装置，包括热解装置和捕集装置；热解装置包括：样品加热装置和设置于所述样品加热装置上的样品承载装置；捕集装置包括：入口设置于所述样品承载装置上方的烟气捕集罩；入口与所述烟气捕集罩出口相连的吸收装置；入口与所述吸收装置出口通过管道连接的吸气装置，所述管道上设置流量控制装置。本发明提供的制备烟油的装置创造性的采用开放式的热解装置，在大气有氧的环境下热解，其产物主要具有烟草香、烘焙香、烟熏香，烟熏的感觉较轻微，感官质量更接近传统卷烟，能有效避免无氧环境下其产物烟熏味过重的问题；同时更换烟草样品方便，便于批量生产。本发明装置简单经济，易实现工业化批量生产，有良好的应用前景。
The invention provides a device for preparing e-liquid, including a pyrolysis device and a trapping device; the pyrolysis device includes: a sample heating device and a sample carrying device arranged on the sample heating device; the trapping device includes: an inlet setting a flue gas trapping hood above the sample carrying device; an absorption device whose inlet is connected to the outlet of the flue gas trapping hood; an aspirating device whose inlet is connected to the outlet of the absorption device through a pipeline, and a flow rate is set on the pipeline control device. The device for preparing e-liquid provided by the present invention creatively adopts an open pyrolysis device, which is pyrolyzed in the atmosphere with aerobic environment, and the products mainly have tobacco aroma, baking aroma, and smoky aroma, and the smoky feeling is slight. The sensory quality is closer to traditional cigarettes, which can effectively avoid the problem of excessive smoky taste in the anaerobic environment; at the same time, it is convenient to replace tobacco samples and facilitate mass production. The device of the invention is simple and economical, easy to realize industrialized mass production, and has good application prospects.
Description
Technical field
The present invention relates to technical field of cigarettes, more particularly, to a kind of device and method for preparing tobacco tar.
Background technique
Traditional cigarette generates flue gas by lighting pipe tobacco and meets consumer demand, and when cigarette burning is waved by substance
Hair, pyrolysis and high―temperature nuclei, make have up to more than 7300 compounds in flue gas, wherein by (nearly 900 DEG C of maximum temperature) production of burning
Raw substance has 2740 kinds, these material parts are related with cigarette characteristic scent, but have moieties be harmful to the human body (such as CO,
Benzo [α] pyrene, condensed-nuclei aromatics etc.).
Due to smoke with environment, anti-smoking campaign continue surging and smoker for health demand, low tar,
Less harmful cigarette is more paid attention to, while also flourishing without the new tobacco products of burning.By using electronic cigarette or
Heating does not burn cigarette come to replace traditional cigarette be current Field of Tobacco developing direction.In electronic cigarette and heat the cigarette that do not burn
In, nicotine and most tobacco flavor ingredients can be transferred in flue gas at a lower temperature (usually less than 500 DEG C), because
This will not generate the harmful substance and side-stream smoke that cigarette is generated by high-temp combustion, and cigarette can be greatly reduced to human health
Harm and the pollution to environment.
Electronic cigarette or the heating cigarette etc. that do not burn have smog but incombustible new tobacco products principle is: by heating,
By present in the mist formations such as glycerol, propylene glycol substance, alkaloid, tobacco or additional aroma substance, other flavoring ingredients together
It evaporates to form aerosol, be enjoyed for smoker.Although these products technically have been achieved for rapid progress, mesh
Preceding these products in the market generally have larger gap on taste and aromatic style with traditional cigarette.Its reason is to lack tradition
Cigarette burning and high-temperature retorting pyrolytic process, also just have lost based on fragrance distinctive in flue gas caused by these processes at
Point, it is difficult that smoker is made to obtain the distinctive pleasure of the senses of traditional cigarette, and add traditional tobacco extract and existing flavors and fragrances
Method can not make up this defect.
For this purpose, people are handled tobacco in the way of high temperature pyrolysis, imitate conventional cigarette in combustion into
The complex reactions process such as capable thermal cracking, Mei Lade obtains tobacco response product and is used for new tobacco products, can be in certain journey
It makes up electronic cigarette on degree or the do not burn new tobacco productses such as cigarette insufficient fragrance, smoke feature of heating lacks or unobvious etc. lack
It falls into.
But the research of the related tobacco pyrolysis of the prior art is concentrated mainly on pyrolysis temperature to Product safety and organoleptic attribute
Influence.Existing heating method will lead to tobacco-containing material uneven heating, wherein the portion temperature with heater contacts is higher, far
It is lower from the portion temperature of heater, the phenomenon that Yi Fasheng is charred, influence the mouthfeel of destructive distillation fraction.Meanwhile the prior art is often
Using being pyrolyzed in closed container, offal is easy to blackening in anaerobic high-temperature heating process, is also easy to produce the tobacco tar of black, obtains
Product smoke is overweight.Meanwhile there is arresting efficiency difference in the prior art.
Summary of the invention
In view of this, the present invention provides the technical problem to be solved in the present invention is that providing a kind of preparation facilities of tobacco tar
The tobacco tar concentration that is prepared of device it is big, smoke is moderate while that the content of fragrance is prepared is high.
The present invention provides a kind of devices for preparing tobacco tar, including pyrolysis installation and capturing device；
Pyrolysis installation includes: sample heating device and the sample bearing device that is set on the sample heating device；
Capturing device includes: the smoke collecting cover that entrance is set to above the sample bearing device；Entrance and the cigarette
The connected absorption plant in gas fume trap cover outlet；Entrance exports the getter device connecting by pipeline with the absorption plant, described
Volume control device is set on pipeline.
Preferably, the sample heating device is heater；The sample bearing device is sample disc；The absorption plant
For absorption bottle；The volume control device is flow valve.
Preferably, the entrance of the smoke collecting cover is 0.1~0.5cm at a distance from the sample bearing device；Flue gas
The inlet diameter of fume trap cover is not less than sample bearing device diameter.
Preferably, the entrance of the smoke collecting cover is cone；The angle of centrum end pipeline and centrum axle center
Less than 90 °.
The present invention provides a kind of devices for preparing tobacco tar, including pyrolysis installation and capturing device；
Pyrolysis installation includes: sample heating device, the sample bearing device being set on the sample heating device, is used for
It drives the transmission device of the sample bearing device rotation and is set to filling above the transmission device for carrying to sample
Set the feeding device of charging；
Capturing device includes: the smoke collecting cover that entrance is set to above the sample bearing device；Entrance and the cigarette
The connected absorption plant in gas fume trap cover outlet；Entrance exports the getter device connecting by pipeline with the absorption plant, described
Volume control device is set on pipeline.
Preferably, the transmission device includes transmission belt and driving wheel；The feeding device is hopper.
The present invention provides a kind of methods for preparing tobacco tar, comprising:
Tobacco sample is placed on sample bearing device, is pyrolyzed through sample heating device, the flue gas after being pyrolyzed；
Getter device is opened, volume control device adjusting gas flow is passed through；Flue gas after pyrolysis is caught through smoke collecting cover
Collection, absorption plant absorb, and obtain smoke fragrance.
Preferably, the temperature of the pyrolysis is 200~450 DEG C；The time of the pyrolysis is 0.5~30min.
Preferably, the tobacco sample is placed in front of sample bearing device by pretreatment, and the pretreatment is at using enzyme
Tobacco sample is managed, the enzyme is selected from one or more of cellulase and pectase.
The present invention provides a kind of methods for preparing tobacco tar, comprising:
Sample is added under the drive of transmission device, through feeding device in tobacco sample bogey, then heats and fill through sample
Set pyrolysis, the flue gas after being pyrolyzed；
Getter device is opened, volume control device adjusting gas flow is passed through；Flue gas after pyrolysis is caught through smoke collecting cover
Collection, absorption plant absorb, and obtain smoke fragrance.
Compared with prior art, the present invention provides a kind of devices for preparing tobacco tar, including pyrolysis installation and capturing device；
Pyrolysis installation includes: sample heating device and the sample bearing device that is set on the sample heating device；Capturing device packet
Include: entrance is set to the smoke collecting cover above the sample bearing device；Entrance is connected with smoke collecting cover outlet
Absorption plant；Entrance exports the getter device connecting by pipeline with the absorption plant, and flow control is arranged on the pipeline
Device.The device provided by the invention for preparing tobacco tar it is creative using open pyrolysis installation, in the environment that atmosphere is aerobic
Lower pyrolysis, product mainly have fragrant tobacco, baking perfume, sootiness fragrant, and the feeling of sootiness is slighter, the closer tradition of aesthetic quality
Cigarette can effectively avoid the problem that its product smoke is overweight under oxygen-free environment；It is convenient that tobacco sample is replaced simultaneously, convenient for batch
Production.Apparatus of the present invention simple economy, Yi Shixian industrialized mass production have good application prospect.
Detailed description of the invention
Fig. 1 is the device that tobacco tar is prepared described in the one of embodiment of the present invention；
Fig. 2 is the device that tobacco tar is prepared described in another embodiment of the present invention.
Specific embodiment
The present invention provides a kind of devices for preparing tobacco tar, including pyrolysis installation and capturing device；
Pyrolysis installation includes: sample heating device and the sample bearing device that is set on the sample heating device；
Capturing device includes: the smoke collecting cover that entrance is set to above the sample bearing device；Entrance and the cigarette
The connected absorption plant in gas fume trap cover outlet；Entrance exports the getter device connecting by pipeline with the absorption plant, described
Volume control device is set on pipeline.
The device of preparation smoke fragrance provided by the invention includes pyrolysis installation.
Pyrolysis installation includes sample heating device and the sample bearing device that is set on the sample heating device.
Pyrolysis installation provided by the invention is used to tobacco sample heat resolve generating flue gas.
According to the present invention, the pyrolysis installation includes sample heating device.The present invention for the heating device without
It limits, the heating device well known to those skilled in the art that sample can be heated.The sample heating device is preferably
Heater.The present invention is for heating method without restriction, including but not limited to electric heating, microwave heating, infrared heating, electricity
Beamlet heating etc..
The pyrolysis installation includes sample bearing device.The present invention for the sample bearing device without limit, can
To carry sample.Preferably sample disc.The present invention for the sample disc diameter without limit, can be according to need
It is adjusted, the diameter of the sample disc is less than the inlet diameter of smoke collecting cover.
Capturing device provided by the invention includes: the smoke collecting cover that entrance is set to above the sample bearing device；
Entrance exports the absorption plant being connected with the smoke collecting cover；Entrance exports the suction connecting by pipeline with the absorption plant
Volume control device is arranged on the pipeline in device of air.
In the present invention, capturing device includes smoke collecting cover.Fume trap cover of the present invention includes that the flue gas of cone is caught
Collect cover entrance and fume trap cover pipeline, smoke collecting cover is connected by pipeline with solvent bogey.
Centrum end of the present invention pipeline and the angle in centrum axle center are preferably smaller than 90 °.Above-mentioned angle can prevent cold
Product reflux is coagulated to sample disc.
According to the present invention, the entrance of the smoke collecting cover is set to above the sample bearing device.
The entrance of smoke collecting cover of the present invention is preferably 0.1~0.5cm at a distance from the sample bearing device；More
Preferably 0.1~0.4cm.The inlet diameter of smoke collecting cover of the present invention is not less than sample bearing device diameter.Preferably, described
The inlet diameter of smoke collecting cover and the sample bearing device diameter ratio are 1.2~1:1.
Capturing device provided by the invention includes: the absorption plant that entrance is connected with smoke collecting cover outlet.
The present invention for the absorption plant without limiting, preferably absorption bottle, preferred dress in advance in the absorption bottle
Enter lyosoption；The solvent be preferably water, ethyl alcohol, ether, acetone, petroleum ether, solvent naphtha, n-hexane, hexamethylene, pentane,
One or more of methylene chloride and ethyl acetate.
Absorption bottle of the present invention is preferably disposed in cold-trap, and the temperature in the cold-trap is preferably -15~-20 DEG C.
Capturing device provided by the invention includes: that entrance is filled with absorption plant outlet by the air-breathing that pipeline is connect
It sets.
The present invention for the getter device without limit, it is well known to those skilled in the art.It can be to gas
Generate the flow direction of gas especially air in device for controlling sucking force.
The present invention for the getter device and absorption plant connecting pipe without limiting, those skilled in the art are ripe
Know.Volume control device is set on pipeline.The present invention is for the volume control device without restriction, this field skill
Known to art personnel.
By air velocity in volume control device control device, and then control the flow velocity for the flue gas that air carries.
The present invention provides a kind of devices for preparing tobacco tar, including pyrolysis installation and capturing device；Pyrolysis installation includes: sample
Product heating device and the sample bearing device being set on the sample heating device；Capturing device includes: that entrance is set to institute
State the smoke collecting cover above sample bearing device；Entrance exports the absorption plant being connected with the smoke collecting cover；Entrance with
The absorption plant exports the getter device connected by pipeline, and volume control device is arranged on the pipeline.The present invention provides
The device for preparing tobacco tar it is creative using open pyrolysis installation, be pyrolyzed under the aerobic environment of atmosphere, product master
Have fragrant tobacco, baking perfume, sootiness fragrant, the feeling of sootiness is slighter, and aesthetic quality can effectively avoid closer to traditional cigarette
The overweight problem of its product smoke under oxygen-free environment；It is convenient that tobacco sample is replaced simultaneously, convenient for batch production.Apparatus of the present invention
Simple economy, Yi Shixian industrialized mass production have good application prospect.
The present invention provides a kind of devices for preparing tobacco tar, including pyrolysis installation and capturing device；
Pyrolysis installation includes: sample heating device, the sample bearing device being set on the sample heating device, is used for
It drives the transmission device of the sample bearing device rotation and is set to filling above the transmission device for carrying to sample
Set the feeding device of charging；
Capturing device includes: the smoke collecting cover that entrance is set to above the sample bearing device；Entrance and the cigarette
The connected absorption plant in gas fume trap cover outlet；Entrance exports the getter device connecting by pipeline with the absorption plant, described
Volume control device is set on pipeline.
The device of preparation smoke fragrance of the invention, including pyrolysis installation and capturing device.
Wherein, pyrolysis installation includes sample heating device.The present invention is for the heating device without restriction, this field
The heating device that can be heated sample known to technical staff.The sample heating device is preferably heater.This hair
It is bright for heating method without limit, including but not limited to electric heating, microwave heating, infrared heating, electron beam heating etc..
The pyrolysis installation includes sample bearing device.The present invention for the sample bearing device without limit, can
To carry sample.Preferably sample disc.The present invention for the sample disc diameter without limit, can be according to need
It is adjusted, the diameter of the sample disc is less than the inlet diameter of smoke collecting cover.
In the present invention, the pyrolysis installation includes the transmission device for driving the sample bearing device rotation.
The present invention without limiting, can drive the sample bearing device to rotate the transmission device.
Preferably include transmission belt and driving wheel.The present invention for the transmission belt and driving wheel concrete specification without limit, with sample
The matching of product bogey.The quantity of the transmission belt is preferably one；The driving wheel is preferably two.Sample carrying dress
The drive set in transmission belt is moved to the heating of sample heating zone, and mobile overturning empties downwards sample carrying and fills after pyrolysis
It sets.
Pyrolysis installation of the present invention includes being set to above the transmission device to be used to feed to sample bearing device
Feeding device；The present invention is for the feeding device without restriction, preferably hopper.
Sample bearing device completes charging in the case where the drive of transmission belt is moved to hopper.To complete auto feed.Together
When combine above-mentioned timing empty, avoid pyrolysis excessively generate be charred taste.
Capturing device of the present invention is above-mentioned to be clearly described, and details are not described herein.
The device that tobacco tar is prepared described in the one of embodiment of the present invention is as depicted in figs. 1 and 2, Fig. 1 be the present invention its
The device of tobacco tar is prepared described in middle one embodiment, wherein 1 is sample heating device, and 2 be sample bearing device；3 be flue gas
Fume trap cover；4 be absorption plant, and 5 be volume control device, and 6 be getter device.
Fig. 2 is the device of preparation smoke fragrance described in another embodiment of the present invention, wherein 1 is sample heating device,
2 be sample bearing device；3 be smoke collecting cover；4 be absorption plant, and 5 be volume control device, and 6 be getter device；7 be charging
Device；8 be transmission belt, and 9 be driving wheel.
The present invention provides a kind of methods for preparing tobacco tar, comprising:
Tobacco sample is placed on sample bearing device, is pyrolyzed through sample heating device, the flue gas after being pyrolyzed；
Getter device is opened, volume control device adjusting gas flow is passed through；Flue gas after pyrolysis is caught through smoke collecting cover
Collection, absorption plant absorb, and be absorbed liquid, and absorbing liquid is concentrated to obtain smoke fragrance.
Tobacco sample is placed on sample bearing device by the method for preparation cigarette taste substance provided by the invention first, through sample
Heating device pyrolysis, the flue gas after being pyrolyzed.
The present invention, without restriction, can carry out the tobacco sample of pyrolysis preparation smoke fragrance for the tobacco sample,
To its shape without limiting, tobacco leaf, pipe tobacco and offal；Preferably offal.
In the present invention, the tobacco sample is placed in front of sample bearing device preferably through pretreatment, and the pretreatment is excellent
It is selected as using enzymatic treatment tobacco sample, the enzyme is selected from one or more of cellulase and pectase.The enzymatic treatment
Mode specifically:
By offal moisture regulation to 15%-20%, complex enzyme is then added, contains cellulase and pectin in complex enzyme
The mass ratio of enzyme, cellulase and pectase is 1:1~10；Preferably, the mass ratio of cellulase and pectase is 1:1~5,
Wherein, the enzyme activity of used cellulase is 150,000 U/g, and the enzyme activity of used pectase is 30,000 U/g；Complex enzyme
Additive amount is the 0.01%~1.0% of offal quality, preferably 0.05%~1.0%；Hydrolysis temperature is 30~60 DEG C, preferably
40~50 DEG C；Enzymolysis time 4~24 hours, preferably 6~10 hours.
It is preferred that specifically: by offal moisture regulation to 18%, 0.005g complex enzyme (cellulose is then added with every gram of offal
The mass ratio of enzyme and pectase is 1:2), it is digested 8 hours under the conditions of 45 DEG C after mixing, for being pyrolyzed after enzymatic hydrolysis.With not
It is directly pyrolyzed products therefrom using enzymatic hydrolysis to compare, reheating solution products therefrom has denseer baking fragrant after digesting, and mouthfeel is more
Comfortably.
After enzymatic treatment, moisture content is preferably adjusted.Enzyme both degradable cell wall substance makes fragrance matter be easier to discharge,
It also can produce fragrance matter after catabolite pyrolysis；Adjusting moisture can make its moisture content be maintained at certain value, in heating process
Middle moisture takes fragrance matter out of while evaporation, while guaranteeing that tobacco-containing material can reach the temperature of needs at the same time
Degree.
Pretreatment of the present invention can also adjust moisture and contain to mix in offal material with Maillard reaction raw material
Amount.Maillard reaction raw material can be sugar and/or amino acid, be heated using the later period, make between admixture or admixture and cigarette
Maillard reaction occurs between last chemical component, generates fragrance matter.
Pretreatment of the present invention can also adjust moisture content to mix in offal material with Alevaire.Alevaire is
Propylene glycol or glycerol, Alevaire infiltrate tobacco material, can reduce tobacco material coking bring burning in pyrolytic process, simultaneously
Its fibr tissue can be made to be swollen, be conducive to aroma component volatilization, and Alevaire can dissolve aroma component, in pyrolysis installation
When middle atomization, aroma component can be also carried out.
The temperature of pyrolysis of the present invention is preferably 200 DEG C~450 DEG C；More preferably 250 DEG C~350 DEG C；The pyrolysis
Time be preferably 0.5~30min；More preferably 1~5min.
Getter device is opened, volume control device adjusting gas flow is passed through.Gas flow is air mass flow herein.Pass through
Air mass flow is controlled, to control the flow velocity of the flue gas of air carrying, the present invention is for the gas flow without restriction, root
Depending on single unit system size, preferably flue gas can condense well.
Flue gas after pyrolysis is absorbed through smoke collecting cover trapping, absorption plant, and be absorbed liquid.
Wherein, solvent of the present invention is preferably water, ethyl alcohol, ether, acetone, petroleum ether, solvent naphtha, n-hexane, hexamethylene
One of alkane, pentane, methylene chloride and ethyl acetate are a variety of；More preferably ethyl alcohol, ether, acetone, petroleum ether, solvent
One of oil, n-hexane and hexamethylene are a variety of；Most preferably ethyl alcohol.
The absorption plant is preferably disposed in cold-trap, and the temperature of the cold-trap is preferably -15~-20 DEG C.
The concentration of the ethanol solution is preferably 90%~95%.The gas flow is preferably 100~120mL/min.
It is absorbed after liquid, absorbing liquid is concentrated to obtain smoke fragrance.
The present invention for the concentration concrete mode without limit, it is well known to those skilled in the art.It is preferred that
To be concentrated under reduced pressure.
The present invention is pyrolyzed tobacco sample in atmospheric environment (aerobic), and product mainly has tobacco perfume, bakes
Fragrant, sootiness perfume, but the feeling of sootiness is slighter, and aesthetic quality can effectively avoid its under oxygen-free environment from producing closer to traditional cigarette
The overweight problem of object smoke；Each a small amount of offal, can make offal sample reach the temperature of needs in a very short period of time,
Pyrolytic process is closer with traditional cigarette, and product organoleptic quality is closer to traditional cigarette；Each sample is only stopped in heating zone
It several minutes, that is, is avoided that the taste that is charred of product, and production efficiency can be improved；It is open to be easily changed sample, it is more suitable for industrializing
Production.Product qualities can be improved in offal pretreatment of the present invention.Thermal decomposition product purification, pyrolysis residue are extracted and product assembles
Etc. subsequent processings can make full use of offal raw material, also can be further improved product qualities.
The present invention provides a kind of methods for preparing tobacco tar, comprising:
Sample is added under the drive of transmission device, through feeding device in tobacco sample bogey, then heats and fill through sample
Set pyrolysis, the flue gas after being pyrolyzed；
Getter device is opened, volume control device adjusting gas flow is passed through；Flue gas after pyrolysis is caught through smoke collecting cover
Collection, absorption plant absorb, and be absorbed liquid, and absorbing liquid is concentrated to obtain smoke fragrance.
In the present invention, tobacco sample bogey is under the drive of transmission device, and sample is added in feeding device, then through sample
The pyrolysis of product heating device, the flue gas after being pyrolyzed.
The present invention for the transmission device speed without limit.
More preferably specific: sample disc steps to sample after hopper feeds under the drive of transmission belt according to set time
The flat-temperature zone of product heater stops the regular hour；Sample the flat-temperature zone of heater by pyrolysis after, with the band of transmission belt
Dynamic, downwards, sample disc is emptied for overturning；Sample disc after emptying is loaded when turning to below hopper, to recycle
Automatically tobacco tar is prepared.
The present invention is above-mentioned for remaining step of the method for the preparation smoke fragrance to be clearly described, herein not
It repeats again.
The present invention preferably passes through GC-MS and analyzes the fragrance component for the smoke fragrance being prepared, and analysis condition is such as
Under:
Sample pre-treatments: a certain amount of anethole is added in trapping solution as internal standard, concentration is excessively to be analyzed after film.
Gas chromatography-mass spectrography parameter:
Gas-chromatography: analytical column is HP-5MS (30m × 0.25mm × 0.25um)；Carrier gas is helium, purity >=
99.999%；Constant current mode, flow velocity 1.0mL/min；Injector temperature is 250 DEG C；Split ratio is 10:1；Column temperature takes program
Heating mode: 50 DEG C of initial temperature, 2min is kept, is then warming up to 250 DEG C with 5 DEG C/min, is kept, 30min.
Mass spectrum: 250 DEG C of transmission line temperature；Ionization mode: electron bombardment ionization source (EI+)；Monitoring mode: full scan mode is fixed
Property, scanning range: 33-550amu；Ionizing energy: 70eV；200 DEG C of ion source temperature；Quadrupole rod temperature are as follows: 150 DEG C；Solvent prolongs
It is slow: 6.5min.
The present invention, please be special by being used for electronic cigarette after taking absorbing liquid to mix with propylene glycol, glycerine by 1:1:1 (volume ratio)
Family smokes panel test.
In order to further illustrate the present invention, with reference to embodiments to it is provided by the invention preparation smoke fragrance device and
Method is described in detail.
Embodiment 1
Device is connected according to of the present invention, specifically: sample disc is placed on adjustable thermostatic heater, flue gas trapping
Cone of the cover for back-off, entrance face sample disc, Edge Distance sample disc mouth edge 0.3cm, cone end and centrum
The angle in axle center is 75 °, and smoke collecting cover inlet diameter is identical as sample disk diameter.Getter device is opened, flow is adjusted, is absorbed
It is placed with solvent in bottle, absorption bottle is placed in -15 DEG C of cold hydrazines, and the entrance of absorption bottle is connected with smoke collecting cover outlet.Absorption bottle
Outlet be connected with getter device by pipeline, flow valve is provided on pipeline.
Embodiment 2
Device is connected according to of the present invention, specifically: sample disc is placed on transmission belt, by belt pulley with its turn
Dynamic, adjustable thermostatic heater is placed in above transmission belt for heating sample disc, hopper.Smoke collecting cover is the cone of back-off,
The angle in entrance face sample disc, Edge Distance sample disc mouth edge 0.3cm, cone end and centrum axle center is 75 °, cigarette
Gas fume trap cover inlet diameter is identical as sample disk diameter.Getter device is opened, flow is adjusted, is placed with solvent in absorption bottle, absorb
Bottle is placed in -15 DEG C of cold hydrazines, and the entrance of absorption bottle is connected with smoke collecting cover outlet.The outlet of absorption bottle is by pipeline and inhales
Device of air is connected, and flow valve is provided on pipeline.
Embodiment 3
Device is connected according to the embodiment of the present invention 1,3 identical absorption bottles (4) of connecting, each absorption bottle is provided with
20mL95% ethanol solution, absorption bottle are placed in -15 DEG C of cold-traps.It opens getter device (6), adjusts flow valve, make gas flow
Amount is 100mL/min.It opens sample heating device (1), temperature is set as 300 DEG C, 1 gram of offal is taken to be laid in sample disc, it will
Sample disc is placed in heating zone, is pyrolyzed 5min, changes next sample after 5min, so 10 samples of circulation pyrolysis.After pyrolysis
Merge the solvent of 3 absorption bottles, and wash out the smoke condensate in smoke collecting cover with 10mL95% ethanol solution, with 95% second
Amalgamation liquid volume is supplied 80mL by alcohol, for electricity after taking 20mL liquid to mix with propylene glycol, glycerine by 1:1:1 (volume ratio)
Sub- cigarette, asks expert to smoke panel test.
Embodiment 4
Device is connected according to the embodiment of the present invention 2,3 identical absorption bottles (4) of connecting, each absorption bottle is provided with
20mL95% ethanol solution, absorption bottle are placed in -15 DEG C of cold-traps.It opens getter device (6), adjusts flow valve, make gas flow
Amount is 100mL/min.It is rotated in each sample disc by transmission belt, by hopper 1 gram of offal sample of charging, opens sample heating
Temperature is set as 300 DEG C by device (1), after sample heating device temperature reaches setting value, is taken sample disc to warm area and is carried out heat
Solution, automatic transmission changes next sample after being pyrolyzed 5min, and 10 samples of such continuous pyrolysis merge 3 absorptions after pyrolysis
The solvent of bottle, and with the smoke condensate in 10mL95% ethanol solution wash-off smoke collecting cover, with 95% ethyl alcohol by amalgamation liquid
Volume supplies 80mL, and electronic cigarette is used for after taking 20mL liquid to mix with propylene glycol, glycerine by 1:1:1 (volume ratio), please be special
Family smokes panel test.
Comparative example 1
The present embodiment is substantially the same manner as Example 3, the difference is that pyrolysis section is using common in the art close
Container pyrolysis is closed, and uses nitrogen protection, specifically: 3 identical absorption bottles (4) of connecting, each absorption bottle is provided with
20mL95% ethanol solution, absorption bottle are placed in -15 DEG C of cold-traps.It opens getter device (6), adjusts flow valve, make gas flow
Amount is 100mL/min.It opens sample heating device (1), temperature is set as 300 DEG C, under nitrogen protection by 10 grams of offal samples
It is pyrolyzed 50min, the solvent of 3 absorption bottles is merged after pyrolysis, and washed out in smoke collecting cover with 10mL95% ethanol solution
Smoke condensate, amalgamation liquid volume is supplied into 80mL with 95% ethyl alcohol, takes 20mL liquid and propylene glycol, glycerine by 1:1:
It is used for electronic cigarette after 1 (volume ratio) mixing, expert is asked to smoke panel test.
Embodiment 5
Device is connected according to the embodiment of the present invention 1,3 identical absorption bottles (4) of connecting, each absorption bottle is provided with
20mL95% ethanol solution, absorption bottle are placed in -15 DEG C of cold-traps.It opens getter device (6), adjusts flow valve, make gas flow
Amount is 100mL/min.It opens sample heating device (1), temperature is set as 300 DEG C, 1 gram of offal through enzymolysis processing is taken to be laid in
In sample disc, the enzymolysis processing specifically: then compound with every gram of offal addition 0.005g by offal moisture regulation to 18%
Enzyme (mass ratio of cellulase and pectase is 1:2), digests 8 hours under the conditions of 45 DEG C after mixing, is used for after enzymatic hydrolysis
Pyrolysis.Sample disc is placed in heating zone, 5min is pyrolyzed, changes next sample after 5min, so 10 samples of circulation pyrolysis.Pyrolysis
After merge 3 absorption bottles solvent, and with 10mL95% ethanol solution wash out smoke collecting cover in smoke condensate, use
Amalgamation liquid volume is supplied 80mL by 95% ethyl alcohol, after taking 20mL liquid to mix with propylene glycol, glycerine by 1:1:1 (volume ratio)
For electronic cigarette, expert is asked to smoke panel test.
Embodiment 6
Expert's smoking result: embodiment 3,4 products therefrom of embodiment are in electronic cigarette in application, it mainly has tobacco
Sootiness perfume fragrant, baking is fragrant and weaker, mouthfeel are relatively comfortable；Compared with 1 products therefrom of comparative example is applied in electronic cigarette, solving
Certainly smoke, be charred taste it is overweight while, the baking that can obviously increase tobacco is fragrant, and mouthfeel is finer and smoother；Embodiment 5 and embodiment 3
It compares, 5 products therefrom of embodiment is in application, fragrant with denseer baking in electronic cigarette, and mouthfeel is more comfortable, and aesthetic quality is bright
It is aobvious to be better than embodiment 3.
GC/MS analyze flavor component the result shows that, main baking perfume (or spice) substance (such as furfural, 5- methyl chaff of embodiment 5
Aldehyde, 5 hydroxymethyl furfural) content is 1.2 times or more of embodiment 3.Embodiment 3 is compared with comparative example 1,3 products therefrom of embodiment
Containing richer fragrance matter, fragrant class (such as 2- acetyl furan, 2 (5H)-furanones) content is baked for comparative example 1
1.2 times or more, and smoke substance (such as guaiacol) content is 0.8 times of comparative example 1 hereinafter, therefore, embodiment 3 can increase
Perfume is baked, reduction is charred taste and smoke, and mouthfeel is more comfortable, and aesthetic quality is substantially better than comparative example 1.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered
It is considered as protection scope of the present invention.
Claims (7)
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104535396A (en) * | 2015-01-21 | 2015-04-22 | 中国烟草总公司郑州烟草研究院 | Method for generating and gathering smoke by externally heating and sucking cigarette and special device for method |
| CN204422287U (en) * | 2015-03-18 | 2015-06-24 | 安徽中烟工业有限责任公司 | A kind of tobacco curing barn flavor component capturing device |
| CN204556433U (en) * | 2015-05-14 | 2015-08-12 | 安徽中烟工业有限责任公司 | A kind of device for real-time analysis tobacco pyrolysis smoke release characteristics |
| CN104931301A (en) * | 2015-06-25 | 2015-09-23 | 华南理工大学 | Incense smoke collection device and method for detecting volatile ingredients of incense smoke |
| CN205749041U (en) * | 2016-05-20 | 2016-11-30 | 云南中烟工业有限责任公司 | A kind of flue gas release capturing device based on Nicotiana tabacum L. heating non-burning smoke generator Imitating heater |
| CN206240233U (en) * | 2016-11-10 | 2017-06-13 | 江苏华威机械制造有限公司 | Flue dust unhurried current particulate autoprecipitation collection device |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201400668Y (en) * | 2009-05-04 | 2010-02-10 | 中国科学院植物研究所 | A plant volatile oil extraction device |
| CN202478622U (en) * | 2012-01-11 | 2012-10-10 | 攀钢集团攀枝花钢铁研究院有限公司 | Vacuum reduced pressure distillation separating device |
| US9629391B2 (en) * | 2013-08-08 | 2017-04-25 | R.J. Reynolds Tobacco Company | Tobacco-derived pyrolysis oil |
| CN203525354U (en) * | 2013-10-28 | 2014-04-09 | 四川剑南春（集团）有限责任公司 | Rectifier for laboratory |
| CN105212262A (en) * | 2015-11-13 | 2016-01-06 | 中国烟草总公司郑州烟草研究院 | A kind of preparation method of tobacco flavor material |
| CN105935151B (en) * | 2016-04-20 | 2017-09-19 | 江苏中烟工业有限责任公司 | Treatment method suitable for shredded tobacco of low-temperature non-burning cigarettes |
| CN205931336U (en) * | 2016-08-29 | 2017-02-08 | 广州姿采化妆品厂 | Automatic filling device |
| CN106391901A (en) * | 2016-09-19 | 2017-02-15 | 宜兴华威封头有限公司 | Automatic feeding and discharging device of punch machine |
| CN206275050U (en) * | 2016-11-10 | 2017-06-27 | 马倩影 | A kind of millet cake processing injection mold device |
-
2017
- 2017-07-07 CN CN201710551397.7A patent/CN107156897B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104535396A (en) * | 2015-01-21 | 2015-04-22 | 中国烟草总公司郑州烟草研究院 | Method for generating and gathering smoke by externally heating and sucking cigarette and special device for method |
| CN204422287U (en) * | 2015-03-18 | 2015-06-24 | 安徽中烟工业有限责任公司 | A kind of tobacco curing barn flavor component capturing device |
| CN204556433U (en) * | 2015-05-14 | 2015-08-12 | 安徽中烟工业有限责任公司 | A kind of device for real-time analysis tobacco pyrolysis smoke release characteristics |
| CN104931301A (en) * | 2015-06-25 | 2015-09-23 | 华南理工大学 | Incense smoke collection device and method for detecting volatile ingredients of incense smoke |
| CN205749041U (en) * | 2016-05-20 | 2016-11-30 | 云南中烟工业有限责任公司 | A kind of flue gas release capturing device based on Nicotiana tabacum L. heating non-burning smoke generator Imitating heater |
| CN206240233U (en) * | 2016-11-10 | 2017-06-13 | 江苏华威机械制造有限公司 | Flue dust unhurried current particulate autoprecipitation collection device |
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