CN102773323B - Strong force rotary pressing molding method of nanocrystalline/superfine crystal carbon steel cylindrical piece - Google Patents
Strong force rotary pressing molding method of nanocrystalline/superfine crystal carbon steel cylindrical piece Download PDFInfo
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Abstract
本发明公开了一种纳米晶/超细晶碳钢筒形件的强力旋压成形方法,该方法根据金属筒形零件的尺寸,按照变形过程中材料体积不变原理和工件产生85~90%的总厚度减薄率的要求,预制无焊缝筒形或杯形毛坯;然后将毛坯套装在芯模上,经过多道次错距旋压使其壁部厚度减薄率达到60~70%;再将工件放入惰性气体保护炉中进行再结晶处理;最后将工件再次套装在芯模上,经过多道次错距旋压变形使总的壁部厚度减薄率达到85~90%。本发明针对低碳钢薄壁筒形零件不仅具有高精度外形尺寸,还具有整体而非表面的超细晶/纳米化的微观晶粒组织,因此具有良好的整体机械性能。
The invention discloses a powerful spinning forming method for a nanocrystalline/ultrafine-grained carbon steel cylindrical part. The method is based on the size of the metal cylindrical part, the principle of constant material volume in the deformation process, and 85-90% of workpiece production According to the requirements of the total thickness reduction rate, prefabricated non-welded cylindrical or cup-shaped blanks; then the blanks are set on the mandrel, and the wall thickness reduction rate reaches 60-70% after multiple passes of staggered spinning ; Then put the workpiece into an inert gas protection furnace for recrystallization treatment; finally, put the workpiece on the mandrel again, and through multi-pass spinning deformation, the total wall thickness reduction rate reaches 85-90%. The invention aims at low-carbon steel thin-walled cylindrical parts not only having high-precision external dimensions, but also having ultrafine-grained/nano-sized microscopic grain structures on the whole rather than on the surface, thus having good overall mechanical properties.
Description
技术领域 technical field
本发明涉及一种纳米/超细晶材料,特别是涉及一种纳米晶/超细晶碳钢筒形件的强力旋压成形方法,属于金属材料的塑性成形领域。The invention relates to a nano/ultra-fine crystal material, in particular to a powerful spinning forming method for a nano-crystal/ultra-fine crystal carbon steel cylinder, belonging to the field of plastic forming of metal materials.
背景技术 Background technique
超细晶/纳米材料是纳米科学技术的一个重要的发展方向。超细晶材料的晶粒特征维度尺寸在微米量级以下(100nm~1000nm),纳米材料的晶粒特征维度尺寸在纳米量级(1nm~100nm)。由于极细的晶粒,大量处于晶界和晶粒内缺陷的中心原子以及其本身具有的量子尺寸效应、小尺寸效应、表面效应和宏观量子隧道效应等,超细晶/纳米材料与同组成的常规微米晶体材料相比,在催化、光学、磁性、力学等方面具有许多奇异的性能,因而成为材料科学和凝聚态物理领域中的研究热点,在机械零件加工中也逐渐得到重视和推广应用。Ultrafine crystal/nano material is an important development direction of nano science and technology. The characteristic dimension of grains of ultra-fine-grained materials is below the micron level (100nm to 1000nm), and the characteristic dimension of grains of nanomaterials is on the order of nanometers (1nm to 100nm). Due to the extremely fine grains, a large number of central atoms located in the grain boundaries and defects in the grains, and its own quantum size effect, small size effect, surface effect and macroscopic quantum tunneling effect, ultrafine grain/nanomaterials and the same composition Compared with conventional micron crystal materials, it has many exotic properties in catalysis, optics, magnetism, mechanics, etc., so it has become a research hotspot in the field of materials science and condensed matter physics, and it has gradually been paid attention to and popularized in the processing of mechanical parts. .
纳米晶/超细晶材料的制备方法,主要是制备具有极小晶粒尺寸的块体材料,再用这种材料加工所需要的零件。这种块体材料的制备一般受技术限制,只能得到尺寸较小的坯料,因此也只加工小尺寸的零件。The preparation method of nanocrystalline/ultrafine crystalline materials is mainly to prepare bulk materials with extremely small grain size, and then use this material to process the required parts. The preparation of such bulk materials is generally limited by technology, and only small-sized blanks can be obtained, so only small-sized parts can be processed.
为了解决大尺寸零件的晶粒细化问题,结合机械零件在实际工作时都是零件表面比较容易受到破坏的特点,形成了表面超细晶/纳米化技术,即采用常规方法先加工出零件,再只针对零件表面进行超细晶/纳米化处理,而零件的大部分体积范围之内的材料晶粒仍然处于常规的微米量级以上。In order to solve the problem of grain refinement of large-sized parts, combined with the fact that the surface of mechanical parts is relatively easy to be damaged during actual work, the surface ultra-fine grain/nanoization technology has been formed, that is, the parts are processed first by conventional methods. Then only the ultra-fine grain/nano treatment is performed on the surface of the part, and the material grains within most of the volume of the part are still above the conventional micron level.
对于实际工程中大量使用的低碳钢薄壁筒形金属零件,由于厚度很小,零件内外表面及材料内部的服役环境非常接近,表面纳米化已经无法满足使用要求。如果零件尺寸较大而又希望得到具有超细晶/纳米晶粒的微观组织,则既不能采用纳米块体材料来加工尺寸较大的零件,又不能对常规方法加工出来的零件仅仅进行表面超细晶/钠米化处理。For the low-carbon steel thin-walled cylindrical metal parts widely used in actual engineering, due to the small thickness, the service environment of the inner and outer surfaces of the parts and the interior of the material is very close, and the surface nanotechnology can no longer meet the use requirements. If the size of the part is large and it is desired to obtain a microstructure with ultra-fine grains/nano-grains, nano-bulk materials cannot be used to process larger parts, and the parts processed by conventional methods cannot only be superficially superficial. Fine-grained/nano-sized treatment.
发明内容 Contents of the invention
为了克服现有技术的不足,本发明提供一种既能得到整体纳米晶/超细晶粒的微观组织结构,又能直接加工出符合产品外形要求的较大尺寸的碳钢薄壁筒形零件的方法。In order to overcome the deficiencies of the prior art, the present invention provides a microstructure that can not only obtain the overall nanocrystalline/ultrafine grain, but also directly process a larger-sized carbon steel thin-walled cylindrical part that meets the requirements of the product shape. Methods.
本发明的目的通过如下技术方案实现:The purpose of the present invention is achieved through the following technical solutions:
一种纳米晶/超细晶碳钢筒形件的强力旋压成形方法,包括如下步骤:A method for powerful spinning forming of nanocrystalline/ultrafine-grained carbon steel cylindrical parts, comprising the steps of:
(1)根据金属筒形零件壁部厚度和零件长度,按照材料体积不变原理和变形过程中碳钢筒形件壁部产生85~90%的总厚度减薄率的要求,预制无焊缝筒形或杯形毛坯;所述碳钢筒形零件的材料为低碳钢;(1) According to the wall thickness and part length of metal cylindrical parts, according to the principle of constant material volume and the requirement of a total thickness reduction rate of 85-90% in the wall of carbon steel cylindrical parts during the deformation process, prefabricated without welds Cylindrical or cup-shaped blank; the material of the carbon steel cylindrical part is low carbon steel;
(2)将毛坯套装在芯模上,经过多道次三旋轮错距旋压变形,使其壁厚减薄率达到60~70%;控制三旋轮的轴向错距量为1.5~2.5mm,径向错距量为0.1~0.3mm;(2) Put the blank on the mandrel, and undergo multi-pass three-rotor stagger spinning deformation, so that the wall thickness reduction rate reaches 60-70%; control the axial stagger of the three-rotor wheel to 1.5- 2.5mm, the radial misalignment is 0.1~0.3mm;
(3)将工件放入温度为400~450℃的惰性气体保护炉中进行加热升温至再结晶保温温度550~600℃,保温0.8~1小时,然后出炉冷却;(3) Put the workpiece into an inert gas protection furnace with a temperature of 400-450°C to heat up to the recrystallization holding temperature of 550-600°C, keep it warm for 0.8-1 hour, and then take it out of the furnace to cool;
(4)将工件再次套装在旋压芯模上,经过多道次三旋轮错距旋压变形使总的壁厚减薄率达到85~90%,再修边以满足零件尺寸要求。(4) Set the workpiece on the spinning mandrel again, and through multi-pass three-roller staggered spinning deformation, the total wall thickness reduction rate reaches 85-90%, and then trims to meet the size requirements of the part.
为进一步实现本发明的目的,设计毛坯尺寸时,在零件长度方向增加30~50mm的修边余量。In order to further realize the purpose of the present invention, when designing the size of the blank, a trimming allowance of 30-50 mm is added in the length direction of the part.
所述碳钢的含碳量优选为0.1%-0.25%。The carbon content of the carbon steel is preferably 0.1%-0.25%.
所述步骤(3)的冷却优选为用水进行冷却。The cooling in step (3) is preferably cooling with water.
所述三旋轮错距旋压变形是使用框架旋轮座式旋压机进行旋压成形,标号分别为1、2、3的三个旋轮呈120°对称分布在框架的中心孔周围,该框架的中心有一通孔,框架通孔的中心点与机床主轴位于同一水平线。标号分别为1、2、3的三个旋轮离中心点的距离分别为R1、R2、R3,标号分别为1、2的旋轮之间的径向错距e12=R1-R2,标号分别为2、3的旋轮之间的径向错距e23=R2-R3;三个旋轮的安装位置在机床主轴方向相互错开,S12为标号为1、2的旋轮之间的轴向错距,S23为标号为2、3旋轮之间的轴向错距。The three-roller staggered-pitch spinning deformation is formed by using a frame-roller-seat spinning machine, and the three spinners with numbers 1, 2, and 3 are distributed symmetrically at 120° around the center hole of the frame. There is a through hole in the center of the frame, and the center point of the frame through hole is located on the same horizontal line as the main shaft of the machine tool. The distances from the center point of the three rotary wheels with labels 1, 2, and 3 are R1, R2, and R3 respectively, and the radial stagger distance between the rotary wheels with labels 1 and 2 respectively is e12=R1-R2, and the labels are respectively The radial stagger distance between the rotary wheels 2 and 3 is e23=R2-R3; the installation positions of the three rotary wheels are staggered in the direction of the machine tool spindle, and S12 is the axial stagger between the rotary wheels labeled 1 and 2. S23 is the axial stagger distance between the 2 and 3 rollers.
步骤(3)的再结晶说明:在步骤(3)的加热和保温过程中,由于工件经过了塑性变形,在合适的温度和保温时间下,在变形金属的显微组织中,会产生无应变的新晶粒──再结晶核心。新晶粒不断长大,直至原来的变形组织完全消失,金属的性能也发生显著变化,这一过程称为再结晶(区别于液体凝固成固体的结晶过程)。再结晶的温度不是固定的,受很多因素影响,主要是材料的化学成分、变形程度等,一般情况下再结晶温度大于材料熔点的0.4倍,准确的再结晶温度主要依靠试验获得。Recrystallization description of step (3): During the heating and holding process of step (3), due to the plastic deformation of the workpiece, under the appropriate temperature and holding time, there will be no strain in the microstructure of the deformed metal. New grains of ─ recrystallization core. The new grains continue to grow until the original deformed structure disappears completely, and the properties of the metal also change significantly. This process is called recrystallization (different from the crystallization process in which liquid solidifies into a solid). The recrystallization temperature is not fixed, and is affected by many factors, mainly the chemical composition of the material, the degree of deformation, etc. Generally, the recrystallization temperature is greater than 0.4 times the melting point of the material, and the accurate recrystallization temperature mainly depends on experiments.
相对于现有技术,本发明具有如下优点和有益效果:Compared with the prior art, the present invention has the following advantages and beneficial effects:
1、本发明可以得到贯穿材料整体而非表面的超细晶/纳米材料微观组织;1. The present invention can obtain the microstructure of ultra-fine crystal/nano material that runs through the whole material instead of the surface;
2、本发明可以得到具有超细晶/纳米材料的实用零件,而不是材料的坯料;2. The present invention can obtain practical parts with ultra-fine crystal/nano-materials instead of blanks of materials;
3、本发明可以得到具有大规格尺寸的超细晶/纳米材料零件;3. The present invention can obtain ultra-fine crystal/nano material parts with large size;
4、本发明与常规旋压得到的材料微观组织相比,所得到的超细晶/纳米微观组织具有更好的力学、化学等方面的性能。4. Compared with the material microstructure obtained by conventional spinning, the ultra-fine grain/nano microstructure obtained by the present invention has better mechanical and chemical properties.
附图说明 Description of drawings
图1是本发明一种金属薄壁筒形零件的结构示意图。Fig. 1 is a structural schematic diagram of a metal thin-walled cylindrical part of the present invention.
图2是本发明所采用的框架旋轮座示意图。Fig. 2 is a schematic view of the frame wheel seat used in the present invention.
图3是图1在A方向投影时,旋轮的位置示意图。Fig. 3 is a schematic diagram of the position of the rotary wheel when Fig. 1 is projected in the direction A.
图4是本发明所采用的管形毛坯图。Fig. 4 is a diagram of a tubular blank used in the present invention.
图5是本发明所采用的杯形毛坯图。Fig. 5 is a diagram of a cup blank used in the present invention.
图6是管形毛坯错距旋压正旋过程示意图。Fig. 6 is a schematic diagram of the normal spinning process of the staggered spinning of the tubular blank.
图7是杯形毛坯错中旋压反旋过程示意图。Fig. 7 is a schematic diagram of the cup-shaped rough blank center spinning reverse spinning process.
图8是本发明成形方法的流程图。Fig. 8 is a flowchart of the forming method of the present invention.
图9是本发明所采用的毛坯材料20钢的原始晶相照片。Fig. 9 is a photograph of the original crystal phase of the rough material 20 steel used in the present invention.
图10是本发明再结晶处理的温度变化曲线。Fig. 10 is a temperature change curve of the recrystallization treatment of the present invention.
图11是本发明20钢旋压成形及再结晶处理后的透射电镜照片。Fig. 11 is a transmission electron microscope photo of 20 steel of the present invention after spinning forming and recrystallization treatment.
具体实施方式 Detailed ways
下面结合附图和实施例对本发明作进一步的说明,但是本发明要求保护的范围并不局限于实施例表述的范围。The present invention will be further described below in conjunction with the drawings and examples, but the protection scope of the present invention is not limited to the range expressed in the examples.
本发明所要加工的零件外形如图1所示,为低碳钢金属薄壁筒形件。采用框架旋轮座式旋压机进行旋压成形,图2所示为框架旋轮座,其中标号分别为1、2、3的三个旋轮呈120°对称分布在框架0的中心孔周围,该框架的中心有一通孔,用于穿过旋压芯模及工件,因此框架通孔的中心Z点与机床主轴位于同一水平线。标号分别为1、2、3的三个旋轮离中心Z点的距离分别为R1、R2、R3,该距离可以根据需要进行调整从而获得旋轮的径向错距,其中标号分别为1、2的旋轮之间的径向错距e12=R1-R2,标号分别为2、3的旋轮之间的径向错距e23=R2-R3;图3所示为三个旋轮的安装位置在机床主轴方向相互错开的示意图,S12为标号为1、2的旋轮之间的轴向错距,S23为标号为2、3旋轮之间的轴向错距,轴向错距量可以根据需要进行调整。The profile of the part to be processed in the present invention is shown in Figure 1, which is a low-carbon steel metal thin-walled cylindrical part. The frame spinning machine is used for spinning forming. Figure 2 shows the frame spinning wheel seat, in which the three spinning wheels labeled 1, 2, and 3 are distributed symmetrically at 120° around the center hole of frame 0. , There is a through hole in the center of the frame, which is used to pass through the spinning mandrel and the workpiece, so the center Z point of the frame through hole is on the same level as the machine tool spindle. The distances from the center Z point of the three rotary wheels with labels 1, 2, and 3 are R1, R2, and R3 respectively. The distances can be adjusted according to the needs to obtain the radial offset of the rotary wheels, where the labels are 1, The radial stagger distance e 12 between the rollers of 2 = R1-R2, the radial stagger distance between the rollers marked 2 and 3 respectively e 23 = R2-R3; Figure 3 shows three rollers Schematic diagram of the staggered installation positions in the direction of the main shaft of the machine tool. S 12 is the axial stagger distance between the rollers marked 1 and 2, and S 23 is the axial stagger distance between the rollers marked 2 and 3. The amount of disclination can be adjusted as needed.
由于三个旋轮在径向和轴向存在一定的错距,所以这种旋压成形方式叫做错距旋压。旋压成形时,已经调整好轴向和径向错距量的三个旋轮同时向左移动,并先后接触工件。通过调整旋轮的径向位置R1、R2、R3来实现所设计的工件壁厚总减薄量及各个旋轮分别承担的减薄量。Since there is a certain offset in the radial and axial directions of the three rollers, this spinning forming method is called offset spinning. During spinning, the three spinning wheels that have adjusted the axial and radial offsets move to the left at the same time, and contact the workpiece successively. By adjusting the radial positions R1, R2, and R3 of the rollers, the designed total thickness reduction of the workpiece and the respective reductions undertaken by each roller are realized.
如图6、7所示,筒形件旋压芯模4外形为圆柱形状,通过端部的法兰与机床主轴固定连接,图4所示的管形毛坯或图5所示的杯形毛坯套装在芯模4上,毛坯、芯模与机床主轴一起旋转。为了便于表达,将图6、图7中的三个旋轮分别画在同一圆周角度位置。框架旋轮座安装在机床的工作台上,并可以随工作台沿机床主轴方向移动,即沿芯模4的纵向移动。As shown in Figures 6 and 7, the tubular part spinning mandrel 4 has a cylindrical shape, and is fixedly connected to the main shaft of the machine tool through the flange at the end, the tubular blank shown in Figure 4 or the cup blank shown in Figure 5 Set on the mandrel 4, the blank, the mandrel and the machine tool spindle rotate together. For the convenience of expression, the three rotary wheels in Fig. 6 and Fig. 7 are respectively drawn at the same circumferential angular position. The frame wheel seat is installed on the workbench of the machine tool, and can move with the workbench along the direction of the main axis of the machine tool, that is, move along the longitudinal direction of the mandrel 4 .
当旋压图4所示的管形毛坯时,先将毛坯套在芯模4上,然后将三个旋轮在径向和轴向调整到合适的位置达到所设计的错距量,如图6所示。由于芯模和毛坯绕主轴Z旋转,当旋轮座向左移动、三个旋轮依次接触毛坯时,三个旋轮先后产生自转并向工件施加压力使工件产生变形,使其厚度减小。为防止在变形过程中毛坯与芯模之间打滑,在芯模4的根部固定一个端部带齿的挡圈5,在毛坯受力向左顶紧挡圈5时,挡圈的齿便将工件紧紧咬住,从而实现与芯模同步旋转。由于三个旋轮的轴向移动方向V与变形材料被挤出的流动方向V反相反,所以这种管形毛坯的旋压成形也叫反旋。When spinning the tubular blank shown in Figure 4, first put the blank on the mandrel 4, and then adjust the three rotary wheels to the appropriate position in the radial and axial directions to achieve the designed offset, as shown in the figure 6. Since the mandrel and the blank rotate around the main axis Z, when the wheel base moves to the left and the three wheels contact the blank in turn, the three wheels rotate successively and apply pressure to the workpiece to deform the workpiece and reduce its thickness. In order to prevent slippage between the blank and the mandrel during the deformation process, a retaining ring 5 with teeth at the end is fixed at the root of the mandrel 4, and when the blank is pressed against the retaining ring 5 to the left, the teeth of the retaining ring will The workpiece is bitten tightly so that it can rotate synchronously with the mandrel. Since the axial movement direction V of the three rollers is opposite to the flow direction V in which the deformed material is extruded, this spinning forming of the tubular blank is also called reverse rotation.
当旋压图5所示的杯形毛坯时,先将毛坯套在芯模4上,然后将三个旋轮在径向和轴向调整到合适的位置达到所设计的错距量,如图7所示。由于芯模和毛坯绕主轴Z旋转,当旋轮座向左移动、三个旋轮依次接触毛坯时,三个旋轮先后产生自转并向工件施加压力使工件产生变形,使其厚度减小。由尾顶6与芯模4将工件夹紧,并与芯模同步旋转。由于三个旋轮的轴向移动方向V与变形材料被挤出的流动方向V正相同,所以这种杯形毛坯的旋压成形也叫正旋。When spinning the cup-shaped blank shown in Figure 5, first put the blank on the mandrel 4, and then adjust the three rotary wheels to the appropriate position in the radial and axial directions to achieve the designed offset, as shown in the figure 7. Since the mandrel and the blank rotate around the main axis Z, when the wheel base moves to the left and the three wheels contact the blank in turn, the three wheels rotate successively and apply pressure to the workpiece to deform the workpiece and reduce its thickness. The workpiece is clamped by the tail top 6 and the mandrel 4, and rotates synchronously with the mandrel. Since the axial movement direction V of the three rollers is exactly the same as the flow direction V in which the deformed material is extruded, the spinning forming of this cup-shaped blank is also called positive rotation.
本发明利用上述正旋和反旋方法加工筒形零件。The present invention utilizes the above-mentioned forward rotation and reverse rotation methods to process cylindrical parts.
实施例1Example 1
一种低碳钢金属薄壁筒形件,材料为10钢(含碳量0.1%),形状如图1所示,其中筒形件内腔直径d=68mm,壁厚δ=0.6mm,长度l=1000mm。除形状要求外,还需要获得晶粒尺寸小于1μm的超细晶微观组织。A low-carbon steel metal thin-walled cylindrical part, the material is 10 steel (0.1% carbon content), the shape is shown in Figure 1, in which the diameter of the inner cavity of the cylindrical part is d=68mm, the wall thickness δ=0.6mm, and the length l=1000mm. In addition to shape requirements, it is also necessary to obtain an ultrafine-grained microstructure with a grain size of less than 1 μm.
1、由于市场上可以购买规格为的无缝钢管,其筒形件内腔直径d=68mm、壁厚Δ=4mm。若用这一规格的无缝钢管成形该零件,则壁厚应由4mm减薄至0.6mm,减薄率为85%。因此,该零件拟通过无缝钢管毛坯(如图4所示)经多道次旋压成形及再结晶处理方法加工(如图8所示)。该管坯原材料为退火状态,其晶粒形状为等轴晶,基本与图9相近,晶粒尺寸为30~50μm。1. Since the specifications can be purchased in the market as The seamless steel pipe, the diameter of the inner cavity of the cylindrical part is d=68mm, and the wall thickness is Δ=4mm. If the seamless steel pipe of this specification is used to form the part, the wall thickness should be reduced from 4mm to 0.6mm, and the thinning rate is 85%. Therefore, the part is planned to be processed by the seamless steel pipe blank (as shown in Figure 4) through multi-pass spinning forming and recrystallization treatment (as shown in Figure 8). The blank tube raw material is in an annealed state, and its grain shape is equiaxed, which is basically similar to that shown in Figure 9, and the grain size is 30-50 μm.
将零件加长30mm作为修边余量,按体积不变原理确定无缝钢管毛坯的长度为 Lengthen the part by 30mm as the trimming allowance, and determine the length of the seamless steel pipe blank according to the principle of constant volume as
2、设计一个直径68mm,长度1100mm的旋压芯模,安装在机床主轴上,将规格为长度为L=150mm的无缝钢管毛坯套在芯模上。采用三旋轮反旋错距旋压成形(如图6所示),轴向错距量为s12=s23=2.5mm;径向错距量为e12=e23=0.3mm。由于材料塑性较好,可以通过两道次旋压成形达到70%的壁厚减薄率:第一次旋压成形将工件壁厚由4mm减薄至2.4mm(减薄率为40%),即在满足错距量的情况下,将R3调整为芯模半径加上工件壁厚:R3=34+2.4=36.4(mm),完成一次旋压成形。第二次旋压成形将工件壁厚由2.4mm减薄至1.2mm(总减薄率为70%),即R3=34+1.2=35.2(mm),完成第二次旋压成形。2. Design a spinning mandrel with a diameter of 68mm and a length of 1100mm, install it on the spindle of the machine tool, and set the specification as A seamless steel pipe blank with a length of L=150mm is set on the mandrel. The three-rotation wheel is reverse-rotated and staggered for spinning (as shown in Figure 6). The axial stagger is s 12 =s 23 =2.5mm; the radial stagger is e 12 =e 23 =0.3mm. Due to the good plasticity of the material, a wall thickness reduction rate of 70% can be achieved through two passes of spinning: the first spin forming reduces the wall thickness of the workpiece from 4mm to 2.4mm (thinning rate is 40%), That is to say, in the case of satisfying the amount of misalignment, adjust R3 to the radius of the mandrel plus the wall thickness of the workpiece: R3=34+2.4=36.4 (mm), and complete a spinning forming. The second spinning forming reduces the wall thickness of the workpiece from 2.4mm to 1.2mm (the total thinning rate is 70%), that is, R3=34+1.2=35.2 (mm), and the second spinning forming is completed.
3、根据材料70%的变薄率,结合试验确定再结晶温度为560℃。将工件放至温度为T1=430℃的惰性气体保护炉中加热升温至T2=560℃,保温t=0.8小时,然后出炉水冷,如图10所示。将工件入炉时的炉温确定为430℃而不是室温,主要目的是减少工件占炉时间,并保证在升温至560℃的过程中工件内部具有较好的温度均匀性。3. According to the 70% thinning rate of the material, combined with the test, the recrystallization temperature is determined to be 560°C. Put the workpiece in an inert gas shielded furnace at T 1 =430°C and heat it up to T 2 =560°C, keep it warm for t=0.8 hours, and then take it out of the furnace for water cooling, as shown in Figure 10. The furnace temperature when the workpiece enters the furnace is determined to be 430°C instead of room temperature. The main purpose is to reduce the time the workpiece takes up in the furnace and ensure better temperature uniformity inside the workpiece during the process of heating up to 560°C.
4、将工件再次套装在旋压芯模上,三旋轮径向错距量调整至e12=e23=0.2mm,将工件壁厚由1.2mm减薄至0.6mm(总减薄率为85%),即将R3调整为R3=34+0.6=34.6(mm)完成第三次旋压成形。4. Set the workpiece on the spinning mandrel again, adjust the radial offset of the three-wheel to e 12 =e 23 =0.2mm, and reduce the wall thickness of the workpiece from 1.2mm to 0.6mm (the total thinning rate is 85%), that is, adjust R3 to R3=34+0.6=34.6 (mm) to complete the third spin forming.
由于经过前两道次的旋压成形,原先较为粗大的原始等轴晶粒被拉长成为细长的纤维组织,并且材料原子已聚积了较大的变形内能,在经历上述热处理时,原子重新排列完成再结晶,从而获得晶粒细小的等轴晶粒,与图11相近,可见晶粒尺寸已基本小于1um。再经过最后一道次旋压成形,进一步将细小的等轴晶粒拉长成为纤维组织,从而得到纤维横向的极小尺寸,即零件晶粒的特征维度尺寸极小。而晶粒尺寸的减小,有利于获得优异的材料性能。Due to the first two passes of spinning forming, the original relatively coarse equiaxed grains are elongated into elongated fibrous structures, and the material atoms have accumulated a large deformation internal energy. When undergoing the above heat treatment, the atoms Rearrangement completes recrystallization, thereby obtaining fine equiaxed grains, which is similar to Figure 11, and it can be seen that the grain size is basically smaller than 1um. After the final spinning forming, the fine equiaxed grains are further elongated into a fibrous structure, thereby obtaining an extremely small size in the transverse direction of the fiber, that is, the characteristic dimension of the grain of the part is extremely small. The reduction of the grain size is conducive to obtaining excellent material properties.
此时,工件总长度为1030mm,将两端各切掉15mm余量,得到合乎外形要求的零件,并且零件晶粒特征维度尺寸达100~800nm,为超细晶微观组织。At this time, the total length of the workpiece is 1030mm, and 15mm allowance is cut off at both ends to obtain a part that meets the shape requirements, and the characteristic dimension of the grain of the part reaches 100-800nm, which is an ultra-fine grain microstructure.
实施例2Example 2
一种低碳钢金属薄壁筒形件,材料为10钢(含碳量0.1%),形状如图1所示,其中筒形件内腔直径d=69mm,壁厚δ=0.6mm,长度l=1000mm。除形状要求外,还需要获得晶粒尺寸小于1μm的超细晶微观组织。A low-carbon steel metal thin-walled cylindrical part, the material is 10 steel (0.1% carbon content), the shape is shown in Figure 1, in which the diameter of the inner cavity of the cylindrical part is d=69mm, the wall thickness δ=0.6mm, and the length l=1000mm. In addition to shape requirements, it is also necessary to obtain an ultrafine-grained microstructure with a grain size of less than 1 μm.
1、该零件内径d=69mm,市场上没有与其相近的无缝钢管,该零件拟采用钢板经过拉深成形的杯形件(如图5所示)作为旋压毛坯,再经多道次旋压成形及再结晶处理方法加工(如图8所示)。该管坯原材料为退火状态,其晶粒形状为等轴晶,晶粒尺寸为30~50μm,如图9所示。1. The inner diameter of the part is d=69mm, and there is no similar seamless steel pipe on the market. The part is planned to use a cup-shaped part (as shown in Figure 5) formed by deep drawing of the steel plate as the spinning blank, and then spin through multiple passes. Press forming and recrystallization treatment method processing (as shown in Figure 8). The blank tube raw material is in an annealed state, its grain shape is equiaxed, and its grain size is 30-50 μm, as shown in FIG. 9 .
按总减薄率为85%的要求确定杯形毛坯的壁厚为Δ=4mm,因此可以选用杯形毛坯的厚度Δ=4mm的钢板,按体积不变原理设计直径为220mm的圆片,采用普通拉深成形方法得到杯形毛坯,如图5所示,其中内径d=69mm,杯形毛坯的壁厚Δ=4mm,深度L=150mm。The wall thickness of the cup-shaped blank is determined to be Δ=4mm according to the requirement of a total thinning rate of 85%. Therefore, a steel plate with a thickness of the cup-shaped blank of Δ=4mm can be selected, and a disc with a diameter of 220mm is designed according to the principle of constant volume. The cup-shaped blank is obtained by ordinary drawing forming method, as shown in Figure 5, where the inner diameter d=69mm, the wall thickness of the cup-shaped blank is Δ=4mm, and the depth L=150mm.
2、设计一个直径69mm,长度1100mm的旋压芯模,安装在机床主轴上,将上述拉深成形得到的杯形毛坯套在芯模上。采用三旋轮正旋错距旋压变形(如图7所示),轴向错距量为s12=s23=2mm;径向错距量为e12=e23=0.3mm。由于钢板经过拉深成形,塑性有所下降,与实施例1相比,将再结晶处理前的旋压壁厚减薄率降为60%:第一次旋压成形将R3调整为R3=34.5+2.6(mm),将工件壁厚由4mm减薄至2.6mm(减薄率为35%),第二次旋压成形将R3调整为R3=34.5+1.6(mm),将工件壁厚由2.6mm减薄至1.6mm(总减薄率为60%)。2. Design a spinning mandrel with a diameter of 69 mm and a length of 1100 mm, install it on the spindle of the machine tool, and put the cup-shaped blank obtained by the above-mentioned deep drawing on the mandrel. Using the three-rotor wheel positive rotation offset spinning deformation (as shown in Figure 7), the axial offset is s 12 =s 23 =2mm; the radial offset is e 12 =e 23 =0.3mm. Since the steel plate has undergone deep drawing, the plasticity has decreased. Compared with Example 1, the spinning wall thickness reduction rate before recrystallization treatment is reduced to 60%: the first spin forming adjusts R3 to R3=34.5 +2.6 (mm), reduce the wall thickness of the workpiece from 4mm to 2.6mm (thinning rate is 35%), adjust R3 to R3=34.5+1.6 (mm) in the second spinning forming, and reduce the wall thickness of the workpiece by 2.6mm thinned to 1.6mm (60% total thinning).
3、经过试验,该工件的再结晶处理温度为550℃,与实施例1相比,再结晶温度有所下降,是因为材料经过了拉深变形,虽然杯形毛坯旋压成形时的壁厚减薄率小于实施例1,但累积变形量却有所增加,材料内部应力及能量较高,原子活动能力增强,从而导致再结晶温度有所下降。因此将工件放至温度为T1=400℃的惰性气体保护炉中继续加热升温至T2=550℃,保温t=0.9小时,然后出炉水冷,如图10所示。热处理后材料的晶粒如图11所示。3. After testing, the recrystallization treatment temperature of the workpiece is 550°C. Compared with Example 1, the recrystallization temperature has decreased because the material has undergone deep drawing deformation, although the wall thickness of the cup-shaped blank during spinning The thinning rate is smaller than that of Example 1, but the cumulative deformation has increased, the internal stress and energy of the material are higher, and the atomic mobility is enhanced, resulting in a decrease in the recrystallization temperature. Therefore, put the workpiece in an inert gas shielded furnace with a temperature of T 1 =400°C and continue to heat up to T 2 =550°C, keep it warm for t=0.9 hours, and then take it out of the furnace for water cooling, as shown in Figure 10. The grains of the material after heat treatment are shown in Figure 11.
4、将工件再次套装在旋压芯模上,将R3调整为R3=34.5+0.6(mm),将工件壁厚由1.6mm减薄至0.6mm(总减薄率为85%)。4. Set the workpiece on the spinning mandrel again, adjust R3 to R3=34.5+0.6 (mm), and reduce the wall thickness of the workpiece from 1.6mm to 0.6mm (the total thinning rate is 85%).
此时,工件总长度为1034mm,将工件口部切掉20mm、底部切掉14mm余量(含切掉杯底),得到合乎外形要求的零件,并且零件晶粒特征维度尺寸达80~900nm,为纳米/超细晶微观组织。At this time, the total length of the workpiece is 1034mm. Cut off the mouth of the workpiece by 20mm and the bottom of the workpiece by 14mm (including cutting off the bottom of the cup) to obtain a part that meets the shape requirements, and the characteristic dimension of the grain of the part reaches 80-900nm. It is nano/ultrafine grain microstructure.
实施例3Example 3
一种低碳钢金属薄壁筒形件,材料为25钢(含碳量0.25%),形状如图1所示,其中壁筒形件内腔直径d=140mm,壁厚δ=0.5mm,长度l=500mm。除形状要求外,还需要获得晶粒尺寸小于1μm的超细晶微观组织。A low-carbon steel metal thin-walled cylindrical part, the material is 25 steel (0.25% carbon content), the shape is shown in Figure 1, the inner diameter of the wall cylindrical part d=140mm, the wall thickness δ=0.5mm, Length l=500mm. In addition to shape requirements, it is also necessary to obtain an ultrafine-grained microstructure with a grain size of less than 1 μm.
1、由于市场上可以购买规格为的无缝钢管,其无缝钢管内径d=140mm、无缝钢管壁厚Δ=5mm。若用这一规格的无缝钢管成形该零件,则壁厚应由5mm减薄至0.5mm,减薄率为90%。因此,该零件拟通过无缝钢管毛坯(如图4所示)经多道次旋压成形及再结晶处理方法加工(如图8所示)。该管坯原材料为退火状态,其晶粒形状为等轴晶,晶粒尺寸基本与图9相近。1. Since the specifications can be purchased in the market as seamless steel pipe, the inner diameter of the seamless steel pipe is d=140mm, and the wall thickness of the seamless steel pipe is Δ=5mm. If the seamless steel pipe of this specification is used to form the part, the wall thickness should be reduced from 5mm to 0.5mm, and the thinning rate is 90%. Therefore, the part is planned to be processed by the seamless steel pipe blank (as shown in Figure 4) through multi-pass spinning forming and recrystallization treatment (as shown in Figure 8). The blank tube raw material is in an annealed state, its grain shape is equiaxed, and its grain size is basically similar to that shown in Fig. 9 .
由于零件直径较大,壁厚较薄,旋压成形时口部质量相对较差,因此将成形后的修边余量增加至50mm,按体积不变原理确定毛坯长度为 Due to the large diameter and thin wall thickness of the part, the quality of the mouth part during spinning is relatively poor, so the trimming allowance after forming is increased to 50mm, and the length of the blank is determined according to the principle of constant volume.
2、设计一个直径140mm,长度600mm的旋压芯模,安装在机床主轴上,将规格为长度为L=53.5mm的无缝钢管毛坯套在芯模上。采用三旋轮反旋错距旋压成形(如图6所示),轴向错距量为s12=s23=1.5mm;径向错距量为e12=e23=0.2mm。与实施例1相比,材料的含碳量有所增加,塑性有所下降,因此确定再结晶处理前的总壁厚减薄率为60%。第一次旋压成形将R3调整为R3=70+3.25(mm),将工件壁厚由5mm减薄至3.25mm(减薄率为35%),第二次旋压成形将R3调整为R3=34.5+2(mm),将工件壁厚由3.25mm减薄至2mm(总减薄率为60%)。2. Design a spinning mandrel with a diameter of 140mm and a length of 600mm, install it on the spindle of the machine tool, and set the specification as A seamless steel pipe blank with a length of L=53.5mm is set on the mandrel. Adopt three-rotation wheel anti-rotation and staggered pitch spinning (as shown in Figure 6), the axial staggered amount is s 12 =s 23 =1.5mm; the radial staggered amount is e 12 =e 23 =0.2mm. Compared with Example 1, the carbon content of the material has increased, and the plasticity has decreased, so it is determined that the total wall thickness reduction rate before recrystallization treatment is 60%. Adjust R3 to R3=70+3.25 (mm) for the first spinning forming, and reduce the wall thickness of the workpiece from 5mm to 3.25mm (35% thinning rate), and adjust R3 to R3 for the second spinning forming =34.5+2 (mm), reduce the wall thickness of the workpiece from 3.25mm to 2mm (the total thinning rate is 60%).
3、经过试验,该工件的再结晶温度为600℃,因此将工件放至温度为T1=450℃的惰性气体保护炉中继续加热升温至T2=600℃,保温t=1小时,然后出炉水冷,如图10所示。热处理后材料的晶粒与图11相近。3. After testing, the recrystallization temperature of the workpiece is 600°C, so put the workpiece into an inert gas protection furnace with a temperature of T 1 =450°C and continue heating to T 2 =600°C, keep it warm for t=1 hour, and then Out of the furnace water cooling, as shown in Figure 10. The grain size of the material after heat treatment is similar to that shown in Figure 11.
4、将工件再次套装在旋压芯模上,三旋轮径向错距量调整至e12=e23=0.1mm,先将R3调整为R3=34.5+1.1(mm),将工件壁厚由2mm减薄至1.1mm(总减薄率为78%),再将R3调整为R3=34.5+0.5(mm),将工件壁厚由1.1mm减薄至0.5mm(总减薄率为90%)。4. Set the workpiece on the spinning mandrel again, adjust the radial offset of the three-rotor wheel to e 12 =e 23 =0.1mm, first adjust R3 to R3=34.5+1.1 (mm), and adjust the wall thickness of the workpiece Thinning from 2mm to 1.1mm (the total thinning rate is 78%), then adjust R3 to R3=34.5+0.5 (mm), and reduce the workpiece wall thickness from 1.1mm to 0.5mm (the total thinning rate is 90%) %).
此时,工件总长度为650mm,将两端各切掉25mm余量,得到合乎外形要求的零件,并且零件晶粒特征维度尺寸达100~1000nm,为超细晶微观组织。At this time, the total length of the workpiece is 650mm, and the two ends are cut off with a margin of 25mm to obtain a part that meets the shape requirements, and the characteristic dimension of the grain of the part reaches 100-1000nm, which is an ultra-fine grain microstructure.
在本发明的实施过程中,重点是要保证变形过程中获得很大的工件壁厚减薄率,以及在多道次旋压变形过程中安排再结晶处理工序,将变形过程中的晶粒拉长变细与再结晶处理过程中的晶粒形核及抑制长大有机结合起来,从而获得满足高性能要求的金属薄壁筒形零件。再结晶处理温度受多方面因素的影响,如钢中杂质元素越多,再结晶温度越高;材料变形程度越大,再结晶温度越低等,往往需要通过试验确定工件的再结晶温度。In the implementation process of the present invention, the focus is to ensure that a large workpiece wall thickness reduction rate is obtained in the deformation process, and to arrange a recrystallization process in the multi-pass spinning deformation process to pull the crystal grains in the deformation process. The growth and thinning are organically combined with the grain nucleation and growth suppression during the recrystallization process, so as to obtain metal thin-walled cylindrical parts that meet high performance requirements. The recrystallization treatment temperature is affected by many factors, such as the more impurity elements in the steel, the higher the recrystallization temperature; the greater the deformation of the material, the lower the recrystallization temperature, etc. It is often necessary to determine the recrystallization temperature of the workpiece through experiments.
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