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CN101597682B - Process for ultrafining heat-treatment on crystal grains of axle steel - Google Patents

Process for ultrafining heat-treatment on crystal grains of axle steel Download PDF

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Publication number
CN101597682B
CN101597682B CN 200910304174 CN200910304174A CN101597682B CN 101597682 B CN101597682 B CN 101597682B CN 200910304174 CN200910304174 CN 200910304174 CN 200910304174 A CN200910304174 A CN 200910304174A CN 101597682 B CN101597682 B CN 101597682B
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temperature
heating
fine
axle steel
ultra
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CN101597682A (en
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梁益龙
王兴安
雷旻
杨明
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Guizhou University
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Guizhou University
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Abstract

本发明公开了一种车轴钢晶粒超细化热处理工艺,它将低中碳车轴钢零件通过波动加热的方式将其加热到临界点Ac3附近的温度,以获得超细化奥氏体晶粒和少量的细化铁素体,在进行波动加热时,温度的波动范围要求不超过Ac3±10℃,并且根据零件的有效直径将加热时间控制在4mm/min;当波动加热完成后,再将加热温度提高5℃~10℃,并保持到整个零件截面上的温度基本一致时即可按常规热处理工艺对零件进行淬火回火处理。本发明通过在临界点Ac3附近温度进行波动加热,以获得超细化奥氏体晶粒和少量的极细小块状铁素体后直接淬火,获得以超细化马氏体组织加超细化铁素体的复相组织,可以显著韧化和塑化材料。The invention discloses an ultra-fine heat treatment process for axle steel grains, which heats low- and medium-carbon axle steel parts to a temperature near the critical point A c3 through wave heating to obtain ultra-fine austenite grains. grains and a small amount of refined ferrite, when wave heating is performed, the temperature fluctuation range is required not to exceed A c3 ±10°C, and the heating time is controlled at 4mm/min according to the effective diameter of the part; when the wave heating is completed, Then increase the heating temperature by 5°C to 10°C, and keep it until the temperature on the entire part cross-section is basically the same, then the parts can be quenched and tempered according to the conventional heat treatment process. In the present invention, the temperature is fluctuated and heated near the critical point A c3 to obtain ultra-fine austenite grains and a small amount of extremely fine massive ferrite, and then directly quenched to obtain ultra-fine martensite structure plus ultra-fine The multiphase structure of ferrite can significantly toughen and plasticize the material.

Description

车轴钢晶粒超细化热处理工艺Heat treatment process for ultra-fine grain of axle steel

技术领域 technical field

本发明涉及一种车轴钢晶粒超细化热处理工艺,属于金属热处理技术领域。The invention relates to an ultra-fine heat treatment process for axle steel crystal grains, belonging to the technical field of metal heat treatment.

背景技术 Background technique

近年来随着列车的提速对机车的性能提出了新的挑战,从而对火车车轴性能也提出了更高的要求。要求轮、轴应有足够的强度和冲击韧性,以保证在最高速度与载荷下,绝对安全可靠。轮、轴对于高速列车来说是直接关系列车安全的至关重要的零部件。因此,世界各国都十分重视轮、轴的材料与工艺研究开发。目前车轴热处理大多采用调质热处理加表面强化处理的工艺路线。这种方法存在以下问题,一是车轴在前期进行锻造时具有较粗大的晶粒尺寸,后续热处理易于发生组织遗传导致调质热处理后也具有粗大的晶粒尺寸。二是调质加热过程温度较高导致混晶现象出现,降低强韧性对列车的运行安全产生威胁。因此,现有的车轴钢热处理工艺的效果还是不够理想。In recent years, with the speed increase of trains, new challenges have been put forward to the performance of locomotives, thus higher requirements have been put forward for the performance of train axles. It is required that the wheels and shafts should have sufficient strength and impact toughness to ensure absolute safety and reliability under the highest speed and load. Wheels and axles are vital components directly related to train safety for high-speed trains. Therefore, all countries in the world attach great importance to the research and development of materials and processes for wheels and shafts. At present, the heat treatment of axles mostly adopts the process route of quenching and tempering heat treatment plus surface strengthening treatment. This method has the following problems. First, the axle has a relatively coarse grain size when it is forged in the early stage, and subsequent heat treatment is prone to tissue inheritance, resulting in a coarse grain size after quenching and tempering heat treatment. The second is that the high temperature in the quenching and tempering heating process leads to the phenomenon of mixed crystals, which reduces the strength and toughness and poses a threat to the safety of train operation. Therefore, the effect of the existing axle steel heat treatment process is still not ideal enough.

发明内容 Contents of the invention

本发明的目的在于:提供一种晶粒尺寸较小、不易出现混晶现象、并且强韧性较高的车轴钢晶粒超细化热处理工艺,以克服现有技术的不足。The purpose of the present invention is to provide an ultra-fine heat treatment process for axle steel grains with smaller grain size, less prone to mixed crystal phenomenon, and higher strength and toughness, so as to overcome the shortcomings of the prior art.

本发明是这样实现的:本发明的一种车轴钢晶粒超细化热处理工艺为,将低中碳车轴钢零件通过波动加热的方式将其加热到临界点Ac3附近的温度,以获得超细化奥氏体晶粒和少量的细化铁素体,在进行波动加热时,温度的波动范围要求不超过Ac3±10℃,并且根据零件的有效直径将加热时间控制在4mm/min;当波动加热完成后,再将加热温度提高5℃~10℃,并保持到整个零件截面上的温度基本一致时即可按常规热处理工艺对零件进行淬火-回火处理。The present invention is realized in the following way: an ultra-fine heat treatment process for axle steel grains of the present invention is to heat the low- and medium-carbon axle steel parts to a temperature near the critical point A c3 by means of wave heating, so as to obtain ultra-fine Refined austenite grains and a small amount of refined ferrite. When performing wave heating, the temperature fluctuation range is required not to exceed A c3 ±10°C, and the heating time is controlled at 4mm/min according to the effective diameter of the part; After the wave heating is completed, increase the heating temperature by 5°C to 10°C, and keep the temperature on the entire part section basically the same, then the parts can be quenched and tempered according to the conventional heat treatment process.

当低中碳车轴钢零件为25CrMoA钢材料时,在795℃~815℃的范围进行波动加热。When the low and medium carbon axle steel parts are 25CrMoA steel materials, wave heating is performed in the range of 795°C to 815°C.

可通过对低中碳车轴钢零件重复进行波动加热和淬火的方式来进一步细化零件的奥氏体晶粒和均匀化奥氏体晶粒。The austenite grains of the parts can be further refined and the austenite grains homogenized by repeated wave heating and quenching of low and medium carbon axle steel parts.

由于采用了上述技术方案,本发明针对现有技术中存在的问题,采用在临界点附近进行波动加热的方式,由于在热加过程同时产生高温回火和奥氏体相变,形核率高、加热温度不高、相变时获得的超细化晶粒不易长大,部分未转变的细小铁素体与超细化奥氏体晶粒共存,直接淬火获得以超细化马氏体为主加少量细小铁素体组成的复相组织。这种组织具有优异的强韧性。因此,本发明通过在临界点Ac3附近温度进行波动加热,可以获得超细化奥氏体晶粒和少量的极细小块状铁素体后直接淬火,获得以超细化马氏体组织加超细化铁素体的复相组织,可以显著韧化和塑化材料。并且,本发明在波动加热完成后通过适当提高加热温度使少量铁素体转变为细小的奥氏体再淬火,即可获得全部的超细化马氏体组织,经回火后具有很高的强度韧性配合对提高车轴的安全性和疲劳寿命都具有重要作用。Due to the adoption of the above-mentioned technical scheme, the present invention aims at the problems existing in the prior art, and adopts the method of wave heating near the critical point. Since high-temperature tempering and austenite transformation are simultaneously produced during the heating process, the nucleation rate is high , the heating temperature is not high, and the ultra-fine grains obtained during phase transformation are not easy to grow, and some untransformed fine ferrite and ultra-fine austenite grains coexist, and direct quenching obtains ultra-fine martensite as the It is mainly composed of a small amount of fine ferrite. This organization has excellent strength and toughness. Therefore, the present invention can obtain superfine austenite grains and a small amount of extremely fine massive ferrite by performing fluctuating heating at a temperature near the critical point Ac3 , and then directly quench to obtain superfine martensite structure plus The multi-phase structure of ultra-fine ferrite can significantly toughen and plasticize the material. Moreover, in the present invention, after the wave heating is completed, by properly increasing the heating temperature to transform a small amount of ferrite into fine austenite and then quenching, all ultra-fine martensite structures can be obtained, which has a high hardness after tempering. The combination of strength and toughness plays an important role in improving the safety and fatigue life of the axle.

下面是本发明与传统工艺加工零件的晶粒度对比如下:Below is that the grain size contrast of the present invention and traditional technology processing parts is as follows:

零件材料:25CrMoA车轴钢Part material: 25CrMoA axle steel

锻造后经传统调质热处理工艺处理后的奥氏体晶粒度5~7级;After forging, the austenite grain size after traditional quenching and tempering heat treatment process is 5-7;

经本发明的热处理工艺处理后的奥氏体晶粒度可达到10~13级。The austenite grain size after the heat treatment process of the present invention can reach 10-13 grades.

通过以上数据对比可知,本发明与现有技术相比,本发明不仅具有处理后的零件晶粒尺寸超细小、不会出现混晶现象的优点,而且本发明还具有能有效提高零件的强韧性和疲劳寿命的优点。Through the comparison of the above data, it can be seen that compared with the prior art, the present invention not only has the advantages of ultra-fine grain size of the processed parts and no mixed crystal phenomenon, but also has the advantages of effectively improving the strength of the parts. Advantages of toughness and fatigue life.

具体实施方式 Detailed ways

本发明的实施例:在对低中碳车轴钢零件进行热处理时,采用本发明的一种车轴钢晶粒超细化热处理工艺进行处理,即将低中碳车轴钢零件通过波动加热的方式将其加热到临界点Ac3附近的温度,以获得超细化奥氏体晶粒和少量的细化铁素体,在进行波动加热时,温度的波动范围要求不超过Ac3±10℃,并且根据零件的有效直径将加热时间控制在4mm/min;当波动加热完成后,再将加热温度提高5℃~10℃,并保持到整个零件截面上的温度基本一致时即可按常规热处理工艺对零件进行淬火-回火处理。Embodiment of the present invention: when heat-treating low- and medium-carbon axle steel parts, a kind of axle steel grain ultra-fine heat treatment process of the present invention is used for treatment, that is, the low- and medium-carbon axle steel parts are heated by waves Heating to a temperature near the critical point A c3 to obtain ultra-fine austenite grains and a small amount of refined ferrite. When performing wave heating, the fluctuation range of temperature is required not to exceed A c3 ±10°C, and according to The effective diameter of the part is to control the heating time at 4mm/min; after the wave heating is completed, the heating temperature is increased by 5°C to 10°C, and when the temperature on the entire part section is basically the same, the part can be treated according to the conventional heat treatment process. Quenching-tempering treatment is carried out.

当低中碳车轴钢零件为25CrMoA钢材料时,最好在795℃~815℃的范围内对其进行波动加热。When the low- and medium-carbon axle steel parts are 25CrMoA steel materials, it is best to heat them with fluctuations in the range of 795 ° C to 815 ° C.

为了使零件获得进一步细化的奥氏体晶粒和均匀化奥氏体晶粒,可按上述方式对低中碳车轴钢零件重复进行波动加热和淬火即成。In order to obtain further refined austenite grains and homogenized austenite grains, the low and medium carbon axle steel parts can be repeatedly heated and quenched in the above-mentioned manner.

Claims (2)

1. a process for ultrafining heat-treatment on crystal grains of axle steel is characterized in that: will hang down middle carbon axle steel part and be heated stagnation point A by the mode that heats that fluctuates C3Near temperature, to obtain super-refinement austenite crystal and a small amount of refinement ferrite, when fluctuating heating, the fluctuation range of temperature requires to be no more than A C3± 10 ℃, and will be controlled at 4mm/min heat-up time according to the effective diameter of part; After fluctuation heating is finished, again Heating temperature is improved 5 ℃~10 ℃, and remain to temperature on the whole part section when basically identical routinely thermal treatment process part is quenched-temper; Described low in carbon axle steel part be the 25CrMoA steel, in the heating of fluctuating of 795 ℃~815 ℃ scopes.
2. process for ultrafining heat-treatment on crystal grains of axle steel according to claim 1 is characterized in that: the austenite crystal and the homogenizing austenite crystal that come further refinement part by the mode that carbon axle steel part in low is repeated to fluctuate heating and quench.
CN 200910304174 2009-07-09 2009-07-09 Process for ultrafining heat-treatment on crystal grains of axle steel Expired - Fee Related CN101597682B (en)

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CN101899556B (en) * 2010-08-11 2012-07-04 内蒙古北方重工业集团有限公司 Heat treatment method for thinning coarse grains of ferrite refractory steel for bearing pressure at high temperature
CN104513893A (en) * 2013-09-26 2015-04-15 长春轨道客车装备有限责任公司 Heat treatment method of EA4T steel axle
CN104128755A (en) * 2014-07-24 2014-11-05 成都亨通兆业精密机械有限公司 GCr15 ring gauge machining technology facilitating machining
CN104117829A (en) * 2014-07-24 2014-10-29 成都亨通兆业精密机械有限公司 Method for manufacturing ring gauge convenient to use with GCr15 as base material
CN104128758A (en) * 2014-07-24 2014-11-05 成都亨通兆业精密机械有限公司 Ring gauge manufacturing method with GCR15 as base materials for facilitating machining
CN104108011A (en) * 2014-07-24 2014-10-22 成都亨通兆业精密机械有限公司 Ring gauge production method
CN104128760A (en) * 2014-07-24 2014-11-05 成都亨通兆业精密机械有限公司 Machining technology of GCr15 ring gauges convenient to use
CN104128756A (en) * 2014-07-24 2014-11-05 成都亨通兆业精密机械有限公司 Machining technology of ring gauges convenient to use
CN104227340A (en) * 2014-07-24 2014-12-24 成都亨通兆业精密机械有限公司 GCr15 ring gauge processing process capable of being conveniently processed mechanically and conveniently used
CN104611526A (en) * 2015-02-06 2015-05-13 桂林理工大学 Heating method for refining 50# steel austenite crystal
CN107130088B (en) * 2016-02-29 2018-08-31 鞍钢股份有限公司 Fluctuation tempering process method
CN106906340B (en) * 2017-03-31 2018-11-27 河南科技大学 A kind of fine grain heat treatment method

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