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CN108821868B - Pesticide-fertilizer mixture - Google Patents

Pesticide-fertilizer mixture Download PDF

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Publication number
CN108821868B
CN108821868B CN201810827429.6A CN201810827429A CN108821868B CN 108821868 B CN108821868 B CN 108821868B CN 201810827429 A CN201810827429 A CN 201810827429A CN 108821868 B CN108821868 B CN 108821868B
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parts
fertilizer
pesticide
urea
powder
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CN108821868A (en
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白宝祥
杨秀莲
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Heilongjiang Baoxiang Agricultural Technology Development Co ltd
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Heilongjiang Baoxiang Agricultural Technology Development Co ltd
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/10Solid or semi-solid fertilisers, e.g. powders
    • C05G5/12Granules or flakes
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Soil Sciences (AREA)
  • Fertilizers (AREA)

Abstract

The invention provides a pesticide-fertilizer mixture which comprises the following raw materials in parts by weight: 20-300 parts of nitrogen and phosphorus fertilizer, 1-50 parts of potassium fertilizer, 0.1-15 parts of zinc sulfate, 1-60 parts of animal and vegetable fatty acid, 1-50 parts of sulfuric acid, 6-15 parts of zeolite powder, 8-15 parts of steel slag powder, 10-15 parts of furfural slag, 0.1-10 parts of bactericide and 0.02-0.18 part of regulator. The pesticide-fertilizer mixture provided by the invention can combine two operation steps of field fertilization and pesticide spraying into one, saves labor force, reduces time and energy consumption, has obvious fertilizer efficiency, and can obviously improve crop yield.

Description

Pesticide-fertilizer mixture
Technical Field
The invention belongs to the technical field of agriculture, and particularly relates to a pesticide-fertilizer mixture.
Background
The pesticide is mainly used for controlling pests in crops, the fertilizer provides necessary nutrition for the growth of the crops and is also required by the crops, and when the pesticide and the fertilizer are required by the crops at the same time, the fertilizer provides a strong place for the development of pesticide fertilizers. The pesticide fertilizer is a mixture integrating the functions of pesticide and fertilizer, and the fertilizer and the pesticide are stabilized in a specific compound system through a certain process technology, so that a novel pesticide fertilizer preparation is formed. For the sustainable development of contemporary agriculture, medical manures are a new attempt to support and drive modern agriculture with powerful technology. The pesticide fertilizer can combine two operation steps in the field, which not only saves labor force, but also reduces time and energy consumption. The fertilizer can provide necessary nutrients for crops, promote the growth and development of plant roots, strengthen plants and blade thickness, prevent and treat plant diseases and insect pests, dwarfs plants, resists lodging, increases yield and income.
Disclosure of Invention
The invention aims to provide a pesticide-fertilizer mixture which can combine two operation steps of fertilizing and pesticide spraying in the field, save labor force, reduce time and energy consumption and has good yield increasing effect.
In order to solve the problems, the invention provides a pesticide-fertilizer mixture which comprises the following raw materials in parts by weight:
20-300 parts of nitrogen and phosphorus fertilizer, 1-50 parts of potassium fertilizer, 0.1-15 parts of zinc sulfate, 1-60 parts of animal and vegetable fatty acid, 1-50 parts of sulfuric acid, 1-60 parts of zeolite powder, 1-60 parts of steel slag powder, 1-60 parts of furfural slag, 0.1-10 parts of bactericide and 0.02-0.18 part of regulator.
It should be noted that the pesticide-fertilizer mixture includes, but is not limited to, the above components, and those skilled in the art may also add other substances to the pesticide-fertilizer mixture according to the actual situation.
Preferably, the nitrogen and phosphorus fertilizer is one or more of urea, diammonium phosphate, monoammonium phosphate and ammonium sulfate.
Preferably, the potassium fertilizer is potassium sulfate.
Preferably, the bactericide is one or more of thiram, metalaxyl, tebuconazole, trifloxystrobin and hymexazol.
Preferably, the modulator is one or more of uniconazole, paclobutrazol, naphthylacetic acid, mepiquat chloride. The regulator has the function of regulating the growth of plants.
Preferably, the steel slag powder is 60 meshes and is applied by 100kg per mu. The weight ratio of the steel slag powder to the zeolite powder is 3: 2.
further preferably, the pesticide-fertilizer mixture comprises the following raw materials in parts by weight:
5-16 parts of urea, 1-12 parts of diammonium phosphate, 10-15 parts of monoammonium phosphate, 30-60 parts of ammonium sulfate, 3-7 parts of potassium sulfate, 0.9-2 parts of zinc sulfate, 5-10 parts of animal and plant fatty acid, 4-8 parts of sulfuric acid, 6-15 parts of zeolite powder, 8-15 parts of steel slag powder, 10-15 parts of furfural slag, 0.5-0.8 part of thiram, 0.2-0.5 part of metalaxyl, 0.1-0.7 part of tebuconazole, 0.26-0.5 part of trifloxystrobin, 0.11-0.65 part of hymexazol, 0.01-0.05 part of paclobutrazol, 0.03-0.06 part of uniconazole, 0.012-0.05 part of naphthylacetic acid and 0.015-0.03 part of mepiquat.
Further preferably, the pesticide-fertilizer composition comprises the following raw materials in parts by weight:
8 parts of urea, 4 parts of diammonium phosphate, 12 parts of monoammonium phosphate, 45 parts of ammonium sulfate, 5 parts of potassium sulfate, 1 part of zinc sulfate, 7 parts of animal and plant fatty acid, 6 parts of sulfuric acid, 10 parts of zeolite powder, 15 parts of steel slag powder, 12 parts of furfural slag, 0.6 part of thiram, 0.3 part of metalaxyl, 0.4 part of tebuconazole, 0.2 part of trifloxystrobin, 0.5 part of hymexazol, 0.03 part of paclobutrazol, 0.05 part of uniconazole, 0.026 part of naphthylacetic acid and 0.02 part of mepiquat.
The preparation method of the pesticide-fertilizer mixture comprises the following steps:
the fertilizer is prepared by uniformly mixing nitrogen phosphorus fertilizer, potash fertilizer, zinc sulfate, animal and vegetable fatty acid, sulfuric acid, zeolite powder, steel slag powder, furfural slag, bactericide and regulator according to the selected weight parts.
Preferably, the preparation method of the pesticide-fertilizer mixture comprises the following steps:
step one, mixing and stirring the furfural residues, zeolite powder, steel residue powder, animal and plant fatty acid and sulfuric acid uniformly, and crushing to 40-80 meshes to obtain a mixture;
step two, taking urea and diammonium phosphate as the nitrogen and phosphorus fertilizer, and respectively crushing the urea and the diammonium phosphate to 40-80 meshes;
thirdly, taking monoammonium phosphate and ammonium sulfate as the nitrogen and phosphorus fertilizer, taking potassium sulfate as a potassium fertilizer, taking thiram, metalaxyl, tebuconazole, trifloxystrobin and hymexazol as the bactericides, taking uniconazole, paclobutrazol, naphthylacetic acid and mepiquat chloride as regulators, sequentially feeding the materials according to the sequence of the monoammonium phosphate, the ammonium sulfate, the potassium sulfate, zinc sulfate, the thiram, the metalaxyl, the tebuconazole, the trifloxystrobin, the hymexazol, the paclobutrazol, the naphthylacetic acid, the mepiquat and the uniconazole, mixing for more than 30min, adding the urea and the diammonium phosphate obtained in the second step, continuously mixing for more than 15min, finally adding the mixture obtained in the first step, and continuously mixing for more than 30min to obtain a medicine-fertilizer mixture;
step four, bagging, weighing and sealing the pesticide-fertilizer mixture obtained in the step three; or granulating, bagging, weighing and sealing the pesticide-fertilizer mixture obtained in the third step.
Compared with the prior art, the technical scheme of the invention has the following beneficial effects:
(1) the pesticide-fertilizer mixture comprises nitrogen and phosphorus fertilizer, potash fertilizer, zinc sulfate, animal and vegetable fatty acid, sulfuric acid, zeolite powder, steel slag powder, furfural slag and bactericide. The pesticide-fertilizer mixture provided by the invention can combine two operation steps of field fertilization and pesticide spraying into one, thereby saving labor force and reducing time and energy consumption.
(2) The pesticide-fertilizer mixture comprises zeolite powder, wherein the zeolite powder is a pure natural environment-friendly mineral product, can be used as a pesticide carrier and a pesticide particle slow-release agent for production, and can also be used as a fertilizer carrier and a soil conditioner, and has the effects of improving the nitrogen content of soil, reducing the viscosity of the soil and improving the water permeability.
The natural zeolite powder is rich in organic matters such as nitrogen, phosphorus, potassium and the like, mineralized trace elements, trace elements and organic active substances, and directly acts on crops through the release, conversion, exchange and replacement of active enzyme, so that direct and indirect nutrient substances required by the growth of the plants are provided, and the water retention and the fertility increasing capability can be improved.
The zeolite powder can also help crops to absorb, transfer and store organic fertilizers, help seedlings of the crops to absorb natural nitrogen fertilizers in the air, decompose more mineral nutrients in soil, is beneficial to a soil recovery system, can meet the nutritional requirements of plants in the growth process, and has the effects of improving the crop yield and improving the product quality;
(3) the pesticide-fertilizer mixture comprises steel slag powder, wherein the steel slag powder contains a large amount of calcium, silicon and phosphorus, contains various nutrients, and can be used as a quick-acting and aftereffect composite mineral fertilizer. The steel slag powder contains a large amount of silicon and sio2More than 15 percent, can be used as silicon fertilizer, the steel slag powder is ground to below 60 meshes to be used as the silicon fertilizer, and the yield can be increased by about 10 percent when the silicon fertilizer is used in rice.
The steel slag powder also contains phosphorus, and practice proves that the steel slag powder is used as a phosphate fertilizer (p)2o5The content is more than 10 percent), even the common steel slag (p)2o5The content is more than 4 percent and more than 7 percent), and the steel slag powder also contains trace elements such as zinc, manganese, iron, copper and the like, and has fertilizer effects of different degrees on different soils and different crops which lack the trace elements.
The steel slag powder has high cao and mgo content and the function of improving acid soil, can be used as an acid soil improver because soil in many areas of China is deficient in phosphorus or acidic, utilizes phosphorus and various trace elements in the steel slag, is not only suitable for acid soil, but also can increase yield when used in phosphorus-deficient alkaline soil. The invention has good effect of paddy field application, and the effect of the steel slag fertilizer can still be achieved even in dry farmland, and the invention is suitable for all crops.
In addition, as the steel slag is calcined at high temperature in the smelting process, the solubility of the steel slag is greatly changed, the soluble amount of various main components contained in the steel slag reaches 1/3-1/2% of the total amount, and some steel slag are even higher and are easily absorbed by plants.
(4) The pesticide-fertilizer mixture is used by the cooperation of the steel slag powder and the zeolite powder, so that the yield of the pesticide-fertilizer mixture is greatly increased when the pesticide-fertilizer mixture is applied to a crop field, and the yield can be increased by 5-16 percent generally. Particularly, when the weight ratio of the steel slag powder to the zeolite powder is 3:2 hours, the yield increasing effect is most obvious and can reach 16 percent at most.
Detailed Description
Those not indicated in the examples of the present invention were carried out under the conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products commercially available. The raw materials used in the examples are all commercially available. Wherein:
the urea is purchased from China oil and gas group, Inc., and the specification is 40 kg/bag;
the diammonium phosphate is purchased from Yuntian chemical group, Limited liability company, and the specification is 50 kg/bag;
the monoammonium phosphate is purchased from Sichuan assorted 37025and chemical company Limited, and the specification is 50 kg/bag;
the ammonium sulfate is purchased from China oil and gas group, Inc., and the specification is 50 kg/bag;
the potassium sulfate is purchased from Limited liability company of Xinjiang apocynum potassium salt and has the specification of 50 kg/bag;
the zinc sulfate is purchased from Hebei Yuanzhong Dazhongzheng Biotech limited and has the specification of 50 kg/bag;
the animal and plant fatty acid is purchased from bioscience and technology Limited, Suzhou Fu, and has a specification of 25 kg/barrel;
the sulfuric acid is purchased from Harbin chemical industry Co., Ltd, and the specification is 25 kg/barrel;
the zeolite powder is purchased from zeolite powder factories of Dehui city, Jilin province, and the specification is 50 kg;
the steel slag powder is purchased from Atheny Steel Co., Ltd, Xilin Steel group, and has a specification of 50kg bags;
the furfural residues are purchased from cattle furfural factories in Wuchang market, and the specification is 25 kg/bag;
the thiram is purchased from Shandong Guihe Biotechnology Co., Ltd, and the specification is 25 kg/bag;
the metalaxyl is purchased from Zhejiang grass science and technology Limited and has the specification of 25 kg/bag;
the tebuconazole is purchased from Shaanxi Kanghuitong Biotechnology pharmaceutical Co., Ltd, and the specification is 25 kg/bag;
the trifloxystrobin is purchased from Song aquatic mountain biotechnology limited company, and the specification is 10 kg/box;
the hymexazol is purchased from Shanxi Yuancheng Lukang actual company Limited, and the specification is 25 kg/barrel;
the paclobutrazol is purchased from Chongqing Tree Rong crop science Co., Ltd, and the specification is 25 kg/bag;
the naphthylacetic acid is purchased from Taida crop science, Zhejiang, and has the specification of 25 kg/bag;
the mepiquat chloride is purchased from Mikan cotton well Biotech limited and has a specification of 10 kg/box;
the uniconazole was purchased from Jinghong Biotechnology Limited, Jiangsu, with a specification of 25 kg/bag.
It should be noted that the above are only sources of the raw materials used in this embodiment, and the raw materials of the present invention may also be other conventional products sold in the market, and the implementation of the technical solution and the implementation of the technical effect of the present invention are not affected by the raw materials of different manufacturers and models.
Example 1
The pesticide-fertilizer mixture comprises the following raw materials in parts by weight:
20 parts of nitrogen and phosphorus fertilizer, 50 parts of potassium fertilizer, 0.1 part of zinc sulfate, 60 parts of animal and vegetable fatty acid, 25 parts of sulfuric acid, 60 parts of zeolite powder, 30 parts of steel slag powder, 60 parts of furfural slag, 5 parts of bactericide and 0.18 part of regulator.
Wherein, the nitrogen and phosphorus fertilizer is urea, diammonium phosphate, monoammonium phosphate and ammonium sulfate according to the proportion of 1:1:1:1 by weight ratio. The potash fertilizer is potassium sulfate. The bactericide is prepared by mixing thiram, metalaxyl, tebuconazole, trifloxystrobin and hymexazol according to the weight ratio of 1:1:1:1: 1. The regulator is prepared by mixing paclobutrazol, uniconazole, naphthylacetic acid and mepiquat chloride according to the weight ratio of 1:1:1: 1.
The preparation method comprises the following steps:
the fertilizer is prepared by uniformly mixing nitrogen phosphorus fertilizer, potash fertilizer, zinc sulfate, animal and vegetable fatty acid, sulfuric acid, zeolite powder, steel slag powder, furfural slag, bactericide and regulator in selected parts by weight.
It should be noted that, those skilled in the art may also add other components to the powder mixture of the present invention according to the actual situation, for example, a surfactant may also be added to the fertilizer mixture.
Example 2
The pesticide-fertilizer mixture comprises the following raw materials in parts by weight:
300 parts of nitrogen and phosphorus fertilizer, 1 part of potash fertilizer, 15 parts of zinc sulfate, 30 parts of animal and vegetable fatty acid, 50 parts of sulfuric acid, 30 parts of zeolite powder, 60 parts of steel slag powder, 1 part of furfural slag, 0.1 part of bactericide and 0.02 part of regulator.
Wherein, the nitrogen and phosphorus fertilizer is urea, diammonium phosphate, monoammonium phosphate and ammonium sulfate according to the ratio of 5: 1:3:1 by weight ratio. The potash fertilizer is potassium sulfate. The bactericide is prepared by mixing thiram, metalaxyl, tebuconazole, trifloxystrobin and hymexazol according to the weight ratio of 1:3:1:2: 1. The regulator is prepared by mixing paclobutrazol, uniconazole, naphthylacetic acid and mepiquat chloride according to the weight ratio of 1:3:1: 1.
The preparation method comprises the following steps:
the fertilizer is prepared by uniformly mixing nitrogen phosphorus fertilizer, potash fertilizer, zinc sulfate, animal and vegetable fatty acid, sulfuric acid, zeolite powder, steel slag powder, furfural slag, bactericide and regulator according to the selected weight parts.
Example 3
The pesticide-fertilizer mixture comprises the following raw materials in parts by weight:
160 parts of nitrogen and phosphorus fertilizer, 25 parts of potash fertilizer, 8 parts of zinc sulfate, 1 part of animal and vegetable fatty acid, 25 parts of sulfuric acid, 1 part of zeolite powder, 1 part of steel slag powder, 30 parts of furfural slag, 10 parts of bactericide and 0.1 part of regulator.
Wherein, the nitrogen and phosphorus fertilizer is urea, diammonium phosphate, monoammonium phosphate and ammonium sulfate according to the ratio of 2: 1:1:1 by weight ratio. The potash fertilizer is potassium sulfate. The bactericide is prepared by mixing thiram, metalaxyl, tebuconazole, trifloxystrobin and hymexazol according to the weight ratio of 1:1:3:1: 1. The regulator is prepared by mixing paclobutrazol, uniconazole, naphthylacetic acid and mepiquat chloride according to the weight ratio of 3:1:1: 2.
The preparation method comprises the following steps:
the fertilizer is prepared by uniformly mixing nitrogen phosphorus fertilizer, potash fertilizer, zinc sulfate, animal and vegetable fatty acid, sulfuric acid, zeolite powder, steel slag powder, furfural slag, bactericide and regulator according to the selected weight parts.
Example 4
The pesticide-fertilizer mixture comprises the following raw materials in parts by weight:
5 parts of urea, 12 parts of diammonium phosphate, 10 parts of monoammonium phosphate, 60 parts of ammonium sulfate, 7 parts of potassium sulfate, 1.5 parts of zinc sulfate, 5 parts of animal and plant fatty acid, 4 parts of sulfuric acid, 10 parts of zeolite powder, 8 parts of steel slag powder, 10 parts of furfural slag, 0.5 part of thiram, 0.5 part of metalaxyl, 0.1 part of tebuconazole, 0.4 part of trifloxystrobin, 0.40 part of hymexazol, 0.03 part of paclobutrazol, 0.05 part of naphthylacetic acid, 0.03 part of mepiquat chloride and 0.03 part of uniconazole.
The preparation method comprises the following steps:
step one, mixing and stirring the furfural residues, zeolite powder, steel residue powder, animal and plant fatty acid and sulfuric acid uniformly, and crushing to 40 meshes to obtain a mixture;
step two, taking urea and diammonium phosphate as the nitrogen and phosphorus fertilizer, and respectively crushing the urea and the diammonium phosphate to 40 meshes;
thirdly, taking monoammonium phosphate and ammonium sulfate as the nitrogen and phosphorus fertilizer, taking potassium sulfate as a potassium fertilizer, taking thiram, metalaxyl, tebuconazole, trifloxystrobin and hymexazol as the bactericides, taking uniconazole, paclobutrazol, naphthylacetic acid and mepiquat chloride as regulators, sequentially feeding the materials according to the sequence of the monoammonium phosphate, the ammonium sulfate, the potassium sulfate, zinc sulfate, the thiram, the metalaxyl, the tebuconazole, the trifloxystrobin, the hymexazol, the paclobutrazol, the naphthylacetic acid, the mepiquat and the uniconazole, mixing for more than 30min, adding the urea and the diammonium phosphate obtained in the second step, continuously mixing for more than 15min, finally adding the mixture obtained in the first step, and continuously mixing for more than 30min to obtain a medicine-fertilizer mixture;
step four, bagging, weighing and sealing the pesticide-fertilizer mixture obtained in the step three.
Example 5
The pesticide-fertilizer mixture comprises the following raw materials in parts by weight:
16 parts of urea, 1 part of diammonium phosphate, 15 parts of monoammonium phosphate, 30 parts of ammonium sulfate, 3 parts of potassium sulfate, 0.9 part of zinc sulfate, 10 parts of animal and plant fatty acid, 8 parts of sulfuric acid, 15 parts of zeolite powder, 12 parts of steel slag powder, 15 parts of furfural slag, 0.8 part of thiram, 0.2 part of metalaxyl, 0.7 part of tebuconazole, 0.5 part of trifloxystrobin, 0.65 part of hymexazol, 0.01 part of paclobutrazol, 0.012 part of naphthylacetic acid, 0.015 part of mepiquat chloride and 0.06 part of uniconazole.
The preparation method comprises the following steps:
step one, mixing and stirring the furfural residues, zeolite powder, steel residue powder, animal and plant fatty acid and sulfuric acid uniformly, and crushing to 80 meshes to obtain a mixture;
step two, taking urea and diammonium phosphate as the nitrogen and phosphorus fertilizer, and respectively crushing the urea and the diammonium phosphate to 80 meshes;
thirdly, taking monoammonium phosphate and ammonium sulfate as the nitrogen and phosphorus fertilizer, taking potassium sulfate as a potassium fertilizer, taking thiram, metalaxyl, tebuconazole, trifloxystrobin and hymexazol as the bactericides, taking uniconazole, paclobutrazol, naphthylacetic acid and mepiquat chloride as regulators, sequentially feeding the materials according to the sequence of the monoammonium phosphate, the ammonium sulfate, the potassium sulfate, zinc sulfate, the thiram, the metalaxyl, the tebuconazole, the trifloxystrobin, the hymexazol, the paclobutrazol, the naphthylacetic acid, the mepiquat and the uniconazole, mixing for more than 30min, adding the urea and the diammonium phosphate obtained in the second step, continuously mixing for more than 15min, finally adding the mixture obtained in the first step, and continuously mixing for more than 30min to obtain a medicine-fertilizer mixture;
and step four, extruding and granulating the pesticide-fertilizer mixture obtained in the step three, bagging, weighing and sealing.
Example 6
The pesticide-fertilizer mixture comprises the following raw materials in parts by weight:
10 parts of urea, 6 parts of diammonium phosphate, 12 parts of monoammonium phosphate, 45 parts of ammonium sulfate, 5 parts of potassium sulfate, 2 parts of zinc sulfate, 12 parts of animal and plant fatty acid, 6 parts of sulfuric acid, 6 parts of zeolite powder, 15 parts of steel slag powder, 12 parts of furfural slag, 0.6 part of thiram, 0.3 part of metalaxyl, 0.4 part of tebuconazole, 0.26 part of trifloxystrobin, 0.11 part of hymexazol, 0.05 part of paclobutrazol, 0.03 part of naphthylacetic acid, 0.02 part of mepiquat chloride and 0.045 part of uniconazole.
The preparation method comprises the following steps:
step one, mixing and stirring the furfural residues, zeolite powder, steel residue powder, animal and plant fatty acid and sulfuric acid uniformly, and crushing to 60 meshes to obtain a mixture;
step two, taking urea and diammonium phosphate as the nitrogen and phosphorus fertilizer, and respectively crushing the urea and the diammonium phosphate to 60 meshes;
thirdly, taking monoammonium phosphate and ammonium sulfate as the nitrogen and phosphorus fertilizer, taking potassium sulfate as a potassium fertilizer, taking thiram, metalaxyl, tebuconazole, trifloxystrobin and hymexazol as the bactericides, taking uniconazole, paclobutrazol, naphthylacetic acid and mepiquat chloride as regulators, sequentially feeding the materials according to the sequence of the monoammonium phosphate, the ammonium sulfate, the potassium sulfate, zinc sulfate, the thiram, the metalaxyl, the tebuconazole, the trifloxystrobin, the hymexazol, the paclobutrazol, the naphthylacetic acid, the mepiquat and the uniconazole, mixing for more than 30min, adding the urea and the diammonium phosphate obtained in the second step, continuously mixing for more than 15min, finally adding the mixture obtained in the first step, and continuously mixing for more than 30min to obtain a medicine-fertilizer mixture;
and step four, extruding and granulating the pesticide-fertilizer mixture obtained in the step three, bagging, weighing and sealing.
Example 7
The pesticide-fertilizer mixture comprises the following raw materials in parts by weight:
8 parts of urea, 4 parts of diammonium phosphate, 12 parts of monoammonium phosphate, 45 parts of ammonium sulfate, 5 parts of potassium sulfate, 1 part of zinc sulfate, 7 parts of animal and plant fatty acid, 6 parts of sulfuric acid, 10 parts of zeolite powder, 15 parts of steel slag powder, 12 parts of furfural slag, 0.6 part of thiram, 0.3 part of metalaxyl, 0.4 part of tebuconazole, 0.2 part of trifloxystrobin, 0.5 part of hymexazol, 0.03 part of paclobutrazol, 0.026 part of naphthylacetic acid, 0.02 part of mepiquat chloride and 0.05 part of uniconazole.
The preparation method comprises the following steps:
the preparation method comprises the following steps:
step one, mixing and stirring the furfural residues, zeolite powder, steel residue powder, animal and plant fatty acid and sulfuric acid uniformly, and crushing to 40 meshes to obtain a mixture;
step two, taking urea and diammonium phosphate as the nitrogen and phosphorus fertilizer, and respectively crushing the urea and the diammonium phosphate to 80 meshes;
thirdly, taking monoammonium phosphate and ammonium sulfate as the nitrogen and phosphorus fertilizer, taking potassium sulfate as a potassium fertilizer, taking thiram, metalaxyl, tebuconazole, trifloxystrobin and hymexazol as the bactericides, taking uniconazole, paclobutrazol, naphthylacetic acid and mepiquat chloride as regulators, sequentially feeding the materials according to the sequence of the monoammonium phosphate, the ammonium sulfate, the potassium sulfate, zinc sulfate, the thiram, the metalaxyl, the tebuconazole, the trifloxystrobin, the hymexazol, the paclobutrazol, the naphthylacetic acid, the mepiquat and the uniconazole, mixing for more than 30min, adding the urea and the diammonium phosphate obtained in the second step, continuously mixing for more than 15min, finally adding the mixture obtained in the first step, and continuously mixing for more than 30min to obtain a medicine-fertilizer mixture;
and step four, extruding and granulating the pesticide-fertilizer mixture obtained in the step three, bagging, weighing and sealing.
Comparative example 1
The pesticide-fertilizer mixture of the comparative example is completely the same as the raw materials and the raw material dosage in example 1, and is different from the pesticide-fertilizer mixture except that zeolite powder and steel slag powder are not included.
The insecticide-fertilizer mixture of the comparative example was prepared by the same preparation method as in example 1.
Comparative example 2
The pesticide-fertilizer mixture of the comparative example is completely the same as the raw materials and the raw material dosage in example 1, and is different from the traditional pesticide-fertilizer mixture except that zeolite powder is not included.
The insecticide-fertilizer mixture of the comparative example was prepared by the same preparation method as in example 1.
Comparative example 3
The pesticide-fertilizer mixture of the comparative example is completely the same as the raw materials and the raw material dosage in example 1, and is different from the method only in that the steel slag powder is not included.
The insecticide-fertilizer mixture of the comparative example was prepared by the same preparation method as in example 1.
Examples of Effect test
In order to verify the technical effect of the pesticide-fertilizer mixture, the following experiments are carried out:
fertilizer effect test for continuously planting rice for 3 years
Selecting a rice test field on a red light farm in the Sublyseius area of Heilongjiang province for carrying out a fertilizer effect application test in 2015-2017 continuously for 3 years; sowing at the end of 3 months, transplanting after 5 months, and harvesting after 10 months of maturity. The test fields are divided into 10 blocks with the same size, and are numbered 1-10 groups respectively, and the pesticide-fertilizer mixture prepared in the examples 1-7 and the comparative examples 1-3 is applied to 1-10 groups respectively. And (3) carrying out soil mixing and seedling raising on 4-1 day and seedling bed broadcasting each pesticide fertilizer once on 5-12 days each year in each test field, applying the same amount of pesticide fertilizer each time, using other cultivation management measures to the local paddy field, calculating the yield per mu after crops are mature and harvested, and calculating the yield increase rate by taking the yield per mu in the 8 th group as a control group.
The results of the above experiments are shown in the following table:
TABLE 1 Rice test field Fertilizer test results
Figure BDA0001742808120000101
Figure BDA0001742808120000111
Second, fertilizer efficiency test of continuously planting soybean for 3 years
Selecting a soybean test field in Zhao Guang farm in Sublized area of Heilongjiang province for fertilizer effect application test in 2015-2017; sowing in 5 months and harvesting after 10 months of maturity. The test fields are divided into 10 blocks with the same size, and are numbered 1-10 groups respectively, and the pesticide-fertilizer mixture prepared in the examples 1-7 and the comparative examples 1-3 is applied to 1-10 groups respectively. Each test field is applied with the pesticide fertilizer once every 5 months and 6 days every year, the same amount of pesticide fertilizer is applied every time, other cultivation management measures are the same as those of the local soybean field, the yield per mu is calculated after crops are mature and harvested, and the yield increase rate is calculated by taking the yield per mu in the 8 th group as a control group.
The results of the above experiments are shown in the following table:
TABLE 2 Soybean test field Fertilizer test results
Figure BDA0001742808120000121
Figure BDA0001742808120000131
Fertilizer effect test for 3-year continuous corn planting
Selecting a corn test field in Lianzhushan Zhengguang village in Mishan city of Heilongjiang province for carrying out fertilizer effect application test in 2015-2017 continuously for 3 years; sowing in late ten months and harvesting after 10 months of maturity. The test fields are divided into 10 blocks with the same size, and are numbered 1-10 groups respectively, and the pesticide-fertilizer mixture prepared in the examples 1-7 and the comparative examples 1-3 is applied to 1-10 groups respectively. Each test field is applied with each pesticide fertilizer once every 4 months and 26 days every year, the same amount of pesticide fertilizer is applied every time, other cultivation and management measures are the same as those of a local corn field, after crops are mature and harvested, the yield per mu is calculated, and the yield increase rate is calculated by taking the yield per mu in the 8 th group as a control group.
The results of the above experiments are shown in the following table:
TABLE 3 Fertilizer test results for corn test field
Figure BDA0001742808120000132
Figure BDA0001742808120000141
Four, fertilizer efficiency test for continuously planting potatoes for 3 years
Selecting a potato test field in a concentric village of the Jianghuan province, the Jianghuan city and the Reynaudian city for carrying out a fertilizer effect application test in 2015-2017 continuously for 3 years; sowing in late ten months and harvesting after 9 months of maturity. The test fields are divided into 10 blocks with the same size, and are numbered 1-10 groups respectively, and the pesticide-fertilizer mixture prepared in the examples 1-7 and the comparative examples 1-3 is applied to 1-10 groups respectively. Each test field is applied with each pesticide fertilizer once every 4 months and 28 days every year, the same amount of pesticide fertilizer is applied every time, other cultivation and management measures are the same as those of the local potato field, the yield per mu is calculated after crops are mature and harvested, and the yield increase rate is calculated by taking the yield per mu in the 8 th group as a control group.
The results of the above experiments are shown in the following table:
TABLE 4 Fertilizer test results for Potato test fields
Figure BDA0001742808120000142
Figure BDA0001742808120000151
Figure BDA0001742808120000161
It can be seen from this that: the pesticide-fertilizer mixture has a good yield increase effect, and particularly has a good yield increase effect when the steel slag powder and the zeolite powder are used together, and the yield increase effect is most remarkable when the ratio of the steel slag powder to the zeolite powder is 3: 2.
It will be appreciated by those skilled in the art that the invention may be embodied in other specific forms without departing from the spirit or essential characteristics thereof. The embodiments disclosed above are therefore to be considered in all respects as illustrative and not restrictive. All changes which come within the scope of or equivalence to the invention are intended to be embraced therein.

Claims (1)

1. The pesticide-fertilizer mixture is characterized by comprising the following raw materials in parts by weight:
8 parts of urea, 4 parts of diammonium phosphate, 12 parts of monoammonium phosphate, 45 parts of ammonium sulfate, 5 parts of potassium sulfate, 1 part of zinc sulfate, 7 parts of animal and plant fatty acid, 6 parts of sulfuric acid, 10 parts of zeolite powder, 15 parts of steel slag powder, 12 parts of furfural slag, 0.6 part of thiram, 0.3 part of metalaxyl, 0.4 part of tebuconazole, 0.2 part of trifloxystrobin, 0.5 part of hymexazol, 0.03 part of paclobutrazol, 0.05 part of uniconazole, 0.026 part of naphthylacetic acid and 0.02 part of mepiquat;
the preparation method of the pesticide-fertilizer mixture comprises the following steps:
step one, mixing and stirring the furfural residues, zeolite powder, steel residue powder, animal and plant fatty acid and sulfuric acid uniformly, and crushing to 40-80 meshes to obtain a mixture;
step two, taking urea and diammonium phosphate as nitrogen and phosphorus fertilizers, and respectively crushing the urea and the diammonium phosphate to 40-80 meshes;
thirdly, taking monoammonium phosphate and ammonium sulfate as nitrogen and phosphorus fertilizers, potassium sulfate as potassium fertilizers, thiram, metalaxyl, tebuconazole, trifloxystrobin and hymexazol as bactericides, uniconazole, paclobutrazol, naphthylacetic acid and mepiquat chloride as regulators, sequentially feeding the materials according to the sequence of the monoammonium phosphate, the ammonium sulfate, the potassium sulfate, zinc sulfate, thiram, the metalaxyl, tebuconazole, trifloxystrobin, the hymexazol, the paclobutrazol, the naphthylacetic acid, the mepiquat chloride and the uniconazole, mixing and stirring for more than 30min, adding the urea and the diammonium phosphate obtained in the second step, continuously mixing and stirring for more than 15min, finally adding the mixture obtained in the first step, and continuously mixing and stirring for more than 30min to obtain a medicine-fertilizer mixture;
step four, bagging, weighing and sealing the pesticide-fertilizer mixture obtained in the step three; or granulating, bagging, weighing and sealing the pesticide-fertilizer mixture obtained in the third step.
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