CN102692424A - Test method for testing soaking effect of sizing in yarns based on scanning electron microscope - Google Patents
Test method for testing soaking effect of sizing in yarns based on scanning electron microscope Download PDFInfo
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- CN102692424A CN102692424A CN2012101906955A CN201210190695A CN102692424A CN 102692424 A CN102692424 A CN 102692424A CN 2012101906955 A CN2012101906955 A CN 2012101906955A CN 201210190695 A CN201210190695 A CN 201210190695A CN 102692424 A CN102692424 A CN 102692424A
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Abstract
本发明公开的一种基于扫描电镜测试浆液在纱线中浸透效果的测试方法，按以下步骤实施，取一块橡胶块并将其裁剪成立方体；将待测浆纱穿入缝纫针的针鼻内；将穿有待测浆纱的缝纫针垂直刺入橡胶块，使缝纫针整个穿过橡胶块至待测浆纱穿进橡胶块内；用钳口将橡胶块夹持住；用锋利的刀片将夹持在两活动式钳口之间橡胶块上的待测浆纱的尾端切割平整；松开钳口取下橡胶块，并将其固定在载玻片上；对载玻片上的固定好的浆纱进行喷金处理后得到浆纱切片；将制成的浆纱切片放到扫描电子显微镜下行拍摄，将拍摄好的浆纱照片储存于计算机。本发明方法能清晰的拍摄浆液在纱线中的浸透形态，用于测试浆液在纱线中的浸透情况。
A method for testing the penetration effect of sizing agent in yarn based on a scanning electron microscope disclosed in the present invention is carried out according to the following steps: take a piece of rubber and cut it into a cube; put the sizing yarn to be tested into the needle nose of a sewing needle ;Pierce the sewing needle with the sizing to be tested into the rubber block vertically, so that the sewing needle passes through the rubber block until the sizing to be tested penetrates into the rubber block; clamp the rubber block with the jaws; use a sharp blade Cut the end of the sizing yarn clamped on the rubber block between the two movable jaws flat; loosen the jaws to take off the rubber block and fix it on the glass slide; After the sizing is sprayed with gold, the sizing slices are obtained; the sizing slices are taken under a scanning electron microscope, and the sizing photos taken are stored in the computer. The method of the invention can clearly photograph the state of the size liquid soaked in the yarn, and is used for testing the state of the size liquid soaked in the yarn.
Description
Technical field
The invention belongs to textile material and quality of textile products control technology field, relate to a kind of method of testing of in yarn, soaking into effect based on the sem test slurries.
Background technology
Usually carrying out often need utilizing microscope when sizing quality analyzes, infiltration situation through sizing sections observation slurries and filoplume form etc.When the observed sizing form of statement, usually adopt the method for Freehandhand-drawing or learn the effect that slurries soak into, but all there was certain limitation in these two kinds of methods in the past in the method that the microscopically with digital filming function is taken pictures.
The degree of accuracy of wherein Freehandhand-drawing method is very poor, tends to produce than big-difference because of illustrator individual's sensation and technical merit; And the method that adopts microscope with digital filming function to take pictures, the primary problem that solves is the manufacture craft of sizing section, has light transmission preferably because the principle of microscope photographing is the section of requirement sizing; So the sizing section must be very thin; Make the sizing section so and often have very big difficulty, simultaneously, adopt microscope to observe the soak into situation of slurries in yarn; Need to use iodine liquid; Influenced whole test accuracy to a certain extent, iodine liquid does not have the colour developing effect to other outer slurry of starch in addition, can't use microscope to observe.
Summary of the invention
The purpose of this invention is to provide and a kind ofly in yarn, soak into the method for testing of effect, can shoot slurries clearly and in yarn, soak into form, be used for testing the soak into situation of slurries at yarn based on the sem test slurries.
The technical scheme that the present invention adopted is, a kind ofly in yarn, soaks into the method for testing of effect based on the sem test slurries, specifically carries out according to the following steps:
Step 1: prepare to cut sizing section to be measured
1) gets a block rubber and block rubber is cut into cubic shaped;
Get sizing to be measured; Fineness according to sizing to be measured is selected sewing needle; The diameter of sewing needle for
wherein Ntex be the special number of sizing to be measured, the value of δ is 0.78 ~ 0.9;
Cutting sizing to be measured, the sizing to be measured that cutting is got off penetrates in the eye of a needle of sewing needle;
2) the sewing needle needle point that is installed with sizing to be measured in the eye of a needle is vertically thrust 1) in the upper surface of the block rubber processed; The pull sewing needle makes sewing needle carry the upper and lower surfaces that sizing to be measured passes block rubber; Because block rubber has curable grip to the sizing to be measured that penetrates wherein; The sizing to be measured that gets in the block rubber is clamped in block rubber, gets rid of the sewing needle of traction sizing to be measured;
Step 2: cut sizing section to be measured
1) with one group of movable jaw the block rubber two ends that are installed with sizing to be measured in the step 1 is fixed, prevented that block rubber from producing slippage;
2) get the sharp blade of a slice, the tail end of sizing to be measured that will pass the block rubber upper surface with blade is along block rubber upper surface flat cut, and removes the sizing that cuts with blade;
Step 3: make sizing section to be measured
1) unclamp one group of movable jaw, the clamping of taking off step 2 processing has the block rubber of sizing to be measured;
2) get microslide, with adhesive tape with 1) in clamping have the block rubber two ends of sizing to be measured to be fixed on the microslide, accomplish the preliminary making of sizing to be measured section;
3) with 2) in the sizing to be measured section that tentatively is made into be placed on and spray platinum under 10mA ~ 20mA electric current and handle, the time of spray platinum is 160 seconds ~ 200 seconds, promptly accomplishes the making of sizing section to be measured after platinum to be painted is accomplished, and obtains sizing section to be measured;
Step 4: the employing ESEM is taken the sizing photo and photo is stored in the computing machine
The sizing section to be measured of 1) step 3 being processed is put under the scanning electron microscope, the enlargement factor of adjustment scanning electron microscope, and enlargement factor is generally between 200 ~ 4000 times;
2) configure enlargement factor after, with scanning electron microscope to sizing to be measured section observe and take pictures, will take the sizing photo to be measured of getting well at last and be stored in computing machine and get final product.
Characteristic of the present invention also is,
The block rubber of making in the step 1 is a cube, is of a size of 10 * 10 * 2mm
3
The invention has the beneficial effects as follows,
The present invention characterizes the soak into situation of slurries in yarn with the traditional hand plotting method and is converted into and adopts ESEM directly to take the sizing cross-section photograph to obtain slurries soaking in yarn; Because the range of choice of ESEM enlargement factor is bigger; When taking, can choose flexibly according to the actual requirements and need amplification multiple; The quantity of taking pictures is also unrestricted; The captured sizing section photo that goes out is clear accurately to have improved sizing test accuracy and testing efficiency, for the detection of sizing quality provides a kind of more convenient, method more accurately.
Description of drawings
Fig. 1 is a kind of electromicroscopic photograph that in yarn, soaks into the textile raw yarn of 14.5tex that the method for testing of effect takes based on the sem test slurries of the present invention;
Fig. 2 is a kind of electromicroscopic photograph that in yarn, soaks into the textile sizing of 14.5tex that the method for testing of effect takes based on the sem test slurries of the present invention.
Fig. 3 is a kind of electromicroscopic photograph that in yarn, soaks into the textile raw yarn of 18.2tex that the method for testing of effect takes based on the sem test slurries of the present invention.
Fig. 4 is a kind of electromicroscopic photograph that in yarn, soaks into the textile sizing of 18.2tex that the method for testing of effect takes based on the sem test slurries of the present invention.
Fig. 5 is a kind of electromicroscopic photograph that in yarn, soaks into the 13tex polyester-cotton blend sizing that the method for testing of effect takes based on the sem test slurries of the present invention.
Embodiment
Below in conjunction with accompanying drawing and embodiment the present invention is elaborated.
A kind ofly in yarn, soak into the method for testing of effect, specifically carry out according to the following steps based on the sem test slurries:
Step 1: prepare to cut sizing section to be measured
1) gets a block rubber and block rubber is cut into cubic shaped;
Get sizing to be measured; Fineness according to sizing to be measured is selected sewing needle; The diameter of sewing needle for
wherein Ntex be the special number of sizing to be measured, the value of δ is 0.78 ~ 0.9;
Cutting sizing to be measured, the sizing to be measured that cutting is got off penetrates in the eye of a needle of sewing needle;
2) the sewing needle needle point that is installed with sizing to be measured in the eye of a needle is vertically thrust 1) in the upper surface of the block rubber processed; The pull sewing needle makes sewing needle carry the upper and lower surfaces that sizing to be measured passes block rubber; Because block rubber has curable grip to the sizing to be measured that penetrates wherein; The sizing to be measured that gets in the block rubber is clamped in block rubber, gets rid of the sewing needle of traction sizing to be measured;
Step 2: cut sizing section to be measured
1) with one group of movable jaw the block rubber two ends that are installed with sizing to be measured in the step 1 is fixed, prevented that block rubber from producing slippage;
2) get the sharp blade of a slice, the tail end of sizing to be measured that will pass the block rubber upper surface with blade is along block rubber upper surface flat cut, and removes the sizing that cuts with blade;
Step 3: make sizing section to be measured
1) unclamp one group of movable jaw, the clamping of taking off step 2 processing has the block rubber of sizing to be measured;
2) get microslide, with adhesive tape with 1) in clamping have the block rubber two ends of sizing to be measured to be fixed on the microslide, accomplish the preliminary making of sizing to be measured section;
3) with 2) in the sizing to be measured section that tentatively is made into be placed on and spray platinum under 10mA ~ 20mA electric current and handle, the time of spray platinum is 160 seconds ~ 200 seconds, promptly accomplishes the making of sizing section to be measured after platinum to be painted is accomplished, and obtains sizing section to be measured;
Step 4: the employing ESEM is taken the sizing photo and photo is stored in the computing machine
The sizing section to be measured of 1) step 3 being processed is put under the scanning electron microscope, the enlargement factor of adjustment scanning electron microscope, and enlargement factor is generally between 200 ~ 4000 times;
2) configure enlargement factor after, with scanning electron microscope to sizing to be measured section observe and take pictures, will take the sizing photo to be measured of getting well at last and be stored in computing machine and get final product.
The captured sizing of the inventive method section picture picture is clear, helps improving the precision and the efficient of sizing test, for the detection of sizing quality provides a kind of new tool.Adopt the inventive method test slurries in yarn, to soak into effect, the enlargement factor adjustable extent is wide.
The operating procedure of the inventive method is simple; The requirement of the sizing section compound scan Electronic Speculum that cuts; Adopt ESEM the sizing serial section is observed and to be taken pictures, generally be impregnated between the fiber in the yarn when slurries, will make take place between the fiber mutual bonding; Because sizing does not have electric conductivity, increase electric conductivity so will handle, after the sizing slice surface carries out the metal spraying processing to sizing section carrying out metal spraying; Make the sizing surface that one deck conductive layer arranged; Through the section of the sizing behind the metal spraying, the section morphology of sizing just can taken and demonstrate to ESEM, through connecting computing machine; Can on the display of counter, observe slurries and whether be impregnated between the fiber, can judge the soak into situation of slurries in yarn thus.
Embodiment 1
Get a block rubber and block rubber is cut into cubic shaped; It is in the eye of a needle of 0.15mm sewing needle that the textile sizing of the 14.5tex that cutting is got off penetrates a diameter; The sewing needle needle point that is installed with sizing in the eye of a needle is vertically thrust in the upper surface of block rubber; Block rubber has curable grip to the sizing that penetrates wherein; Make sizing clamped in block rubber; Just do not spur and can not produce slippage, the pull sewing needle makes sewing needle carry the upper and lower surfaces that textile sizing passes block rubber; The block rubber two ends that will have sizing with one group of movable jaw are fixed, and guarantee that block rubber can not produce slippage; Have one's hair trimmed along the tail end that jaw will be clamped in the textile sizing on the block rubber between two jaws with sharp blade; Unclamp one group of movable jaw, take off the block rubber that has textile sizing that cuts, will cut the block rubber two ends that have textile sizing of getting off with adhesive tape and be fixed on the microslide; The section of the sizing that is made into is placed on sprays platinum under the 15mA electric current and handle, the time of spray platinum is 180 seconds, obtains the sizing section; The sizing section of processing is put under the scanning electron microscope; Adjustment scanning electron microscope enlargement factor is 4000 times; With scanning electron microscope to sizing to be measured section observe and take pictures, will take the sizing photo to be measured of getting well at last and be stored in computing machine and get final product.
Adopt above-mentioned steps to take electromicroscopic photograph the textile raw yarn of 14.5tex, result such as Fig. 1, shown in Figure 2, the space is big between the raw yarn cross-section fibers, has soaked into slurries between the sizing cross-section fibers.
Embodiment 2
Get a block rubber and block rubber is cut into cubic shaped; It is in the eye of a needle of 0.17mm sewing needle that the textile sizing of the 18.2tex that cutting is got off penetrates a diameter; The sewing needle needle point that is installed with sizing in the eye of a needle is vertically thrust in the upper surface of block rubber; Block rubber has curable grip to the sizing that penetrates wherein; Make sizing clamped in block rubber; Just do not spur and can not produce slippage, the pull sewing needle makes sewing needle carry the upper and lower surfaces that textile sizing passes block rubber; The block rubber two ends that will have sizing with one group of movable jaw are fixed, and guarantee that block rubber can not produce slippage; Have one's hair trimmed along the tail end that jaw will be clamped in the textile sizing on the block rubber between two jaws with sharp blade; Unclamp one group of movable jaw, take off the block rubber that has textile sizing that cuts, will cut the block rubber two ends that have textile sizing of getting off with adhesive tape and be fixed on the microslide; The section of the sizing that is made into is placed on sprays platinum under the 10mA electric current and handle, the time of spray platinum is 160 seconds, obtains the sizing section; The sizing section of processing is put under the scanning electron microscope; Adjustment scanning electron microscope enlargement factor is 2000 times; With scanning electron microscope to sizing to be measured section observe and take pictures, will take the sizing photo to be measured of getting well at last and be stored in computing machine and get final product.
Textile raw yarn with 18.2tex adopts above-mentioned steps to take electromicroscopic photograph again, result such as Fig. 3, shown in Figure 4, and the space is big between the raw yarn cross-section fibers, has slurries to soak between the sizing cross-section fibers.
Embodiment 3
Get a block rubber and block rubber is cut into cubic shaped; It is in the eye of a needle of 0.14mm sewing needle that the polyester-cotton blend sizing of the 13ex that cutting is got off penetrates a diameter; The sewing needle needle point that is installed with sizing in the eye of a needle is vertically thrust in the upper surface of block rubber; Block rubber has curable grip to the sizing that penetrates wherein; Make sizing clamped in block rubber; Just do not spur and can not produce slippage, the pull sewing needle makes sewing needle carry the upper and lower surfaces that the polyester-cotton blend sizing passes block rubber; The block rubber two ends that will have sizing with one group of movable jaw are fixed, and guarantee that block rubber can not produce slippage; Have one's hair trimmed along the tail end that jaw will be clamped in the polyester-cotton blend sizing on the block rubber between two jaws with sharp blade; Unclamp one group of movable jaw, take off the block rubber that has the polyester-cotton blend sizing that cuts, will cut the block rubber two ends that have the polyester-cotton blend sizing of getting off with adhesive tape and be fixed on the microslide; The section of the sizing that is made into is placed on sprays platinum under the 10mA electric current and handle, the time of spray platinum is 160 seconds, obtains the sizing section; The sizing section of processing is put under the scanning electron microscope; Adjustment scanning electron microscope enlargement factor is 4000 times; With scanning electron microscope to sizing to be measured section observe and take pictures, will take the sizing photo to be measured of getting well at last and be stored in computing machine and get final product.
Adopt above-mentioned steps to take electromicroscopic photograph on the polyester-cotton blend sizing of 13tex, the result is as shown in Figure 5, has slurries to soak between the sizing cross-section fibers.
Adopt method provided by the invention, the sizing cross section that obtains is very clear, and the soak into situation of slurries in yarn comes into plain view.Compare with classic method, the soak into situation of slurries in yarn is more clear, and the microsection manufacture method is easy.
Claims (2)
1. one kind soaks into the method for testing of effect based on the sem test slurries in yarn, it is characterized in that, specifically carries out according to the following steps:
Step 1: prepare to cut sizing section to be measured
1) gets a block rubber and block rubber is cut into cubic shaped;
Get sizing to be measured; Fineness according to sizing to be measured is selected sewing needle; The diameter of sewing needle for
wherein Ntex be the special number of sizing to be measured, the value of δ is 0.78 ~ 0.9;
Cutting sizing to be measured, the sizing to be measured that cutting is got off penetrates in the eye of a needle of sewing needle;
2) the sewing needle needle point that is installed with sizing to be measured in the eye of a needle is vertically thrust 1) in the upper surface of the block rubber processed; The pull sewing needle makes sewing needle carry the upper and lower surfaces that sizing to be measured passes block rubber; Because block rubber has curable grip to the sizing to be measured that penetrates wherein; The sizing to be measured that gets in the block rubber is clamped in block rubber, gets rid of the sewing needle of traction sizing to be measured;
Step 2: cut sizing section to be measured
1) with one group of movable jaw the block rubber two ends that are installed with sizing to be measured in the step 1 is fixed, prevented that block rubber from producing slippage;
2) get the sharp blade of a slice, the tail end of sizing to be measured that will pass the block rubber upper surface with blade is along block rubber upper surface flat cut, and removes the sizing that cuts with blade;
Step 3: make sizing section to be measured
1) unclamp one group of movable jaw, the clamping of taking off step 2 processing has the block rubber of sizing to be measured;
2) get microslide, with adhesive tape with 1) in clamping have the block rubber two ends of sizing to be measured to be fixed on the microslide, accomplish the preliminary making of sizing to be measured section;
3) with 2) in the sizing to be measured section that tentatively is made into be placed on and spray platinum under 10mA ~ 20mA electric current and handle, the time of spray platinum is 160 seconds ~ 200 seconds, promptly accomplishes the making of sizing section to be measured after platinum to be painted is accomplished, and obtains sizing section to be measured;
Step 4: the employing ESEM is taken the sizing photo and photo is stored in the computing machine
The sizing section to be measured of 1) step 3 being processed is put under the scanning electron microscope, the enlargement factor of adjustment scanning electron microscope, and enlargement factor is generally between 200 ~ 4000 times;
2) configure enlargement factor after, with scanning electron microscope to sizing to be measured section observe and take pictures, will take the sizing photo to be measured of getting well at last and be stored in computing machine and get final product.
2. according to claim 1ly a kind ofly in yarn, soak into the method for testing of effect, it is characterized in that the block rubber of making in the said step 1 is a cube, is of a size of 10 * 10 * 2mm based on the sem test slurries
3
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106932322A (en) * | 2015-12-31 | 2017-07-07 | 立邦涂料（中国）有限公司 | A kind of interior wall tests the method and apparatus of contaminated resistance |
| CN110426323A (en) * | 2019-08-30 | 2019-11-08 | 浙江大学 | A kind of chitosan slurry slurries impregnability, coating property measuring method |
| CN113155676A (en) * | 2021-03-22 | 2021-07-23 | 宁波亚洲浆纸业有限公司 | Method for testing paper surface sizing effect |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20010030287A1 (en) * | 2000-02-24 | 2001-10-18 | Jeol Ltd. | Method of observing image and scanning electron microscope |
| US20020134935A1 (en) * | 2001-03-26 | 2002-09-26 | Ming-Chung Liang | Inspection method to check contact hole open after contact etching |
| US6911421B2 (en) * | 2002-11-01 | 2005-06-28 | Nicca Usa, Inc. | Surfactant blends for removing oligomer deposits from polyester fibers and polyester processing equipment |
| US20070032805A1 (en) * | 2005-08-03 | 2007-02-08 | Sofradim Production | Oxydized cellulose prosthesis |
| CN102302900A (en) * | 2011-08-26 | 2012-01-04 | 国家海洋局天津海水淡化与综合利用研究所 | Method for detecting microstructure of reverse osmosis membrane separating layer |
-
2012
- 2012-06-11 CN CN201210190695.5A patent/CN102692424B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20010030287A1 (en) * | 2000-02-24 | 2001-10-18 | Jeol Ltd. | Method of observing image and scanning electron microscope |
| US20020134935A1 (en) * | 2001-03-26 | 2002-09-26 | Ming-Chung Liang | Inspection method to check contact hole open after contact etching |
| US6911421B2 (en) * | 2002-11-01 | 2005-06-28 | Nicca Usa, Inc. | Surfactant blends for removing oligomer deposits from polyester fibers and polyester processing equipment |
| US20070032805A1 (en) * | 2005-08-03 | 2007-02-08 | Sofradim Production | Oxydized cellulose prosthesis |
| CN102302900A (en) * | 2011-08-26 | 2012-01-04 | 国家海洋局天津海水淡化与综合利用研究所 | Method for detecting microstructure of reverse osmosis membrane separating layer |
Non-Patent Citations (4)
| Title |
|---|
| 仲岑然: "基于计算机图像处理的浆液浸透性测试", 《棉纺织技术》, vol. 38, no. 1, 31 January 2010 (2010-01-31), pages 41 - 43 * |
| 徐明根: "水泥基渗透结晶型防水材料渗透深度扫描电镜和能谱分析", 《铁道科学与工程学报》, vol. 2, no. 3, 30 June 2005 (2005-06-30), pages 67 - 70 * |
| 杨元: "浆纱浆液渗透及被覆测试方法的比较", 《上海纺织科技》, vol. 33, no. 7, 31 July 2005 (2005-07-31), pages 60 - 64 * |
| 武海良等: "应用光学显微镜制作浆纱数码照片的方法", 《棉纺织技术》, vol. 34, no. 12, 31 December 2006 (2006-12-31), pages 747 - 749 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106932322A (en) * | 2015-12-31 | 2017-07-07 | 立邦涂料（中国）有限公司 | A kind of interior wall tests the method and apparatus of contaminated resistance |
| CN110426323A (en) * | 2019-08-30 | 2019-11-08 | 浙江大学 | A kind of chitosan slurry slurries impregnability, coating property measuring method |
| CN110426323B (en) * | 2019-08-30 | 2020-10-20 | 浙江大学 | A kind of chitosan slurry slurry permeability and coating method |
| CN113155676A (en) * | 2021-03-22 | 2021-07-23 | 宁波亚洲浆纸业有限公司 | Method for testing paper surface sizing effect |
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