CN102551211A - Preparation method for instant release type cigarette mouth rod - Google Patents
Preparation method for instant release type cigarette mouth rod Download PDFInfo
- Publication number
- CN102551211A CN102551211A CN2011104386498A CN201110438649A CN102551211A CN 102551211 A CN102551211 A CN 102551211A CN 2011104386498 A CN2011104386498 A CN 2011104386498A CN 201110438649 A CN201110438649 A CN 201110438649A CN 102551211 A CN102551211 A CN 102551211A
- Authority
- CN
- China
- Prior art keywords
- water
- preparation
- cigarette
- cigarette filter
- filter tip
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 120
- 238000002360 preparation method Methods 0.000 title claims abstract description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 61
- 239000006187 pill Substances 0.000 claims abstract description 40
- 239000000725 suspension Substances 0.000 claims abstract description 19
- 239000007788 liquid Substances 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 238000002156 mixing Methods 0.000 claims abstract description 14
- 230000008569 process Effects 0.000 claims abstract description 13
- 239000008367 deionised water Substances 0.000 claims abstract description 7
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 7
- 150000002576 ketones Chemical class 0.000 claims abstract description 5
- 238000005507 spraying Methods 0.000 claims abstract description 3
- 239000010410 layer Substances 0.000 claims description 28
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 26
- 235000010413 sodium alginate Nutrition 0.000 claims description 26
- 239000000661 sodium alginate Substances 0.000 claims description 26
- 229940005550 sodium alginate Drugs 0.000 claims description 26
- 239000000243 solution Substances 0.000 claims description 15
- 238000005516 engineering process Methods 0.000 claims description 11
- 239000004971 Cross linker Substances 0.000 claims description 10
- 230000002308 calcification Effects 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 10
- 230000004927 fusion Effects 0.000 claims description 10
- 239000012943 hotmelt Substances 0.000 claims description 10
- 238000000465 moulding Methods 0.000 claims description 10
- 239000012188 paraffin wax Substances 0.000 claims description 10
- 229920001610 polycaprolactone Polymers 0.000 claims description 10
- 239000004632 polycaprolactone Substances 0.000 claims description 10
- 229920002635 polyurethane Polymers 0.000 claims description 10
- 239000004814 polyurethane Substances 0.000 claims description 10
- 239000007787 solid Substances 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- 239000000463 material Substances 0.000 claims description 9
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 8
- 241000208125 Nicotiana Species 0.000 claims description 6
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 6
- 239000012530 fluid Substances 0.000 claims description 5
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 4
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 239000001110 calcium chloride Substances 0.000 claims description 4
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 4
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 claims description 4
- 229960002401 calcium lactate Drugs 0.000 claims description 4
- 239000001527 calcium lactate Substances 0.000 claims description 4
- 235000011086 calcium lactate Nutrition 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 239000011241 protective layer Substances 0.000 claims description 2
- 239000000779 smoke Substances 0.000 abstract description 6
- 230000000391 smoking effect Effects 0.000 abstract description 4
- 239000002131 composite material Substances 0.000 abstract description 2
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 abstract 3
- 238000000576 coating method Methods 0.000 abstract 3
- 238000004132 cross linking Methods 0.000 abstract 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 238000004140 cleaning Methods 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 239000011259 mixed solution Substances 0.000 description 14
- 239000003205 fragrance Substances 0.000 description 13
- 230000006378 damage Effects 0.000 description 10
- 239000007789 gas Substances 0.000 description 8
- 230000000694 effects Effects 0.000 description 6
- 239000000835 fiber Substances 0.000 description 6
- 230000009467 reduction Effects 0.000 description 6
- 239000000796 flavoring agent Substances 0.000 description 5
- 235000019634 flavors Nutrition 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 4
- 239000003546 flue gas Substances 0.000 description 4
- 239000002304 perfume Substances 0.000 description 4
- 239000007901 soft capsule Substances 0.000 description 4
- 235000021419 vinegar Nutrition 0.000 description 4
- 239000000052 vinegar Substances 0.000 description 4
- 208000027418 Wounds and injury Diseases 0.000 description 3
- 239000000654 additive Substances 0.000 description 3
- 230000000996 additive effect Effects 0.000 description 3
- 208000014674 injury Diseases 0.000 description 3
- 238000009736 wetting Methods 0.000 description 3
- 230000004888 barrier function Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 230000002950 deficient Effects 0.000 description 2
- 241000411851 herbal medicine Species 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 210000000697 sensory organ Anatomy 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 239000007961 artificial flavoring substance Substances 0.000 description 1
- 238000000429 assembly Methods 0.000 description 1
- 230000000712 assembly Effects 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 239000000416 hydrocolloid Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
Images
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
A preparation method for an instant release type cigarette mouth rod relates to a cigarette composite mouth rod and a preparation method of the mouth rod. The preparation method comprises the steps of a dissolving essence for ketone cigarettes into deionized water or mixed liquid of ethanol and water or mixed liquid of the water and propylene glycol according to a proportion of 0.1%-1%, and evenly mixing the liquid; b dissolving sodium alga acid into the liquid in step a, and evenly mixing the liquid in suspension mode to obtain suspension; c dropping the suspension prepared in step b into cross-linking solution through a dropping method to obtain dropping pills; d cleaning cross-linking solution on the surfaces of the dropping pills; e coating coatings on the outer surfaces of the dropping pills according to process of spraying the coatings; and adopting a cigarette mouth rod forming device to prepare the instant release type cigarette mouth rod. The preparation method for the instant release type cigarette mouth rod can maintain moisture in smoke of the cigarette, and can improve integral moist feeling and increase aroma amount by instantly releasing the dropping pills without influencing smoking quality and the style of the cigarette.
Description
Technical field
The present invention relates to a kind of cigarette composite tip stick and preparation method thereof.
Background technology
The dry sense of the flue gas of cigarette is to cause cigarette in unjoyful factor of when suction; When through instant-free type filter stick; Can when suction, discharge moisture, the dried thorn sense in the time of can reducing cigarette smoking greatly improves the suction of cigarette and distinguishes the flavor of; But and the harmful substance in the effectively catching cigarette, reduce the injury of cigarette to a certain extent to human body.
Traditional in addition perfuming cigarette method adds odor additive and does not reach gratifying effect, and fails to arrive the taste of expectation, and combines fragrance emanation property; So that the inhomogeneity of spices in cigarette; Need be to the additive fragrance of cigarette and the assurance of addition, present technique is added the improvement of preserving with medicament with cigarette flavors and is combined, and cigarette flavors is moved in the paper roll cigarette holder stick; It is combined with main flume, thus the particularity of minimizing cigarette taste and sensation.
The number of applying for a patent is 98216267.7 openly to have introduced a kind of Aqueous mouthpiece cigarette; It is that droplet of pinching brokenly or little water column with membrane sealed are added in the fiber of cigarette filter tip, thereby wetting fiber is strengthened filtering function; Thereby alleviate injury to human body; This cigarette is considered the droplet of rod adding or the loading amount of little water column can't be accomplished accurate loading amount, when wetting cigarette is considered excellent fiber, can cause forming paper or yew paper because runny distortion causes suction inconvenience.
The number of applying for a patent is that 201020664191.9 openly to have introduced a kind of instant-free assembly that contains be staple fibre mouth rod; It is the staple fibre filter core that the different shape instant-free assembly that will contain natural perfume material, artificial flavors or Chinese herbal medicine solution places cigarette; Reach and overcome cigarette moist-keeping flavouring or the unabiding defective of fragrance; The instant-free assembly that this cigarette adds is the cigarette filter tip that continues perfuming, rather than instant-free fragrance to be reaching the wetting effect of cigarette characteristic perfume and cigarette rapidly, and on the fragrant suction flavor of the Chinese herbal medicine characteristic of cigarette limitation comparatively.
Number of patent application is 201020671818.3 openly to have introduced a kind of soft capsule assembly mouth rod; Promptly considering rod at cigarette is that some soft capsule assemblies are alternately wrapped up in embedding in the fabric filter element; Aspiration procedure can slightly firmly be squeezed the broken liquid outflow in the soft capsule assembly that make with pointing, and the infiltration tow has reached and remedied cigarette flavor, improves and sucks taste and strengthen the purpose that the excellent filter effect of worry reaches; And can only increase the fragrance of cigarette at present with soft capsule, and to the dry sense of cigarette and do the thorn sense and can't improve.
Number of patent application is 200620006234.8 openly to have introduced a kind of wax-wrapped pill of seal fluid; The liquid of its sealing is alcohol and light-coloured vinegar; Slightly firmly extruding when cigarette smoking, wax-wrapped pill is squeezed broken, and alcohol or light-coloured vinegar discharge and soak the cigarette filter rod fiber; Thereby reach the evolution flue gas, reduce of the injury of flue gas harmful substance human body.The liquid that wax-wrapped pill sealed that adds in this cigarette filter rod comparatively limits to, and is alcohol and light-coloured vinegar, and alcohol and light-coloured vinegar volatilize distinctive odor when releasing, and can cause the inharmonious of flue gas, influence smoking quality.
Number of patent application 200410045085.1 has openly been introduced a kind of reducing tar and reducing harm filter tip; Be about in high hydrocolloid particles parcel of 90-50% and the cigarette tows; Because colloid is moisture more than 95%, and have porous network structure, get water-soluble harmful substance in the adsorbable cigarette smoke.The disclosed filter tip of this patent can't reach the effect of instant-free, and the preservation of moisture can't guarantee also.
Summary of the invention
The object of the invention is intended to overcome the defective of prior art; A kind of brand-new instant-free type cigarette filter rod is provided; Under the prerequisite that does not change cigarette odor-absorbing and style, improve the sense organ comfort of cigarette targetedly, and utilize brand-new cigarette harm reduction system to solve the technical barrier of reducing cigarette tar and reducing harm reduction; The stable storage of flowing shape essence or water-soluble additive in a kind of cigarette filter rod is provided, and the preparation method of the instant-free type cigarette filter tip of ability instant-free.
Its preparation method of preparation method of instant-free type cigarette filter tip of the present invention is following:
A. directly remove the mixing material of ionized water or second alcohol and water or the mixing material and ketone flavouring essence for tobacco of water and propane diols with moisture feeling; According to the ratio of 0.1%-1% the ketone flavouring essence for tobacco is dissolved in the mixing material of mixing material or water and propane diols of deionized water or second alcohol and water, and mixes;
B. get sodium alginate and be dissolved in the liquid that mixes of step a gained, stir with the ratio of weight ratio 0.5-3%, suspendible even suspension;
C. the suspension of b being produced splashes in the crosslinker solution with dropping preparation method, makes its surface mass calcification, forms layer protecting film, and the suspension that wraps step b gained makes dripping pill;
D. after the dripping pill moulding, with its taking-up, place pure water after 1-10 minute, the surface-crosslinked solution of flush away;
E. with solid paraffin; Polycaprolactone; PLA, one or several hot melt fusions of polyurethane place dressing equipment; Technology by spray coating is coated in step c gained dripping pill outer surface with it, becomes the protective layer of tight adhesion in the one or more layers even thickness on surface after making its drying;
F. adopt cigarette filter tip former and the cigarette filter tip equipment complex that adds particle to make an addition in the cigarette filter rod, process instant-free type cigarette filter tip.
Described water is deionized water, and the ratio of water and ethanol is 7-15:10-18, and the ratio of water and propane diols is 5-9:2-5.
The addition of described sodium alginate is the 0.2-1.5% of the moisture weight ratio content of step a gained solution.
The described crosslinked fluid of step c is a kind of or two kinds of mixing in calcium chloride water, the calcium lactate aqueous solution.The mass concentration of a kind of two kinds of mixing in calcium chloride water, the calcium lactate aqueous solution is 1-5%.
The described dropping preparation method of step c drips the system suspension, and the time that splashes in the crosslinked fluid is 0.5-2 minute.
Preparation method of the present invention provides a kind of brand-new instant-free type cigarette filter rod; Under the prerequisite that does not change cigarette odor-absorbing and style; Improve the sense organ comfort of cigarette targetedly, and utilize brand-new cigarette harm reduction system to solve the technical barrier of reducing cigarette tar and reducing harm reduction, the moisture of instant-free and spices; Can in sucking process, can not only keep the moisture in the cigarette smoke; Do not influence the sucking quality and the style of cigarette itself, and, can increase whole moisture feeling of cigarette and perfume quantity through instant-free type dripping pill.And can effectively remove water-soluble harmful substance in the cigarette smoke, reached the effect of harm reduction.
The present invention has realized in sucking process, keeping the moisture in the cigarette smoke, does not influence the sucking quality and the style of cigarette itself, and, can increase whole moisture feeling of cigarette and perfume quantity through instant-free type dripping pill.And can effectively remove water-soluble harmful substance in the cigarette smoke, reached the effect of harm reduction.
Description of drawings
The instant-free type dripping pill structure chart that Fig. 1 gets for preparation method of the present invention is prepared.
Fig. 2 contains the cigarette filter tip of the instant-free type particle that gets according to preparation method's preparation of the present invention.
The specific embodiment
Below in conjunction with accompanying drawing and embodiment the present invention is done further explanation, but be not limited to embodiment.
Embodiment 1
1, get sodium alginate and be dissolved in deionized water, ratio is that 0.5:99.5 stirs, and suspendible is even;
2,1 suspension produced is splashed in the crosslinker solution with dropping preparation method, makes the rapid calcification of its surface mass, form layer protecting film, wrap and with the mixed solution of sodium alginate and water, make dripping pill;
3, after the dripping pill moulding, with its taking-up, place pure water after 30 seconds, the surface-crosslinked liquid of flush away;
4, with solid paraffin; Polycaprolactone; PLA; Polyurethane a kind of or two kinds utilize the hot melt fusion, place dressing equipment by specific technology it to be coated in 2 gained dripping pill outer surfaces, become the functional protection layer of tight adhesion in one or more layers even thickness on surface after making its drying;
5, adopt cigarette filter tip former and special cigarette filter tip equipment complex to make an addition in the cigarette filter rod, process instant-free type cigarette filter tip;
6, suction is estimated, the result as follows:
| Cigarette sample | Gloss (5) | Fragrance (32) | Coordinate (6) | Assorted gas (12) | Excitant (20) | Pleasant impression (25) | Add up to (100) |
| 1 | 4 | 29 | 3 | 5 | 9 | 13 | 63 |
Embodiment 2
1, get sodium alginate and be dissolved in deionized water, ratio is that 1:99 stirs, and suspendible is even;
2,1 suspension produced is splashed in the crosslinker solution with dropping preparation method, makes the rapid calcification of its surface mass, form layer protecting film, wrap and with the mixed solution of sodium alginate and water, make dripping pill;
3, after the dripping pill moulding, with its taking-up, place pure water after 30 seconds, the surface-crosslinked liquid of flush away;
4, with solid paraffin; Polycaprolactone; PLA; Polyurethane a kind of or two kinds utilize the hot melt fusion, place dressing equipment by specific technology it to be coated in 2 gained dripping pill outer surfaces, become the functional protection layer of tight adhesion in one or more layers even thickness on surface after making its drying;
5, adopt cigarette filter tip former and special cigarette filter tip equipment complex to make an addition in the cigarette filter rod, process instant-free type cigarette filter tip;
6, suction is estimated, the result as follows:
| Cigarette sample | Gloss (5) | Fragrance (32) | Coordinate (6) | Assorted gas (12) | Excitant (20) | Pleasant impression (25) | Add up to (100) |
| 1 | 4 | 27 | 3.5 | 5 | 9 | 13 | 63 |
Embodiment 3
1, the second alcohol and water is mixed according to 10:20;
2, get sodium alginate and 1 gained mixed solution suspendible is even, the ratio of sodium alginate and water is that 0.5:99 stirs, and suspendible is even;
3,1 suspension produced is splashed in the crosslinker solution with dropping preparation method, makes the rapid calcification of its surface mass, form layer protecting film, wrap and with the mixed solution of sodium alginate and water, make dripping pill;
4, after the dripping pill moulding, with its taking-up, place pure water after 30 seconds, the surface-crosslinked liquid of flush away;
5, with solid paraffin; Polycaprolactone; PLA, two kinds of one or several of polyurethane utilize the hot melt fusion; Place dressing equipment it to be coated in 3 gained dripping pill outer surfaces, become the functional protection layer of tight adhesion after making its drying in one or more layers even thickness on surface by specific technology;
6, adopt cigarette filter tip former and special cigarette filter tip equipment complex to make an addition in the cigarette filter rod, process instant-free type cigarette filter tip;
7, suction is estimated, the result as follows:
| Cigarette sample | Gloss (5) | Fragrance (32) | Coordinate (6) | Assorted gas (12) | Excitant (20) | Pleasant impression (25) | Add up to (100) |
| 1 | 4 | 29 | 3 | 5 | 9 | 13 | 63 |
Embodiment 4
1, the second alcohol and water is mixed according to 9:11;
2, get sodium alginate and 1 gained mixed solution suspendible is even, the ratio of sodium alginate and water is that 1:99 stirs, and suspendible is even;
3,1 suspension produced is splashed in the crosslinker solution with dropping preparation method, makes the rapid calcification of its surface mass, form layer protecting film, wrap and with the mixed solution of sodium alginate and water, make dripping pill;
4, after the dripping pill moulding, with its taking-up, place pure water after 30 seconds, the surface-crosslinked liquid of flush away;
5, with solid paraffin; Polycaprolactone; PLA; Polyurethane a kind of or two kinds utilize the hot melt fusion, place dressing equipment by specific technology it to be coated in 3 gained dripping pill outer surfaces, become the functional protection layer of tight adhesion in one or more layers even thickness on surface after making its drying;
6, adopt cigarette filter tip former and special cigarette filter tip equipment complex to make an addition in the cigarette filter rod, process instant-free type cigarette filter tip;
7, suction is estimated, the result as follows:
| Cigarette sample | Gloss (5) | Fragrance (32) | Coordinate (6) | Assorted gas (12) | Excitant (20) | Pleasant impression (25) | Add up to (100) |
| 1 | 4 | 29 | 3 | 5 | 9 | 13 | 63 |
Embodiment 5
1, propane diols and water are mixed according to 2:5;
2, get sodium alginate and 1 gained mixed solution suspendible is even, the ratio of sodium alginate and water is that 0.5:99.5 stirs, and suspendible is even;
3,2 suspensions produced are splashed in the crosslinker solution with dropping preparation method, make the rapid calcification of its surface mass, form layer protecting film, wrap and with the mixed solution of sodium alginate and water, make dripping pill;
4, after the dripping pill moulding, with its taking-up, place pure water after 30 seconds, the surface-crosslinked liquid of flush away;
5, with solid paraffin; Polycaprolactone; PLA, polyurethane a kind of or two kinds utilize the hot melt fusion; Place dressing equipment it to be coated in 3 gained dripping pill outer surfaces, become the functional protection layer of tight adhesion after making its drying in one or more layers even thickness on surface by specific technology;
6, adopt cigarette filter tip former and special cigarette filter tip equipment complex to make an addition in the cigarette filter rod, process instant-free type cigarette filter tip;
7, suction is estimated, the result as follows:
| Cigarette sample | Gloss (5) | Fragrance (32) | Coordinate (6) | Assorted gas (12) | Excitant (20) | Pleasant impression (25) | Add up to (100) |
| 1 | 4 | 29 | 3 | 5 | 9 | 13 | 63 |
Embodiment 6
1, propane diols and water are mixed according to 3:7;
2, get sodium alginate and 1 gained mixed solution suspendible is even, the ratio of sodium alginate and water is that 1:99 stirs, and suspendible is even;
3,2 suspensions produced are splashed in the crosslinker solution with dropping preparation method, make the rapid calcification of its surface mass, form layer protecting film, wrap and with the mixed solution of sodium alginate and water, make dripping pill;
4, after the dripping pill moulding, with its taking-up, place pure water after 30 seconds, the surface-crosslinked liquid of flush away;
5, with solid paraffin; Polycaprolactone; PLA, polyurethane a kind of or two kinds utilize the hot melt fusion; Place dressing equipment it to be coated in 3 gained dripping pill outer surfaces, become the functional protection layer of tight adhesion after making its drying in one or more layers even thickness on surface by specific technology;
6, adopt cigarette filter tip former and special cigarette filter tip equipment complex to make an addition in the cigarette filter rod, process instant-free type cigarette filter tip:
7, suction is estimated, the result as follows:
| Cigarette sample | Gloss (5) | Fragrance (32) | Coordinate (6) | Assorted gas (12) | Excitant (20) | Pleasant impression (25) | Add up to (100) |
| 1 | 4 | 29 | 3 | 5 | 9 | 13 | 63 |
Embodiment 7
1, flavouring essence for tobacco and water are mixed according to 0.1:9;
2, get sodium alginate and 1 gained mixed solution suspendible is even, the ratio of sodium alginate and water is that 0.5:99.5 stirs, and suspendible is even;
3,2 suspensions produced are splashed in the crosslinker solution with dropping preparation method, make the rapid calcification of its surface mass, form layer protecting film, wrap and with the mixed solution of sodium alginate and water, make dripping pill;
4, after the dripping pill moulding, with its taking-up, place pure water after 30 seconds, the surface-crosslinked liquid of flush away;
5, with solid paraffin; Polycaprolactone; PLA, polyurethane a kind of or two kinds utilize the hot melt fusion; Place dressing equipment it to be coated in 3 gained dripping pill outer surfaces, become the functional protection layer of tight adhesion after making its drying in one or more layers even thickness on surface by specific technology;
6, adopt cigarette filter tip former and special cigarette filter tip equipment complex to make an addition in the cigarette filter rod, process instant-free type cigarette filter tip;
7, suction is estimated, the result as follows:
| Cigarette sample | Gloss (5) | Fragrance (32) | Coordinate (6) | Assorted gas (12) | Excitant (20) | Pleasant impression (25) | Add up to (100) |
| 1 | 4 | 29 | 3 | 5 | 9 | 13 | 63 |
Embodiment 8
1, flavouring essence for tobacco and water are mixed according to 0.2:9;
2, get sodium alginate and 1 gained mixed solution suspendible is even, the ratio of sodium alginate and water is that 1:99 stirs, and suspendible is even;
3,2 suspensions produced are splashed in the crosslinker solution with dropping preparation method, make the rapid calcification of its surface mass, form layer protecting film, wrap and with the mixed solution of sodium alginate and water, make dripping pill;
4, after the dripping pill moulding, with its taking-up, place pure water after 30 seconds, the surface-crosslinked liquid of flush away;
5, with solid paraffin; Polycaprolactone; PLA, polyurethane a kind of or two kinds utilize the hot melt fusion; Place dressing equipment it to be coated in 3 gained dripping pill outer surfaces, become the functional protection layer of tight adhesion after making its drying in one or more layers even thickness on surface by specific technology;
6, adopt cigarette filter tip former and special cigarette filter tip equipment complex to make an addition in the cigarette filter rod, process instant-free type cigarette filter tip;
7, suction is estimated, the result as follows:
| Cigarette sample | Gloss (5) | Fragrance (32) | Coordinate (6) | Assorted gas (12) | Excitant (20) | Pleasant impression (25) | Add up to (100) |
| 1 | 4 | 29 | 3 | 5 | 9 | 13 | 63 |
Claims (5)
1. the preparation method of instant-free type cigarette filter tip is characterized in that preparation method is following:
A. directly remove the mixing material of ionized water or second alcohol and water or the mixing material and ketone flavouring essence for tobacco of water and propane diols with moisture feeling; According to the ratio of 0.1%-1% the ketone flavouring essence for tobacco is dissolved in the mixing material of mixing material or water and propane diols of deionized water or second alcohol and water, and mixes;
B. get sodium alginate and be dissolved in the liquid that mixes of step a gained, stir with the ratio of weight ratio 0.5-3%, suspendible even suspension;
C. the suspension of b being produced splashes in the crosslinker solution with dropping preparation method, makes its surface mass calcification, forms layer protecting film, and the suspension that wraps step b gained makes dripping pill;
D. after the dripping pill moulding, with its taking-up, place pure water after 1-10 minute, the surface-crosslinked solution of flush away;
E. with solid paraffin; Polycaprolactone; PLA, one or several hot melt fusions of polyurethane place dressing equipment; Technology by spray coating is coated in step c gained dripping pill outer surface with it, becomes the protective layer of tight adhesion in the one or more layers even thickness on surface after making its drying;
F. adopt cigarette filter tip former and the cigarette filter tip equipment complex that adds particle to make an addition in the cigarette filter rod, process instant-free type cigarette filter tip.
2. the preparation method of instant-free type cigarette filter tip according to claim 1 is characterized in that institute's water is a deionized water, and the ratio of water and ethanol is 7-15:10-18, and the ratio of water and propane diols is 5-9:2-5.
The preparation method of instant-free type cigarette filter tip according to claim 1, the addition that it is characterized in that sodium alginate is the 0.2-1.5% of the moisture weight ratio content of step a gained solution.
3. the preparation method of instant-free type cigarette filter tip according to claim 1 is characterized in that, the described crosslinked fluid of step c is a kind of or two kinds of mixing in calcium chloride water, the calcium lactate aqueous solution.
4. the preparation method of instant-free type cigarette filter tip according to claim 4, the mass concentration that it is characterized in that a kind of two kinds of mixing in calcium chloride water, the calcium lactate aqueous solution is 1-5%.
5. the preparation method of instant-free type cigarette filter tip according to claim 1 is characterized in that, the described dropping preparation method of step c drips the system suspension, and the time that splashes in the crosslinked fluid is 0.5-2 minute.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011104386498A CN102551211A (en) | 2011-12-25 | 2011-12-25 | Preparation method for instant release type cigarette mouth rod |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011104386498A CN102551211A (en) | 2011-12-25 | 2011-12-25 | Preparation method for instant release type cigarette mouth rod |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102551211A true CN102551211A (en) | 2012-07-11 |
Family
ID=46398853
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011104386498A Pending CN102551211A (en) | 2011-12-25 | 2011-12-25 | Preparation method for instant release type cigarette mouth rod |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102551211A (en) |
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102972865A (en) * | 2012-12-24 | 2013-03-20 | 华宝食用香精香料（上海）有限公司 | Preparation method of flavoring particles for cigarette filter tip by coating method, obtained product and use |
| CN103071459A (en) * | 2013-01-30 | 2013-05-01 | 福建中烟工业有限责任公司 | Ammonia complex composite capable of selectively reducing ammonia in smoke |
| CN103141939A (en) * | 2013-02-27 | 2013-06-12 | 湖北中烟工业有限责任公司 | Interception agent for reducing phenol content in cigarette smoke and filter stick provided with interception agent |
| CN105105334A (en) * | 2015-07-17 | 2015-12-02 | 云南中烟工业有限责任公司 | Spice slow-release filter tip additive with polymer covering film as well as preparation method and application thereof |
| CN105813486A (en) * | 2013-12-31 | 2016-07-27 | 菲利普莫里斯生产公司 | Smoking article with liquid release component |
| CN106390874A (en) * | 2016-08-30 | 2017-02-15 | 湖北中烟工业有限责任公司 | Dripping pill treatment technique for improving stability of dripping pill for cigarette |
| CN109907367A (en) * | 2019-03-01 | 2019-06-21 | 江西中烟工业有限责任公司 | A kind of cigarette gel explosive beads and preparation method thereof |
| CN110506990A (en) * | 2018-05-21 | 2019-11-29 | 湖南中烟工业有限责任公司 | Flavor-increasing cooling filter stick, application and cigarette |
| CN110506991A (en) * | 2018-05-21 | 2019-11-29 | 湖南中烟工业有限责任公司 | A cooling filter rod, application and cigarette |
| CN110506992A (en) * | 2019-08-20 | 2019-11-29 | 云南南中科技有限公司 | A kind of heat melts coating device and its coating method |
| CN112143563A (en) * | 2020-08-28 | 2020-12-29 | 深圳波顿香料有限公司 | Essence for temperature-sensitive cigarette and preparation method thereof |
| KR20210011423A (en) * | 2018-05-21 | 2021-02-01 | 차이나 토바코 후난 인더스트리얼 코포레이션 리미티드 | Cooling filter rod, application and cigarette |
| CN113088389A (en) * | 2021-04-08 | 2021-07-09 | 武汉黄鹤楼香精香料有限公司 | Water-soluble dropping pill prepared from porous material and preparation method thereof |
| CN113636164A (en) * | 2021-08-13 | 2021-11-12 | 新火智造(深圳)有限公司 | Packaging method for heating non-burning cartridge |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1270999A (en) * | 1999-12-21 | 2000-10-25 | 沈阳东宇企业集团有限公司研究院 | Spice pellets and preparation process |
| US20040074507A1 (en) * | 1993-09-30 | 2004-04-22 | Macadam Kevin Gerard | Tobacco smoke filter elements |
| CN101203148A (en) * | 2005-06-21 | 2008-06-18 | 玛奈·菲尔萨公司 | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule |
| CN101766332A (en) * | 2009-12-31 | 2010-07-07 | 云南烟草科学研究院 | Pills capable of adding fragrance to cigarettes |
| CN101836764A (en) * | 2010-03-30 | 2010-09-22 | 广东神农烟科技术有限公司 | Natural plant extract microcapsule and cigarette filter containing same |
| CN101925403A (en) * | 2008-01-25 | 2010-12-22 | R.J.雷诺兹烟草公司 | Process for manufacturing breakable capsules useful in tobacco products |
| CN102068038A (en) * | 2010-12-31 | 2011-05-25 | 贵州中烟工业有限责任公司 | Method for preparing heat-sensitive moisture-retaining central line filter stick of cigarette |
-
2011
- 2011-12-25 CN CN2011104386498A patent/CN102551211A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040074507A1 (en) * | 1993-09-30 | 2004-04-22 | Macadam Kevin Gerard | Tobacco smoke filter elements |
| CN1270999A (en) * | 1999-12-21 | 2000-10-25 | 沈阳东宇企业集团有限公司研究院 | Spice pellets and preparation process |
| CN101203148A (en) * | 2005-06-21 | 2008-06-18 | 玛奈·菲尔萨公司 | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule |
| CN101925403A (en) * | 2008-01-25 | 2010-12-22 | R.J.雷诺兹烟草公司 | Process for manufacturing breakable capsules useful in tobacco products |
| CN101766332A (en) * | 2009-12-31 | 2010-07-07 | 云南烟草科学研究院 | Pills capable of adding fragrance to cigarettes |
| CN101836764A (en) * | 2010-03-30 | 2010-09-22 | 广东神农烟科技术有限公司 | Natural plant extract microcapsule and cigarette filter containing same |
| CN102068038A (en) * | 2010-12-31 | 2011-05-25 | 贵州中烟工业有限责任公司 | Method for preparing heat-sensitive moisture-retaining central line filter stick of cigarette |
Cited By (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102972865A (en) * | 2012-12-24 | 2013-03-20 | 华宝食用香精香料（上海）有限公司 | Preparation method of flavoring particles for cigarette filter tip by coating method, obtained product and use |
| CN102972865B (en) * | 2012-12-24 | 2014-04-09 | 华宝食用香精香料（上海）有限公司 | Preparation method of flavoring particles for cigarette filter tip by coating method, obtained product and use |
| CN103071459A (en) * | 2013-01-30 | 2013-05-01 | 福建中烟工业有限责任公司 | Ammonia complex composite capable of selectively reducing ammonia in smoke |
| CN103071459B (en) * | 2013-01-30 | 2015-02-11 | 福建中烟工业有限责任公司 | Ammonia complex composite capable of selectively reducing ammonia in smoke |
| CN103141939A (en) * | 2013-02-27 | 2013-06-12 | 湖北中烟工业有限责任公司 | Interception agent for reducing phenol content in cigarette smoke and filter stick provided with interception agent |
| CN105813486A (en) * | 2013-12-31 | 2016-07-27 | 菲利普莫里斯生产公司 | Smoking article with liquid release component |
| CN105105334A (en) * | 2015-07-17 | 2015-12-02 | 云南中烟工业有限责任公司 | Spice slow-release filter tip additive with polymer covering film as well as preparation method and application thereof |
| CN106390874A (en) * | 2016-08-30 | 2017-02-15 | 湖北中烟工业有限责任公司 | Dripping pill treatment technique for improving stability of dripping pill for cigarette |
| CN110506991A (en) * | 2018-05-21 | 2019-11-29 | 湖南中烟工业有限责任公司 | A cooling filter rod, application and cigarette |
| JP2021523716A (en) * | 2018-05-21 | 2021-09-09 | チャイナ タバコ フーナン インダストリアル カンパニー リミテッド | Temperature lowering filter rod, its use, and cigarette |
| KR102652799B1 (en) | 2018-05-21 | 2024-03-28 | 차이나 토바코 후난 인더스트리얼 코포레이션 리미티드 | Cooling filter rod, application and cigarette |
| CN110506991B (en) * | 2018-05-21 | 2022-08-09 | 湖南中烟工业有限责任公司 | Cooling filter rod, application and cigarette |
| JP7089066B2 (en) | 2018-05-21 | 2022-06-21 | チャイナ タバコ フーナン インダストリアル カンパニー リミテッド | Temperature lowering filter rod, its use, and cigarette |
| KR20210011423A (en) * | 2018-05-21 | 2021-02-01 | 차이나 토바코 후난 인더스트리얼 코포레이션 리미티드 | Cooling filter rod, application and cigarette |
| EP3797606A4 (en) * | 2018-05-21 | 2022-03-09 | China Tobacco Hunan Industrial Co., Ltd. | COOLING FILTER, APPLICATION AND CIGARETTE STICK |
| CN110506990A (en) * | 2018-05-21 | 2019-11-29 | 湖南中烟工业有限责任公司 | Flavor-increasing cooling filter stick, application and cigarette |
| CN109907367B (en) * | 2019-03-01 | 2021-07-16 | 江西中烟工业有限责任公司 | A kind of gel explosive beads for cigarette and preparation method thereof |
| CN109907367A (en) * | 2019-03-01 | 2019-06-21 | 江西中烟工业有限责任公司 | A kind of cigarette gel explosive beads and preparation method thereof |
| CN110506992A (en) * | 2019-08-20 | 2019-11-29 | 云南南中科技有限公司 | A kind of heat melts coating device and its coating method |
| CN112143563A (en) * | 2020-08-28 | 2020-12-29 | 深圳波顿香料有限公司 | Essence for temperature-sensitive cigarette and preparation method thereof |
| CN113088389A (en) * | 2021-04-08 | 2021-07-09 | 武汉黄鹤楼香精香料有限公司 | Water-soluble dropping pill prepared from porous material and preparation method thereof |
| CN113636164A (en) * | 2021-08-13 | 2021-11-12 | 新火智造(深圳)有限公司 | Packaging method for heating non-burning cartridge |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102551211A (en) | Preparation method for instant release type cigarette mouth rod | |
| US10264824B2 (en) | Cartridge assembly for an electronic vaping device | |
| CN113993398B (en) | Method of manufacturing smoking article comprising tubular filter and smoking article | |
| CN101390657B (en) | Slow-release menthol cigarette filter rod and its production process | |
| CN111802702B (en) | Flavor slow-release material, heating rod, cigarette holder rod, preparation method of flavor slow-release material and cigarette holder rod, and application of flavor slow-release material and cigarette holder rod in heating of non-combustible tobacco products | |
| TW201002219A (en) | Smoking article | |
| CN101296627A (en) | Menthol cigarette | |
| TW201116219A (en) | Coated impregnated porous filter plug | |
| CN109820243A (en) | Flavored gel with sustained release effect and its preparation and application in cigarettes | |
| CN105105334A (en) | Spice slow-release filter tip additive with polymer covering film as well as preparation method and application thereof | |
| CN114009826B (en) | Heating cigarette core material and preparation method thereof | |
| CN104705788A (en) | Preparing method for large-particle additive for cigarette filter | |
| CN112293790A (en) | Tobacco product, plant flavoring filter stick thereof and manufacturing method thereof | |
| TWI816402B (en) | Smoking article with reduced tobacco odor and manufacturing method thereof | |
| US20240260654A1 (en) | A consumable for use with an aerosol provision device | |
| JP2024530130A (en) | Consumables for use with aerosol delivery devices | |
| CN110754688B (en) | Fragrant bead capable of pinching and breaking hollow large-particle filter stick and preparation method thereof | |
| CN115191644B (en) | A method for preparing a tobacco flavor aerosol-generating matrix stick | |
| CN115191645B (en) | A tobacco flavor aerosol generating matrix rod and its preparation method and aerosol generating product containing the same | |
| CN117441931A (en) | Aerosol-generating matrix precursor and preparation method thereof | |
| CN107568790A (en) | Cigarette filter tip and cigarette containing zeolite perfume (or spice) pearl zeolite perfume (or spice) pearl preparation method | |
| CN115736337A (en) | Composite gel for cigarette filter stick and preparation method thereof | |
| CN221330211U (en) | A binary composite filter rod and heated cigarette | |
| KR102838798B1 (en) | Flavor sheet comprising active carbon, filter and smoking article comprising the same | |
| CN213486875U (en) | Non-burning cigarette containing recombined plant core |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20120711 |