CN102532941B - Composite brilliant blue disperse dye - Google Patents
Composite brilliant blue disperse dye Download PDFInfo
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- CN102532941B CN102532941B CN2011104573403A CN201110457340A CN102532941B CN 102532941 B CN102532941 B CN 102532941B CN 2011104573403 A CN2011104573403 A CN 2011104573403A CN 201110457340 A CN201110457340 A CN 201110457340A CN 102532941 B CN102532941 B CN 102532941B
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- 239000002131 composite material Substances 0.000 title claims abstract description 43
- SGHZXLIDFTYFHQ-UHFFFAOYSA-L Brilliant Blue Chemical compound [Na+].[Na+].C=1C=C(C(=C2C=CC(C=C2)=[N+](CC)CC=2C=C(C=CC=2)S([O-])(=O)=O)C=2C(=CC=CC=2)S([O-])(=O)=O)C=CC=1N(CC)CC1=CC=CC(S([O-])(=O)=O)=C1 SGHZXLIDFTYFHQ-UHFFFAOYSA-L 0.000 title claims abstract description 39
- 239000000986 disperse dye Substances 0.000 title claims abstract description 39
- 239000000975 dye Substances 0.000 claims abstract description 101
- 239000000178 monomer Substances 0.000 claims abstract description 78
- 239000012752 auxiliary agent Substances 0.000 claims description 39
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 12
- 150000001875 compounds Chemical class 0.000 claims description 10
- 238000009833 condensation Methods 0.000 claims description 10
- 230000005494 condensation Effects 0.000 claims description 10
- 239000007859 condensation product Substances 0.000 claims description 10
- SRDOTWUOTQTGAK-UHFFFAOYSA-N C=O.C1(=CC=CC2=CC=CC=C12)S(=O)(=O)OCC1=CC=CC=C1 Chemical compound C=O.C1(=CC=CC2=CC=CC=C12)S(=O)(=O)OCC1=CC=CC=C1 SRDOTWUOTQTGAK-UHFFFAOYSA-N 0.000 claims description 6
- NVVZQXQBYZPMLJ-UHFFFAOYSA-N formaldehyde;naphthalene-1-sulfonic acid Chemical compound O=C.C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 NVVZQXQBYZPMLJ-UHFFFAOYSA-N 0.000 claims description 6
- WODGMMJHSAKKNF-UHFFFAOYSA-N 2-methylnaphthalene-1-sulfonic acid Chemical compound C1=CC=CC2=C(S(O)(=O)=O)C(C)=CC=C21 WODGMMJHSAKKNF-UHFFFAOYSA-N 0.000 claims description 4
- 229920001732 Lignosulfonate Polymers 0.000 claims description 4
- -1 alkyl naphthalene sulfonic acid formaldehyde Chemical compound 0.000 claims description 4
- 235000019357 lignosulphonate Nutrition 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 229920005552 sodium lignosulfonate Polymers 0.000 claims description 4
- 238000004043 dyeing Methods 0.000 abstract description 14
- 229920000728 polyester Polymers 0.000 abstract description 4
- 238000000859 sublimation Methods 0.000 abstract description 4
- 230000008022 sublimation Effects 0.000 abstract description 4
- 238000005406 washing Methods 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 2
- 238000007639 printing Methods 0.000 abstract description 2
- 239000004615 ingredient Substances 0.000 abstract 1
- 230000008018 melting Effects 0.000 abstract 1
- 238000002844 melting Methods 0.000 abstract 1
- LZWFXVJBIZIHCH-UHFFFAOYSA-N 1-Ethenylhexyl butanoate Chemical compound CCCCCC(C=C)OC(=O)CCC LZWFXVJBIZIHCH-UHFFFAOYSA-N 0.000 description 10
- 239000002270 dispersing agent Substances 0.000 description 9
- 239000004744 fabric Substances 0.000 description 9
- 239000000047 product Substances 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- 238000001035 drying Methods 0.000 description 6
- 238000000227 grinding Methods 0.000 description 5
- 238000005507 spraying Methods 0.000 description 5
- 239000001045 blue dye Substances 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 108091060290 Chromatid Proteins 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 2
- 210000004756 chromatid Anatomy 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- 239000003643 water by type Substances 0.000 description 2
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
- XREZMAAQVYVESP-UHFFFAOYSA-N acetyloxymethyl 2-[n-[2-(acetyloxymethoxy)-2-oxoethyl]-2-[2-[2-[bis[2-(acetyloxymethoxy)-2-oxoethyl]amino]-4-fluorophenoxy]ethoxy]-5-fluoroanilino]acetate Chemical compound CC(=O)OCOC(=O)CN(CC(=O)OCOC(C)=O)C1=CC(F)=CC=C1OCCOC1=CC=C(F)C=C1N(CC(=O)OCOC(C)=O)CC(=O)OCOC(C)=O XREZMAAQVYVESP-UHFFFAOYSA-N 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000006103 coloring component Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000009973 dope dyeing Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000013508 migration Methods 0.000 description 1
- 230000005012 migration Effects 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 238000009970 yarn dyeing Methods 0.000 description 1
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Abstract
The invention discloses a composite brilliant blue disperse dye, which mainly comprises the components in parts by weight as follows: 5-25 parts of dye monomer A shown as formula (I) and 0.05-2 parts of dye monomer B shown as formula (II). The composite brilliant blue disperse dye can be further added with an accessory ingredient. The composite brilliant blue disperse dye is suitable for dyeing polyester materials, coloration and printing. The composite brilliant blue disperse dye has extremely excellent high temperature hot melting dyeing property, excellent fastness, and good insolation fastness, sublimation fastness and washing fastness.
Description
(1) technical field
The present invention relates to a kind of composite brilliant blue disperse dye.
(2) background technology
From the textile fabric present situation, the shared ratio of the fabric that has multiple fiber combinations to form increases year by year, and some the medium-to-high grade fabrics as domestic, comprise polyester blended fabric etc.The dispersed dye of supply in the market, can't well meet the printing and dyeing needs of such textiles: its thermal migration and washing fastness are not ideal enough, have affected the various wet fastness of dope dyeing, and peripheral environment is also brought to more pollution.
(3) summary of the invention
For overcoming the deficiency of existing dispersed dye, the object of the invention is to provide the composite brilliant blue disperse dye that a kind of dye uptake is high, washing fastness good, fastness is good, heat-resisting transport property is little, is suitable for the dyeing of multifilament fabric as the polyester blended fabric.
The technical solution used in the present invention is:
A kind of composite brilliant blue disperse dye mainly forms by following mass parts by the dye monomer A suc as formula shown in (I) with suc as formula the dye monomer B shown in (II):
The 5-25 mass parts suc as formula the dye monomer A shown in (I)
0.05-2 mass parts suc as formula the dye monomer B shown in (II)
Preferred described composite brilliant blue disperse dye mainly forms by following mass parts by the dye monomer A suc as formula shown in (I) with suc as formula the dye monomer B shown in (II):
The 5-15 mass parts suc as formula the dye monomer A shown in (I)
0.05-0.15 mass parts suc as formula the dye monomer B shown in (II).
The implication of above-mentioned " mainly " refers to that the active coloring component of described composite brilliant blue disperse dye is chromatid A and the chromatid B combination with above-mentioned mass fraction, in dyestuff, can also add other on color not impact but dyeing other auxiliary agents commonly used.
Composite brilliant blue disperse dye of the present invention, can be composed of the following components: the 5-25 mass parts suc as formula the dye monomer A shown in (I), the 0.05-2 mass parts suc as formula the dye monomer B shown in (II).This is the former dyestuff that does not add auxiliary agent.
Further, described composite reactive blue dye can also comprise auxiliary agent, and described composite brilliant blue disperse dye is comprised of following component and auxiliary agent:
The 5-25 mass parts suc as formula the dye monomer A shown in (I), 0.05-2 mass parts suc as formula the dye monomer B shown in (II).
Described auxiliary agent quality consumption is generally 2.7～18.8 times of total mass of dye monomer A and dye monomer B, is preferably 5.6～～18.8 times of total mass of dye monomer A and dye monomer B.
Preferred, described composite reactive blue dye forms by following mass fraction by the dye monomer A suc as formula shown in (I) with suc as formula the dye monomer B shown in (II) and auxiliary agent: suc as formula the dye monomer A 5-25 mass parts shown in (I), suc as formula the dye monomer B 0.05-2 mass parts shown in (II), 2.7～18.8 times of the total mass that auxiliary agent quality consumption is dye monomer A and dye monomer B, preferred, the total mass of dye monomer A, dye monomer B and auxiliary agent is 100 mass parts.
Preferred, described composite reactive blue dye forms by following mass fraction by the dye monomer A suc as formula shown in (I) with suc as formula the dye monomer B shown in (II) and auxiliary agent: suc as formula the dye monomer A 5-15 mass parts shown in (I), suc as formula the dye monomer B 0.05-0.15 mass parts shown in (II), 5.6～18.8 times of the total mass that auxiliary agent quality consumption is dye monomer A and dye monomer B, preferred, the total mass of dye monomer A, dye monomer B and auxiliary agent is 100 mass parts.
Most preferred, described composite reactive blue dye forms by following mass fraction by the dye monomer A suc as formula shown in (I) with suc as formula the dye monomer B shown in (II) and auxiliary agent: suc as formula the dye monomer A 5-11 mass parts shown in (I), suc as formula the dye monomer B 0.05-0.13 mass parts shown in (II), 8～18.8 times of the total mass that auxiliary agent quality consumption is dye monomer A and dye monomer B, preferred, the total mass of dye monomer A, dye monomer B and auxiliary agent is 100 mass parts.
Due to the singularity of dye industry, be difficult to also there is no need to make sterling, usually generally can be with a small amount of impurity in some making processes.
Auxiliary agent of the present invention is the dyestuff usual auxiliaries.Usually can be one of following or the mixture of two or more arbitrary proportions: naphthalene sulfonic acidformaldehyde condensation product, alkyl naphthalene sulfonic acid formaldehyde condensation products, sulfonated lignin or benzyl naphthalenesulfonate formaldehyde condensation compound.Described naphthalene sulfonic acidformaldehyde condensation product is as dispersing agent NNO (naphthalene sulfonic acidformaldehyde condensation product); The alkyl naphthalene sulfonic acid formaldehyde condensation products is as Dispersant MF (condensation compound of methyl naphthalene sulfonic acid and formaldehyde); The benzyl naphthalenesulfonate formaldehyde condensation compound is as dispersing agent CNF (benzyl naphthalenesulfonate formaldehyde condensation compound); Sulfonated lignin are as sodium lignosulfonate (as dispersion agent Reax83A, the Reax85A sold on market) etc.This is auxiliary agent commonly used as well known to those skilled in the art.
The preparation method of composite brilliant blue disperse dye provided by the invention is: dye monomer A, dye monomer B, the auxiliary agent that will measure ratio add in water or other wetting agent, carry out grinding distribution with shredder, then spraying drying makes described composite brilliant blue disperse dye.This is to well known to a person skilled in the art the preparation method.Above-mentioned dye monomer A, dye monomer B, can adopt respectively commercially available prod C.I. EX-SF DISPERSE BLUE EX-SF 300 354 former dyestuffs, the former dyestuff of C.I. DISPERSE YELLOW 184:1.
Also can prepare as follows by composite brilliant blue disperse dye of the present invention: first by dye monomer A and auxiliary agent 1, make finished product dyestuff C.I. EX-SF DISPERSE BLUE EX-SF 300 354, by dye monomer B and auxiliary agent 2, make finished product dyestuff C.I. DISPERSE YELLOW 184:1.By above-mentioned finished product dyestuff C.I. EX-SF DISPERSE BLUE EX-SF 300 354, finished product dyestuff C.I. DISPERSE YELLOW 184:1 and auxiliary agent 3 by metering than after adding the water blending, grinding distribution, and then spraying drying makes described composite brilliant blue disperse dye; Or directly buy finished product dyestuff C.I. EX-SF DISPERSE BLUE EX-SF 300 354 and finished product C.I. DISPERSE YELLOW 184:1, then with auxiliary agent 4 by metering than after adding the water blending, grinding distribution, and then spraying drying makes described composite brilliant blue disperse dye.The consumption of described finished product dyestuff C.I. EX-SF DISPERSE BLUE EX-SF 300 354 with the quality of dye monomer A wherein measure, the consumption of finished product dyestuff C.I. DISPERSE YELLOW 184:1 measures with the quality of dye monomer B wherein.Described auxiliary agent 1, auxiliary agent 2, auxiliary agent 3 or auxiliary agent 4 mean the step of using in different step, and can mean identical can be also different auxiliary agents, and those skilled in the art should choose suitable auxiliary agent and prepare dyestuff.
The consumption of described water is generally 1～2 times of total mass of all raw materials.
Composite brilliant blue disperse dye provided by the invention, a kind of dispersed dye of bright blue coloured silk are provided, blueness is very gorgeous, be highly suitable for dying polyester material, yarn dyeing and stamp, high temperature pad-dry-cure dyeing performance is splendid, the fastness excellent property, as sunlight fastness, fastness to sublimation, wash resistant fastness all show well.
(4) accompanying drawing explanation
The dyeing photo of the composite brilliant blue disperse dye that Fig. 1 commercial dye C.I. EX-SF DISPERSE BLUE EX-SF 300 354, C.I. DISPERSE YELLOW 184:1 and embodiment 1 make.
(5) embodiment
Below in conjunction with embodiment, the invention will be further described, but protection scope of the present invention is not limited to this.
Embodiment 1-8
According to continuous data shown in table 1, by dye monomer A (the former dyestuff of C.I. EX-SF DISPERSE BLUE EX-SF 300 354, purchased from Zhejiang rich Australia dyestuffs industries company limited), dye monomer B (the former dyestuff of C.I. DISPERSE YELLOW 184:1, purchased from Zhejiang rich Australia dyestuffs industries company limited), after auxiliary agent (Dispersant MF (condensation compound of methyl naphthalene sulfonic acid and formaldehyde), dispersing agent CNF (benzyl naphthalenesulfonate formaldehyde condensation compound), dispersing agent NNO (naphthalene sulfonic acidformaldehyde condensation product), sodium lignosulfonate) adds the water blending, carry out grinding distribution with shredder, spraying drying gets final product.
Table 1
Example 9-16
According to continuous data shown in table 2, by C.I. EX-SF DISPERSE BLUE EX-SF 300 354 (commercial dyes, monomer A content is 50%, all the other are auxiliary agent, purchased from Zhejiang rich Australia dyestuffs industries company limited), C.I. DISPERSE YELLOW 184:1 (commercial dye, monomers B content is 10%, all the other are auxiliary agent, purchased from Zhejiang rich Australia dyestuffs industries company limited), auxiliary agent (Dispersant MF (condensation compound of methyl naphthalene sulfonic acid and formaldehyde), dispersing agent CNF (benzyl naphthalenesulfonate formaldehyde condensation compound), dispersing agent NNO (naphthalene sulfonic acidformaldehyde condensation product), sodium lignosulfonate) after adding the water blending, carry out grinding distribution with shredder, spraying drying.
Table 2
Embodiment 17
Respectively get the composite brilliant blue disperse dye that 0.5 gram embodiment 1-16 makes, be dispersed in the water of 500 milliliters, mix with 60 ml waters after drawing 20 milliliters.Adjust dye bath pH=5 with acetic acid, be warming up to 70 ℃ and put into wash/cotton of 2 grams simultaneously and dyeed, in 30 minutes, temperature rises to 130 ℃ (2 normal atmosphere) by 70 ℃, is incubated 30 minutes, starts the sampling to the cloth after dyeing while being cooled to 90 ℃ and is detected.Adopt that GB GB/T3921-1997, GB/T3920-1997, GB/T8427-1998, GB/T5718-1997. test respectively that it is water-fastness, rub resistance, colour fastness to light and sub limation fastness.Test result is in Table 3.And the cloth after the composite brilliant blue disperse dye that embodiment 1 is made dyeing takes pictures, accompanying drawing 1 is shown in by photo.
Table 3
| The embodiment title | Water-fastness | Rub resistance | Fast light | Sublimation fastness (90 ℃) |
| Embodiment 1 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 2 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 3 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 4 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 5 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 6 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 7 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 8 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 9 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 10 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 11 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 12 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 13 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 14 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 15 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
| Embodiment 16 | 4 grades | 4～5 grades | 6 grades | 4～5 grades |
Comparative example 1-2
Respectively get 0.5 gram C.I. EX-SF DISPERSE BLUE EX-SF 300 354 (commercial dyes, monomer A content is 50%, all the other are auxiliary agent, purchased from Zhejiang rich Australia dyestuffs industries company limited), C.I. DISPERSE YELLOW 184:1 (commercial dye, monomers B content is 10%, and all the other are auxiliary agent, purchased from Zhejiang rich Australia dyestuffs industries company limited), be dispersed in the water of 500 milliliters, mix with 60 ml waters after drawing 20 milliliters.Adjust dye bath pH=5 with acetic acid, be warming up to 70 ℃ and put into wash/cotton of 2 grams simultaneously and dyeed, in 30 minutes, temperature rises to 130 ℃ (2 normal atmosphere) by 70 ℃, be incubated 30 minutes, take out while being cooled to 90 ℃, after drying, the cloth after dyeing is taken pictures, accompanying drawing 1 is shown in by photo.
From accompanying drawing 1, can find out, the blueness that 354 dyeing of C.I. EX-SF DISPERSE BLUE EX-SF 300 obtain is darker, partially red, and after C.I. DISPERSE YELLOW 184:1 dyeing, is the yellow with fluorescence, and what composite brilliant blue disperse dye dyeing obtained is more gorgeous blueness, slightly partially greenish blue.
Embodiment 18
Get the composite brilliant blue disperse dye that embodiment 1～3 makes, take the commercial dye Disperse Blue-60 as standard specimen, after equal conditions dyeing, test its color scale, acquired results is in Table 4.Can find out both difference.
Table 4
Claims (10)
1. a composite brilliant blue disperse dye is characterized in that described composite brilliant blue disperse dye mainly forms by following mass parts by the dye monomer A suc as formula shown in (I) with suc as formula the dye monomer B shown in (II):
The 5-25 mass parts suc as formula the dye monomer A shown in (I)
0.05-2 mass parts suc as formula the dye monomer B shown in (II)
2. composite brilliant blue disperse dye according to claim 1 is characterized in that described composite brilliant blue disperse dye mainly forms by following mass parts by the dye monomer A suc as formula shown in (I) with suc as formula the dye monomer B shown in (II):
The 5-15 mass parts suc as formula the dye monomer A shown in (I)
0.05-0.15 mass parts suc as formula the dye monomer B shown in (II).
3. composite brilliant blue disperse dye according to claim 1 is characterized in that described composite brilliant blue disperse dye is composed of the following components:
The 5-25 mass parts suc as formula the dye monomer A shown in (I), 0.05-2 mass parts suc as formula the dye monomer B shown in (II).
4. composite brilliant blue disperse dye according to claim 1 is characterized in that described composite brilliant blue disperse dye is comprised of following component and auxiliary agent:
The 5-25 mass parts suc as formula the dye monomer A shown in (I), 0.05-2 mass parts suc as formula the dye monomer B shown in (II).
5. composite brilliant blue disperse dye according to claim 4,2.7～18.8 times of the total mass that the quality consumption that it is characterized in that described auxiliary agent is dye monomer A and dye monomer B.
6. composite brilliant blue disperse dye according to claim 5,5.6～18.8 times of the total mass that the quality consumption that it is characterized in that described auxiliary agent is dye monomer A and dye monomer B.
7. composite brilliant blue disperse dye according to claim 6, it is characterized in that described composite brilliant blue disperse dye forms by following mass fraction by the dye monomer A suc as formula shown in (I) with suc as formula the dye monomer B shown in (II) and auxiliary agent: the 5-15 mass parts suc as formula the dye monomer A shown in (I), 0.05-0.15 mass parts suc as formula the dye monomer B shown in (II), 5.6～18.8 times of the total mass that the quality consumption of auxiliary agent is dye monomer A and dye monomer B.
8. according to the described composite brilliant blue disperse dye of one of claim 4～7, it is characterized in that described auxiliary agent is one of following or the mixture of two or more arbitrary proportions: naphthalene sulfonic acidformaldehyde condensation product, alkyl naphthalene sulfonic acid formaldehyde condensation products, sulfonated lignin or benzyl naphthalenesulfonate formaldehyde condensation compound.
9. composite brilliant blue disperse dye according to claim 8, is characterized in that described alkyl naphthalene sulfonic acid formaldehyde condensation products is condensation compound of methyl naphthalene sulfonic acid and formaldehyde.
10. composite brilliant blue disperse dye according to claim 8, is characterized in that described sulfonated lignin are sodium lignosulfonate.
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| CN103740136B (en) * | 2013-12-29 | 2016-01-06 | 浙江龙盛集团股份有限公司 | A kind of high fastness disperses bright blue dye composite |
| CN107418249B (en) * | 2017-06-23 | 2019-08-16 | 浙江博澳染料工业有限公司 | A kind of bright blue dyestuff of economy composite type dispersion |
| CN114262526A (en) * | 2021-12-30 | 2022-04-01 | 江苏德旺数码科技有限公司 | Disperse dye composition and disperse brilliant blue dye |
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| JPH073179A (en) * | 1993-06-15 | 1995-01-06 | Nippon Kayaku Co Ltd | Ink composition for ink jet printing and dyeing method using the same |
| JP2952134B2 (en) * | 1993-07-09 | 1999-09-20 | キヤノン株式会社 | Ink jet printing method and printed matter |
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| US7582121B2 (en) * | 2005-05-31 | 2009-09-01 | L'oreal S.A. | Composition for dyeing keratin fibers, comprising at least one diamino-N,N-dihydropyrazolone derivative, at least one coupler, and at least one heterocyclic direct dye |
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| WO2006068823A1 (en) * | 2004-12-20 | 2006-06-29 | Eastman Kodak Company | Thermal donor for high-speed printing |
| WO2007123825A3 (en) * | 2006-04-18 | 2008-01-17 | Eastman Kodak Co | Slipping layer for dye-donor element |
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