CN103211740B - Moisturizing emulsion composition containing guava extractive and hydrolyzed pearl - Google Patents
Moisturizing emulsion composition containing guava extractive and hydrolyzed pearl Download PDFInfo
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Abstract
本发明涉及一种含番石榴提取物和水解珍珠的润泽保湿乳液组合物，所述乳液组合物由以下的组份构成：相1：聚二甲基硅氧烷、生育酚乙酸酯、白油、氢化聚癸烯、棕榈酸乙基己酯、山梨坦硬脂酸酯/蔗糖椰油酸酯、角鲨烷、羟苯丙酯，相2：去离子水、透明质酸钠、甘油、卡波姆、丙二醇、羟苯甲酯、丁二醇，相3：三乙醇胺、水解珍珠、番石榴提取物、香精、DMDM乙内酰脲/碘丙炔醇丁基氨甲酸酯，制备方法：相1放入容器中混合，加热至80℃；相2放入另一容器中加热至80℃；相1加入相2，乳化，均质，搅拌均匀，降温至50℃，加入相3，搅拌均匀后，出料。该组合物具有持久保湿、调理肌肤，改善肤色，调整暗黄状态，使肌肤润泽嫩白的特点。The present invention relates to a moisturizing emulsion composition containing guava extract and hydrolyzed pearls, said emulsion composition is composed of the following components: phase 1: polydimethylsiloxane, tocopheryl acetate, white Oil, Hydrogenated Polydecene, Ethylhexyl Palmitate, Sorbitan Stearate/Sucrose Cocoate, Squalane, Propylparaben, Phase 2: Deionized Water, Sodium Hyaluronate, Glycerin, Carbomer, Propylene Glycol, Methylparaben, Butylene Glycol, Phase 3: Triethanolamine, Hydrolyzed Pearl, Guava Extract, Fragrance, DMDM Hydantoin/Iodopropynyl Butylcarbamate, Preparation Method : Mix phase 1 in a container and heat to 80°C; put phase 2 into another container and heat to 80°C; add phase 1 to phase 2, emulsify, homogenize, stir evenly, cool down to 50°C, add phase 3, After stirring evenly, discharge. The composition has the characteristics of lasting moisturizing, conditioning the skin, improving the skin tone, adjusting the dark yellow state, and making the skin moist and white.
Description
本专利申请是发明专利申请（申请号：201110289313X申请日：2011-9-27，发明创造名称：一种润泽保湿乳液组合物及其制备方法）的分案申请。This patent application is a divisional application of an invention patent application (application number: 201110289313X application date: 2011-9-27, invention name: a moisturizing emulsion composition and its preparation method).
技术领域technical field
本发明属于一种长时补水的润泽保湿乳液组合物及其制备方法。The invention belongs to a moisturizing emulsion composition for long-term water replenishment and a preparation method thereof.
背景技术Background technique
由于现代人们生活节奏快，以及受各种环境影响，皮肤经常干燥、暗淡无光泽。Due to the fast-paced life of modern people and the influence of various environments, the skin is often dry and dull.
中国发明专利申请（申请号：200910010837.3申请日：2009-03-24）公开了一种美容护肤保湿剂。它是由以下组分按下述重量份数比组成的:护肤基料∶天然二甲基氨酸脯氨酸∶甘油∶蜂蜜∶乳木果油∶维生素E=80-120∶5-12∶1-3∶10-20∶1-3∶2-4。该发明含乳木果油、甘油、蜂蜜等活性滋养保湿成份,能够迅速帮助滋润干燥肌肤,令肌肤细腻柔滑。Chinese invention patent application (application number: 200910010837.3 application date: 2009-03-24) discloses a moisturizing agent for beauty and skin care. It is composed of the following components according to the following weight ratio: skin care base material: natural dimethyl amino acid proline: glycerin: honey: shea butter: vitamin E = 80-120: 5-12: 1-3: 10-20: 1-3: 2-4. The invention contains active nourishing and moisturizing ingredients such as shea butter, glycerin, and honey, which can quickly help moisturize dry skin and make skin delicate and smooth.
中国发明专利申请（申请号：200710150410.4申请日：2007-11-26）公开了一种含有木糖醇的化妆品保湿剂,它是由下述重量份数的原料组成:2-10份保湿剂,0.1-2份油脂,乳化剂5-15份,水60～80份。该发明的化妆品保湿剂能够较深入扩散到皮肤深处,与深层水结合,保持皮肤的润泽。Chinese invention patent application (application number: 200710150410.4 filing date: 2007-11-26) discloses a cosmetic moisturizer containing xylitol, which is composed of the following raw materials in parts by weight: 2-10 parts of moisturizer, 0.1-2 parts of oil, 5-15 parts of emulsifier, 60-80 parts of water. The cosmetic moisturizing agent of the invention can be deeply diffused into the deep skin, and combined with deep water to keep the skin moisturized.
发明内容Contents of the invention
为了解决人们皮肤经常干燥、暗淡无光泽的问题，本发明的一个目的是提供一种润泽保湿乳液组合物，该组合物具有持久保湿、调理肌肤，改善肤色，调整暗黄状态，使肌肤润泽嫩白的特点。本发明另外一个目的是提供一种上述的润泽保湿乳液组合物的制备方法。In order to solve the problem that people's skin is often dry and dull, an object of the present invention is to provide a moisturizing lotion composition, which has the functions of lasting moisturizing, skin conditioning, improving skin color, adjusting dark yellow state, and making skin moist and tender. white features. Another object of the present invention is to provide a method for preparing the above moisturizing emulsion composition.
为了实现上述第一个目的，本发明采用了以下的技术方案：In order to realize above-mentioned first object, the present invention adopts following technical scheme:
一种润泽保湿乳液组合物，所述乳液组合物按质量百分比计包括以下的组份：A moisturizing emulsion composition, said emulsion composition comprises the following components by mass percentage:
（a）0.01%至30%的润肤油脂；(a) 0.01% to 30% emollient oils;
（b）0.01%至20%的保湿剂；(b) 0.01% to 20% humectants;
（c）0.01%至10%的表面活性剂；(c) 0.01% to 10% surfactant;
（d）0.01%至10%的增稠聚合物；(d) 0.01% to 10% thickening polymer;
（e）0.01%至10%皮肤调理剂；和(e) 0.01% to 10% skin conditioning agents; and
（f）10%至90%的去离子水。(f) 10% to 90% deionized water.
作为优选，所述乳液组合物按质量百分比计包括以下的组份：As preferably, the emulsion composition comprises the following components by mass percentage:
（a）1%至20%的润肤油脂；(a) 1% to 20% emollient oils;
（b）1%至20%的保湿剂；(b) 1% to 20% humectants;
（c）0.01%至8%的表面活性剂；(c) 0.01% to 8% surfactant;
（d）0.01%至8%的增稠聚合物；(d) 0.01% to 8% thickening polymer;
（e）0.01%至8%皮肤调理剂；和(e) 0.01% to 8% skin conditioning agents; and
（f）10%至90%的去离子水。(f) 10% to 90% deionized water.
作为再优选，所述乳液组合物按质量百分比计包括以下的组份：As another preference, the emulsion composition comprises the following components by mass percentage:
（a）5%至15%的润肤油脂；(a) 5% to 15% emollient oils;
（b）2%至20%的保湿剂；(b) 2% to 20% humectants;
（c）0.01%至6%的表面活性剂；(c) 0.01% to 6% surfactant;
（d）0.01%至6%的增稠聚合物；(d) 0.01% to 6% thickening polymer;
（e）0.01%至6%皮肤调理剂；和(e) 0.01% to 6% skin conditioning agents; and
（f）10%至90%的去离子水。(f) 10% to 90% deionized water.
作为优选，上述的润肤油脂选自聚二甲基硅氧烷、矿油、棕榈酸乙基己酯、角鲨烷、杏仁油和氢化聚癸烯中的一种或多种。Preferably, the above-mentioned emollient oil is selected from one or more of polydimethylsiloxane, mineral oil, ethylhexyl palmitate, squalane, almond oil and hydrogenated polydecene.
作为优选，上述的保湿剂选用丙二醇、山梨醇、丁二醇、1,2-己二醇、辛甘醇、二丙二醇、甘油、双甘油、戊二醇、聚乙二醇中的一种或多种；再优选是甘油或丙二醇。As preferably, the above-mentioned moisturizing agent is selected from one of propylene glycol, sorbitol, butanediol, 1,2-hexanediol, caprylyl glycol, dipropylene glycol, glycerin, diglycerin, pentylene glycol, polyethylene glycol or Various; more preferably glycerin or propylene glycol.
作为优选，上述的表面活性剂天然绿色乳化剂；再优选是山梨坦硬脂酸酯和蔗糖椰油酸酯一种或两种。As preferably, above-mentioned surfactant natural green emulsifier; More preferably one or both of sorbitan stearate and sucrose cocoate.
作为优选，上述的增稠剂选用羧酸聚合物、交联聚丙烯酸酯聚合物、纤维素醚类合成的高分子聚合物、天然的高分子聚合物中的一种或多种；再优选是丙烯酸交联聚合物，更优选是按CTFA命名为卡波姆的物质。As preferably, the above-mentioned thickener is selected from one or more of carboxylic acid polymers, cross-linked polyacrylate polymers, cellulose ether synthetic polymers, and natural polymers; more preferably The acrylic crosslinked polymer, more preferably the CTFA designation Carbomer.
作为优选，上述的皮肤调理剂选用水解珍珠、三色堇花提取物、番石榴果提取物和透明质酸钠中的一种或多种。Preferably, the above-mentioned skin conditioning agent is selected from one or more of hydrolyzed pearls, pansy flower extract, guava fruit extract and sodium hyaluronate.
作为优选，上述的组合物还包含了抗氧化剂、pH调节剂、防腐剂和香精中的一种或多种，所述的抗氧化剂为生育酚乙酸酯；抗氧化剂的质量含量优选0.01%～8%，更优选为0.01%～6%。As a preference, the above-mentioned composition also includes one or more of antioxidants, pH regulators, preservatives and essences, and the antioxidants are tocopherol acetate; the mass content of antioxidants is preferably 0.01% to 8%, more preferably 0.01% to 6%.
本发明组合物还可包括各种各样的其他成分。本发明的组合物的具体成份的功能和效果将在下文中详细描述。The compositions of the present invention may also include a wide variety of other ingredients. The functions and effects of specific ingredients of the composition of the present invention will be described in detail hereinafter.
润肤油脂Moisturizer
本发明组合物中的润肤油脂，可以锁住水分，防止过度挥发，使皮肤保持水嫩光泽。本发明组合物中的润肤油脂聚二甲基硅氧烷，其按所述组合物的重量计约0.01%至20%，优选约为0.01%至15%，更优选约0.01%至10%。它无毒，对皮肤和粘膜无刺激性，但对眼睛有刺激性。一般公认是安全的。具有优良的化学稳定性，抗静电性和透气性，使皮肤能够自由呼吸。The emollient oil in the composition of the invention can lock moisture, prevent excessive volatilization, and keep the skin supple and lustrous. Emollient oil dimethicone in the compositions of the present invention, from about 0.01% to 20%, preferably from about 0.01% to 15%, more preferably from about 0.01% to 10%, by weight of the composition . It is non-toxic and non-irritating to the skin and mucous membranes, but irritating to the eyes. Generally recognized as safe. It has excellent chemical stability, antistatic properties and air permeability, allowing the skin to breathe freely.
本发明组合物中的润肤油脂白油，其按所述组合物的重量计约0.01%至20%，优选约为0.01%至15%，更优选约0.01%至10%。它为无色透明油状液体，没有气味，对酸、光、热均稳定，是石油的润滑油馏分经加氢精制而得的，广泛应用于化妆品。Emollient white oil is present in the compositions of the present invention at from about 0.01% to 20%, preferably from about 0.01% to 15%, more preferably from about 0.01% to 10%, by weight of the composition. It is a colorless transparent oily liquid with no odor and is stable to acid, light and heat. It is obtained by hydrotreating petroleum lubricating oil fractions and is widely used in cosmetics.
本发明组合物中的润肤油脂棕榈酸乙基己酯，其按所述组合物的重量计约0.01%至20%，优选约为0.01%至15%，更优选约0.01%至10%。它是一种微黄色的油状液体，不易氧化、不变色、稳定性好，有良好的润肤、延展和渗透性，滋润和软化肌肤，又无油腻感，是良好的润肤剂。The emollient oil ethylhexyl palmitate in the composition of the present invention is present at about 0.01% to 20%, preferably about 0.01% to 15%, more preferably about 0.01% to 10%, by weight of the composition. It is a kind of yellowish oily liquid, which is not easy to oxidize, does not change color, has good stability, has good emollient, extensible and penetrating properties, moisturizes and softens the skin, and has no greasy feeling. It is a good emollient.
本发明组合物中的润肤油脂角鲨烷，其按所述组合物的重量计约0.01%至20%，优选约为0.01%至15%，更优选约0.01%至10%。它具有天然角鲨烷的化妆品特性，是一种无色、无味、无毒的高纯度液体衣钩直链烷烃，能赋予化妆品极好而高贵的手感，滋润不油腻，保湿润滑，渗透力强，且稳定性好。The emollient oil squalane is present in the compositions of the present invention at from about 0.01% to 20%, preferably from about 0.01% to 15%, more preferably from about 0.01% to 10%, by weight of the composition. It has the cosmetic properties of natural squalane. It is a colorless, odorless, non-toxic, high-purity liquid cloacane linear alkane, which can give cosmetics an excellent and noble feel, moisturizing and non-greasy, moisturizing and lubricating, and strong penetration. , and good stability.
本发明组合物中的润肤油脂杏仁油，其按所述组合物的重量计约0.01%至20%，优选约为0.01%至15%，更优选约0.01%至10%。本发明组合物中的杏仁油，微黄透明，是一种优良的天然植物油，含有蛋白质、不饱和脂肪酸、维生素、无机盐和人体所需的微量元素等，滋养皮肤，良好的抗氧化性，可抚平细纹，延缓衰老。The emollient almond oil is present in the compositions of the present invention at about 0.01% to 20%, preferably from about 0.01% to 15%, more preferably from about 0.01% to 10%, by weight of the composition. The almond oil in the composition of the present invention is slightly yellow and transparent, and is an excellent natural vegetable oil, containing protein, unsaturated fatty acids, vitamins, inorganic salts and trace elements needed by the human body, etc., nourishes the skin, and has good oxidation resistance. Smoothes fine lines and delays aging.
本发明组合物中的润肤油脂氢化聚癸烯，其按所述组合物的重量计约0.01%至20%，优选约为0.01%至15%，更优选约0.01%至10%。本发明组合物中的氢化聚癸烯，是一类无色,无味的透明液体,是高级化妆品的油性原料和活性原料的助渗剂,可应用于各种化妆品中。稳定性好，具有丝滑的肤感。The emollient oil hydrogenated polydecene present in the compositions of the present invention comprises from about 0.01% to 20%, preferably from about 0.01% to 15%, more preferably from about 0.01% to 10%, by weight of the composition. The hydrogenated polydecene in the composition of the present invention is a kind of colorless, odorless transparent liquid, which is an oily raw material of high-grade cosmetics and a penetration aid of active raw materials, and can be applied to various cosmetics. Good stability and silky skin feel.
保湿剂moisturizer
本发明中的以重量计约0.01%至20%的保湿剂为多元醇，本文所述组合物优选包含按所述组合物的重量计约1%至20%，更优选的是2%-20%的保湿剂，实例包括丙二醇、山梨醇、丁二醇、1,2-己二醇、辛甘醇、二丙二醇、甘油、双甘油、戊二醇、聚乙二醇，以及它们的混合物，优选用于本组合物的是甘油、丙二醇。From about 0.01% to 20% by weight of the humectant of the present invention is a polyol, and the compositions described herein preferably comprise from about 1% to 20%, more preferably from 2% to 20% by weight of the composition. % humectants, examples include propylene glycol, sorbitol, butylene glycol, 1,2-hexanediol, caprylyl glycol, dipropylene glycol, glycerin, diglycerin, pentylene glycol, polyethylene glycol, and mixtures thereof, Preferred for use in the present composition are glycerin, propylene glycol.
表面活性剂Surfactant
本发明组合物中的表面活性剂为山梨坦硬脂酸酯/蔗糖椰油酸酯，其按所述组合物的重量计约0.01%至10%，优选约为0.01%至8%，更优选约0.01%至6%。本发明组合物山梨坦硬脂酸酯/蔗糖椰油酸酯，是一种天然糖苷的液晶乳化剂，温和无刺激，能形成液晶结构，带给肌肤丝一般的肤感。The surfactant in the compositions of the present invention is sorbitan stearate/sucrose cocoate at about 0.01% to 10% by weight of the composition, preferably at about 0.01% to 8%, more preferably About 0.01% to 6%. The composition of the present invention, sorbitan stearate/sucrose cocoate, is a natural glycoside liquid crystal emulsifier, mild and non-irritating, capable of forming a liquid crystal structure, and bringing silky skin feel to the skin.
增稠剂thickener
在一些实施方案中，本发明的组合物还可以包括一种或多种增稠剂，所述组合物包括按所述组合物的重量计约0.01%至10%，优选约为0.01%至8%，更优选约0.01%至6%的增稠剂。In some embodiments, the compositions of the present invention may also include one or more thickeners, the composition comprising from about 0.01% to 10%, preferably from about 0.01% to 8% by weight of the composition. %, more preferably from about 0.01% to 6% of thickener.
增稠剂的非限制性种类包括选自以下物质：羧酸聚合物（如Carbopol980）、交联聚丙烯酸酯聚合物、合成的高分子聚合物（如纤维素醚类）、天然的高分子聚合物（如树胶），优选的是丙烯酸交联聚合物，更优选的是按CTFA命名为卡波姆的物质。Non-limiting types of thickeners include substances selected from the following: carboxylic acid polymers (such as Carbopol 980), cross-linked polyacrylate polymers, synthetic polymers (such as cellulose ethers), natural polymers Substances such as gums, preferably acrylic crosslinked polymers, more preferably the CTFA nomenclature Carbomer.
皮肤调理剂skin conditioner
本发明组合物所添加的多种皮肤调理剂为水解珍珠、三色堇花提取物、番石榴果提取物、透明质酸钠。The various skin conditioning agents added to the composition of the present invention are hydrolyzed pearls, pansy flower extract, guava fruit extract, sodium hyaluronate.
本发明组合物的水解珍珠,其含量按本发明组合物的重量计约0.01%至10%，优选约为0.01%至8%，更优选约为0.01%至6%，其活性物含量按本发明组合物的重量计约0.001%至10%，优选约0.001%至8%，更优选约0.001%至6%。The hydrolyzed pearl of the composition of the present invention, its content is about 0.01% to 10% by weight of the composition of the present invention, preferably about 0.01% to 8%, more preferably about 0.01% to 6%. The inventive compositions comprise from about 0.001% to 10%, preferably from about 0.001% to 8%, more preferably from about 0.001% to 6%, by weight.
本发明组合物的水解珍珠，是通过珍珠粉的酶解工艺得到的，含有大量的钙离子和珍珠蛋白质，具有消除氧自由基，抗衰老作用，淡斑，使肌肤亮丽光泽。The hydrolyzed pearl of the composition of the present invention is obtained through the enzymatic hydrolysis process of pearl powder, contains a large amount of calcium ions and pearl protein, has the functions of eliminating oxygen free radicals, anti-aging, lightening spots, and making skin bright and lustrous.
本发明组合物添加的三色堇花提取物的含量按所述组合物的重量计优选为约0.01%至8%，更优选约0.01%至6%，本发明组合物的三色堇花提取物的活性含量按所述组合物的重量计优选约0.001%至8%，更优选约0.001%至6%。The content of the pansy flower extract added to the composition of the present invention is preferably about 0.01% to 8%, more preferably about 0.01% to 6%, by weight of the composition. The pansy flower extract of the composition of the present invention The active content of the compound is preferably from about 0.001% to 8%, more preferably from about 0.001% to 6%, by weight of the composition.
本发明组合物的三色堇花提取物，富含芸香甙，皂甙和维生素C、生育酚等。全面调理肌肤至水油平衡的健康状态，具有抗菌作用，明显的消痘功效。The pansy flower extract of the composition of the present invention is rich in rutin, saponin, vitamin C, tocopherol and the like. Fully regulate the skin to a healthy state of water and oil balance, has antibacterial effect, and has obvious anti-acne effect.
本发明组合物添加的番石榴果提取物的含量按所述组合物的重量计优选为约0.01%至8%，更优选约0.01%至6%，本发明组合物的番石榴果提取物的活性含量按所述组合物的重量计优选约0.001%至8%，更优选约0.001%至6%。The content of the guava fruit extract added to the composition of the present invention is preferably from about 0.01% to 8%, more preferably from about 0.01% to 6%, by weight of the composition, the guava fruit extract of the composition of the present invention The active level is preferably from about 0.001% to 8%, more preferably from about 0.001% to 6%, by weight of the composition.
本发明组合物的番石榴果提取物，富含维生素C、蛋白质、脂肪、维生素A、B类维生素、钙、磷、铁等微量元素，能有效中和自由基，促进新陈代谢，帮助肌肤排出“毒素”，即时发挥美白保湿功效。The guava fruit extract of the composition of the present invention is rich in vitamin C, protein, fat, vitamin A, B vitamins, calcium, phosphorus, iron and other trace elements, which can effectively neutralize free radicals, promote metabolism, and help the skin to discharge " toxins” to instantly exert the whitening and moisturizing effect.
本发明组合物的透明质酸钠，是一种仿生物黏糖，分子量大于100万，本发明组合物的透明质酸钠含量按发明组合物重量计约0.01%至10%，优选约0.01%至5%，更优选约为0.01%至3%。The sodium hyaluronate of the composition of the present invention is a kind of imitation bioglucose, the molecular weight is greater than 1 million, and the sodium hyaluronate content of the composition of the present invention is about 0.01% to 10% by weight of the composition of the invention, preferably about 0.01% to 5%, more preferably about 0.01% to 3%.
正常人皮肤角质层中含有10%至20%的水分，其对滋润皮肤，防止皮肤老化、防止外界环境的各种刺激都有重大作用。随着年龄的增长或环境的变化，水分会降到10%以下，皮肤会干燥，产生皱纹。本发明组合物的透明质酸钠可以缓解这一问题，它的理论保水值达1000ml/g，是人体皮肤中保水的关键成分，不但保湿效果好，而且无油腻感和堵塞毛孔的等缺点。还可以消除氧自由基，修复晒后损伤的皮肤。The stratum corneum of normal human skin contains 10% to 20% water, which plays an important role in moisturizing the skin, preventing skin aging, and preventing various stimuli from the external environment. As we grow older or the environment changes, the moisture content drops below 10%, and the skin becomes dry and wrinkled. The sodium hyaluronate in the composition of the present invention can alleviate this problem, and its theoretical water retention value reaches 1000ml/g, which is the key component of water retention in human skin. It can also eliminate oxygen free radicals and repair damaged skin after sun exposure.
抗氧化剂Antioxidants
本发明组合物的抗氧化剂为生育酚乙酸酯，其含量按发明组合物重量计约0.01%至10%，优选约0.01%至8%，更优选约为0.01%至6%。本发明组合物生育酚乙酸酯是维生素E类，可作为抗氧化剂，消除体内自由基，减少紫外线对人体的伤害。由于维生素E有较强的还原性，在人体新陈代谢过程中有抗氧化性而防止衰老的作用。The antioxidant of the composition of the present invention is tocopheryl acetate, and its content is about 0.01% to 10%, preferably about 0.01% to 8%, more preferably about 0.01% to 6% by weight of the composition of the invention. The tocopherol acetate in the composition of the present invention is vitamin E and can be used as an antioxidant to eliminate free radicals in the body and reduce the damage of ultraviolet rays to the human body. Because vitamin E has a strong reducing property, it has anti-oxidation and anti-aging effects in the process of human metabolism.
润肤油脂Moisturizer
本发明组合物中的润肤油脂，可以锁住水分，防止过度挥发，使皮肤保持水嫩光泽。The emollient oil in the composition of the invention can lock moisture, prevent excessive volatilization, and keep the skin supple and lustrous.
本发明组合物中的润肤油脂聚二甲基硅氧烷，其按所述组合物的重量计约0.01%至20%，优选约为0.01%至15%，更优选约0.01%至10%。它无毒，对皮肤和粘膜无刺激性，但对眼睛有刺激性。一般公认是安全的。具有优良的化学稳定性，抗静电性和透气性，使皮肤能够自由呼吸。Emollient oil dimethicone in the compositions of the present invention, from about 0.01% to 20%, preferably from about 0.01% to 15%, more preferably from about 0.01% to 10%, by weight of the composition . It is non-toxic and non-irritating to the skin and mucous membranes, but irritating to the eyes. Generally recognized as safe. It has excellent chemical stability, antistatic properties and air permeability, allowing the skin to breathe freely.
本发明组合物中的润肤油脂白油，其按所述组合物的重量计约0.01%至20%，优选约为0.01%至15%，更优选约0.01%至10%。它为无色透明油状液体，没有气味，对酸、光、热均稳定，是石油的润滑油馏分经加氢精制而得的，广泛应用于化妆品。Emollient white oil is present in the compositions of the present invention at from about 0.01% to 20%, preferably from about 0.01% to 15%, more preferably from about 0.01% to 10%, by weight of the composition. It is a colorless transparent oily liquid with no odor and is stable to acid, light and heat. It is obtained by hydrotreating petroleum lubricating oil fractions and is widely used in cosmetics.
本发明组合物中的润肤油脂棕榈酸乙基己酯，其按所述组合物的重量计约0.01%至20%，优选约为0.01%至15%，更优选约0.01%至10%。它是一种微黄色的油状液体，不易氧化、不变色、稳定性好，有良好的润肤、延展和渗透性，滋润和软化肌肤，又无油腻感，是良好的润肤剂。The emollient oil ethylhexyl palmitate in the composition of the present invention is present at about 0.01% to 20%, preferably about 0.01% to 15%, more preferably about 0.01% to 10%, by weight of the composition. It is a kind of yellowish oily liquid, which is not easy to oxidize, does not change color, has good stability, has good emollient, extensible and penetrating properties, moisturizes and softens the skin, and has no greasy feeling. It is a good emollient.
本发明组合物中的润肤油脂角鲨烷，其按所述组合物的重量计约0.01%至20%，优选约为0.01%至15%，更优选约0.01%至10%。它具有天然角鲨烷的化妆品特性，是一种无色、无味、无毒的高纯度液体衣钩直链烷烃，能赋予化妆品极好而高贵的手感，滋润不油腻，保湿润滑，渗透力强，且稳定性好。The emollient oil squalane is present in the compositions of the present invention at from about 0.01% to 20%, preferably from about 0.01% to 15%, more preferably from about 0.01% to 10%, by weight of the composition. It has the cosmetic properties of natural squalane. It is a colorless, odorless, non-toxic, high-purity liquid cloacane linear alkane, which can give cosmetics an excellent and noble feel, moisturizing and non-greasy, moisturizing and lubricating, and strong penetration. , and good stability.
本发明组合物中的润肤油脂杏仁油，其按所述组合物的重量计约0.01%至20%，优选约为0.01%至15%，更优选约0.01%至10%。本发明组合物中的杏仁油，微黄透明，是一种优良的天然植物油，含有蛋白质、不饱和脂肪酸、维生素、无机盐和人体所需的微量元素等，滋养皮肤，良好的抗氧化性，可抚平细纹，延缓衰老。The emollient almond oil is present in the compositions of the present invention at about 0.01% to 20%, preferably from about 0.01% to 15%, more preferably from about 0.01% to 10%, by weight of the composition. The almond oil in the composition of the present invention is slightly yellow and transparent, and is an excellent natural vegetable oil, containing protein, unsaturated fatty acids, vitamins, inorganic salts and trace elements needed by the human body, etc., nourishes the skin, and has good oxidation resistance. Smoothes fine lines and delays aging.
本发明组合物中的润肤油脂氢化聚癸烯，其按所述组合物的重量计约0.01%至20%，优选约为0.01%至15%，更优选约0.01%至10%。本发明组合物中的氢化聚癸烯，是一类无色,无味的透明液体,是高级化妆品的油性原料和活性原料的助渗剂,可应用于各种化妆品中。稳定性好，具有丝滑的肤感。The emollient oil hydrogenated polydecene present in the compositions of the present invention comprises from about 0.01% to 20%, preferably from about 0.01% to 15%, more preferably from about 0.01% to 10%, by weight of the composition. The hydrogenated polydecene in the composition of the present invention is a kind of colorless, odorless transparent liquid, which is an oily raw material of high-grade cosmetics and a penetration aid of active raw materials, and can be applied to various cosmetics. Good stability and silky skin feel.
保湿剂moisturizer
本发明中的以重量计约0.01%至20%的保湿剂为多元醇，本文所述组合物优选包含按所述组合物的重量计约1%至20%，更优选的是2%-20%的保湿剂，实例包括丙二醇、山梨醇、丁二醇、1,2-己二醇、辛甘醇、二丙二醇、甘油、双甘油、戊二醇、聚乙二醇，以及它们的混合物，优选用于本组合物的是甘油、丙二醇。From about 0.01% to 20% by weight of the humectant of the present invention is a polyol, and the compositions described herein preferably comprise from about 1% to 20%, more preferably from 2% to 20% by weight of the composition. % humectants, examples include propylene glycol, sorbitol, butylene glycol, 1,2-hexanediol, caprylyl glycol, dipropylene glycol, glycerin, diglycerin, pentylene glycol, polyethylene glycol, and mixtures thereof, Preferred for use in the present composition are glycerin, propylene glycol.
表面活性剂Surfactant
本发明组合物中的表面活性剂为山梨坦硬脂酸酯/蔗糖椰油酸酯，其按所述组合物的重量计约0.01%至10%，优选约为0.01%至8%，更优选约0.01%至6%。本发明组合物山梨坦硬脂酸酯/蔗糖椰油酸酯，是一种天然糖苷的液晶乳化剂，温和无刺激，能形成液晶结构，带给肌肤丝一般的肤感。The surfactant in the compositions of the present invention is sorbitan stearate/sucrose cocoate at about 0.01% to 10% by weight of the composition, preferably at about 0.01% to 8%, more preferably About 0.01% to 6%. The composition of the present invention, sorbitan stearate/sucrose cocoate, is a natural glycoside liquid crystal emulsifier, mild and non-irritating, capable of forming a liquid crystal structure, and bringing silky skin feel to the skin.
增稠剂thickener
在一些实施方案中，本发明的组合物还可以包括一种或多种增稠剂，所述组合物包括按所述组合物的重量计约0.01%至10%，优选约为0.01%至8%，更优选约0.01%至6%的增稠剂。In some embodiments, the compositions of the present invention may also include one or more thickeners, the composition comprising from about 0.01% to 10%, preferably from about 0.01% to 8% by weight of the composition. %, more preferably from about 0.01% to 6% of thickener.
增稠剂的非限制性种类包括选自以下物质：羧酸聚合物（如Carbopol980）、交联聚丙烯酸酯聚合物、合成的高分子聚合物（如纤维素醚类）、天然的高分子聚合物（如树胶），优选的是丙烯酸交联聚合物，更优选的是按CTFA命名为卡波姆的物质。Non-limiting types of thickeners include substances selected from the following: carboxylic acid polymers (such as Carbopol 980), cross-linked polyacrylate polymers, synthetic polymers (such as cellulose ethers), natural polymers Substances such as gums, preferably acrylic crosslinked polymers, more preferably the CTFA nomenclature Carbomer.
皮肤调理剂skin conditioner
本发明组合物所添加的多种皮肤调理剂为水解珍珠、三色堇花提取物、番石榴果提取物、透明质酸钠。The various skin conditioning agents added to the composition of the present invention are hydrolyzed pearls, pansy flower extract, guava fruit extract, sodium hyaluronate.
本发明组合物的水解珍珠,其含量按本发明组合物的重量计约0.01%至10%，优选约为0.01%至8%，更优选约为0.01%至6%，其活性物含量按本发明组合物的重量计约0.001%至10%，优选约0.001%至8%，更优选约0.001%至6%。The hydrolyzed pearl of the composition of the present invention, its content is about 0.01% to 10% by weight of the composition of the present invention, preferably about 0.01% to 8%, more preferably about 0.01% to 6%. The inventive compositions comprise from about 0.001% to 10%, preferably from about 0.001% to 8%, more preferably from about 0.001% to 6%, by weight.
本发明组合物的水解珍珠，是通过珍珠粉的酶解工艺得到的，含有大量的钙离子和珍珠蛋白质，具有消除氧自由基，抗衰老作用，淡斑，使肌肤亮丽光泽。The hydrolyzed pearl of the composition of the present invention is obtained through the enzymatic hydrolysis process of pearl powder, contains a large amount of calcium ions and pearl protein, has the functions of eliminating oxygen free radicals, anti-aging, lightening spots, and making skin bright and lustrous.
本发明组合物添加的三色堇花提取物的含量按所述组合物的重量计优选为约0.01%至8%，更优选约0.01%至6%，本发明组合物的三色堇花提取物的活性含量按所述组合物的重量计优选约0.001%至8%，更优选约0.001%至6%。The content of the pansy flower extract added to the composition of the present invention is preferably about 0.01% to 8%, more preferably about 0.01% to 6%, by weight of the composition. The pansy flower extract of the composition of the present invention The active content of the compound is preferably from about 0.001% to 8%, more preferably from about 0.001% to 6%, by weight of the composition.
本发明组合物的三色堇花提取物，富含芸香甙，皂甙和维生素C、生育酚等。全面调理肌肤至水油平衡的健康状态，具有抗菌作用，明显的消痘功效。The pansy flower extract of the composition of the present invention is rich in rutin, saponin, vitamin C, tocopherol and the like. Fully regulate the skin to a healthy state of water and oil balance, has antibacterial effect, and has obvious anti-acne effect.
本发明组合物添加的番石榴果提取物的含量按所述组合物的重量计优选为约0.01%至8%，更优选约0.01%至6%，本发明组合物的番石榴果提取物的活性含量按所述组合物的重量计优选约0.001%至8%，更优选约0.001%至6%。The content of the guava fruit extract added to the composition of the present invention is preferably from about 0.01% to 8%, more preferably from about 0.01% to 6%, by weight of the composition, the guava fruit extract of the composition of the present invention The active level is preferably from about 0.001% to 8%, more preferably from about 0.001% to 6%, by weight of the composition.
本发明组合物的番石榴果提取物，富含维生素C、蛋白质、脂肪、维生素A、B类维生素、钙、磷、铁等微量元素，能有效中和自由基，促进新陈代谢，帮助肌肤排出“毒素”，即时发挥美白保湿功效。The guava fruit extract of the composition of the present invention is rich in vitamin C, protein, fat, vitamin A, B vitamins, calcium, phosphorus, iron and other trace elements, which can effectively neutralize free radicals, promote metabolism, and help the skin to discharge " toxins” and instantly exert the whitening and moisturizing effect.
本发明组合物的透明质酸钠，是一种仿生物黏糖，分子量大于100万，本发明组合物的透明质酸钠含量按发明组合物重量计约0.01%至10%，优选约0.01%至5%，更优选约为0.01%至3%。The sodium hyaluronate of the composition of the present invention is a kind of imitation bioglucose, the molecular weight is greater than 1 million, and the sodium hyaluronate content of the composition of the present invention is about 0.01% to 10% by weight of the composition of the invention, preferably about 0.01% to 5%, more preferably about 0.01% to 3%.
正常人皮肤角质层中含有10%至20%的水分，其对滋润皮肤，防止皮肤老化、防止外界环境的各种刺激都有重大作用。随着年龄的增长或环境的变化，水分会降到10%以下，皮肤会干燥，产生皱纹。本发明组合物的透明质酸钠可以缓解这一问题，它的理论保水值达1000ml/g，是人体皮肤中保水的关键成分，不但保湿效果好，而且无油腻感和堵塞毛孔的等缺点。还可以消除氧自由基，修复晒后损伤的皮肤。The stratum corneum of normal human skin contains 10% to 20% water, which plays an important role in moisturizing the skin, preventing skin aging, and preventing various stimuli from the external environment. As we grow older or the environment changes, the moisture content drops below 10%, and the skin becomes dry and wrinkled. The sodium hyaluronate in the composition of the present invention can alleviate this problem. Its theoretical water retention value reaches 1000ml/g, which is the key component of water retention in human skin. It can also eliminate oxygen free radicals and repair damaged skin after sun exposure.
抗氧化剂Antioxidants
本发明组合物的抗氧化剂为生育酚乙酸酯，其含量按发明组合物重量计约0.01%至10%，优选约0.01%至8%，更优选约为0.01%至6%。本发明组合物生育酚乙酸酯是维生素E类，可作为抗氧化剂，消除体内自由基，减少紫外线对人体的伤害。由于维生素E有较强的还原性，在人体新陈代谢过程中有抗氧化性而防止衰老的作用。The antioxidant of the composition of the present invention is tocopheryl acetate, and its content is about 0.01% to 10%, preferably about 0.01% to 8%, more preferably about 0.01% to 6% by weight of the composition of the invention. The tocopherol acetate in the composition of the present invention is vitamin E and can be used as an antioxidant to eliminate free radicals in the body and reduce the damage of ultraviolet rays to the human body. Because vitamin E has a strong reducing property, it has anti-oxidation and anti-aging effects in the process of human metabolism.
作为再优选，所述乳液组合物按质量百分比计由以下的组份构成：As another preference, the emulsion composition consists of the following components in terms of mass percentage:
上述的生育酚乙酸酯、杏仁油和氢化聚癸烯至少具有一种不为0；上述的三色堇花提取物、番石榴提取物和水解珍珠至少具有一种不为0。At least one of the above-mentioned tocopheryl acetate, almond oil and hydrogenated polydecene is not zero; at least one of the above-mentioned pansy flower extract, guava extract and hydrolyzed pearl is not zero.
为了实现上述的第二个目的，本发明采用了以下的技术方案：In order to achieve the above-mentioned second purpose, the present invention adopts the following technical solutions:
一种制备上述的润泽保湿乳液组合物的制备方法，该方法包括以下的步骤：A preparation method for preparing the above-mentioned moisturizing emulsion composition, the method comprises the following steps:
1）将油相物质混合，加热至70℃～90℃；1) Mix the oil phase substances and heat to 70°C to 90°C;
2）将水和水性物质混合，加热至70℃～90℃，至溶解；2) Mix water and water-based substances, heat to 70°C-90°C until dissolved;
3）油相入水相，均质，搅拌均匀，至40℃～60℃，加入其他组分，充分搅拌均匀，出料。3) Put the oil phase into the water phase, homogenize, stir evenly, until 40℃～60℃, add other components, fully stir evenly, and discharge.
本发明由于采用了上述的技术方案，产品在使用后，该润泽保湿乳液组合物可向皮肤补充水分，促进皮肤微循环，对抗氧自由基，延缓皮肤衰老。Because the present invention adopts the above-mentioned technical scheme, after the product is used, the moisturizing lotion composition can replenish moisture to the skin, promote skin microcirculation, resist oxygen free radicals, and delay skin aging.
具体实施方式Detailed ways
本发明的制备过程是将各成分混合至比较均一的状态，步骤为：The preparation process of the present invention is to mix each component to a relatively uniform state, and the steps are:
1.油相混合，加热至80℃左右；1. Mix the oil phase and heat to about 80°C;
2.水、山梨坦硬脂酸酯/蔗糖椰油酸酯、透明质酸钠、卡波姆、丙二醇、甘油，混合，加热至80℃，至溶解；2. Mix water, sorbitan stearate/sucrose cocoate, sodium hyaluronate, carbomer, propylene glycol, glycerin, and heat to 80°C until dissolved;
3.油相入水相，均质，搅拌均匀；3. Put the oil phase into the water phase, homogenize and stir evenly;
4.至50℃左右，加入其他组分，充分搅拌均匀，出料；4. To about 50°C, add other components, stir well, and discharge;
5.贮存→半成品检验→灌装→成品检验→入库。5. Storage→semi-finished product inspection→filling→finished product inspection→warehousing.
具体实施例：Specific examples:
相1放入容器中混合，加热至80℃；相2放入另一容器中加热至80℃；相1加入相2，乳化，均质，搅拌均匀，降温至50℃，加入相3，搅拌均匀后，出料。Mix phase 1 in a container and heat to 80°C; put phase 2 into another container and heat to 80°C; add phase 1 to phase 2, emulsify, homogenize, stir evenly, cool down to 50°C, add phase 3, stir After uniformity, discharge.
测试方法：Test Methods:
为了测试本发明的补水、调理效果，进行了试用调查实验：In order to test the present invention's water replenishment and conditioning effect, a trial investigation experiment has been carried out:
1、调查对象：各地区普通消费者50人，最后收回的试用情况反馈表43份；1. Survey objects: 50 ordinary consumers in various regions, and 43 trial feedback forms were finally collected;
2、调查时间：2008年12月10日-2009年2月10日；2. Investigation time: December 10, 2008-February 10, 2009;
3、使用产品：1号产品为依照本发明的配方制备的产品；2号产品为竞争厂家类似产品；3. Products used: No. 1 product is a product prepared according to the formula of the present invention; No. 2 product is a similar product of a competing manufacturer;
4、测试方法:测试者脸部清洁后，分别将1号产品和2号产品涂在左右两个脸颊上，观测和感受使用效果；4. Test method: After the tester's face is cleaned, apply No. 1 product and No. 2 product on the left and right cheeks respectively, and observe and feel the effect of use;
5、测试表格如下：5. The test form is as follows:
表1 1号产品的使用（60天）反馈总结表Table 1 Feedback summary table for the use of product No. 1 (60 days)
表2 2号产品使用（60天）反馈总结表Table 2 Feedback summary form of No. 2 product use (60 days)
表3 1号产品和2号产品的调理效果对比统计表格Table 3 Statistical Table of Conditioning Effect Comparison of No. 1 Product and No. 2 Product
表4 测试者推荐产品型号的统计表格Table 4 Statistical table of product models recommended by testers
6、反馈结论：6. Feedback conclusion:
测试者均表示，1号产品的补水效果优于2号产品，使用后也不粘腻，吸收快，皮肤迅速饱满水润。经常使用后，使用者表示1号产品的脸颊比2号产品的脸颊明显红润光泽，且回收的问卷中未有人有过敏现象。The testers all said that the hydrating effect of product No. 1 is better than that of product No. 2. It is not sticky after use, absorbs quickly, and the skin is quickly plumped and moisturized. After regular use, users said that the cheeks of product No. 1 were more rosy and shiny than those of product No. 2, and no one in the returned questionnaires had any allergies.
由表5可知，86.05%的人推荐使用1号产品，只有13.95%的人推荐使用2号产品。It can be seen from Table 5 that 86.05% of people recommend using No. 1 product, and only 13.95% of people recommend using No. 2 product.
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| CN101647760A (en) * | 2009-07-24 | 2010-02-17 | 张楚标 | Massage emulsion |
| CN101695467A (en) * | 2009-11-03 | 2010-04-21 | 广东名臣有限公司 | Skin-care composition containing poly alkylene glycol |
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| CN101647760A (en) * | 2009-07-24 | 2010-02-17 | 张楚标 | Massage emulsion |
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Denomination of invention: Moisturizing and moisturizing lotion composition containing guava extract and hydrolyzed pearl Granted publication date: 20140604 Pledgee: Agricultural Bank of China Limited Deqing County sub branch Pledgor: OSMUN BIOLOGICAL Co.,Ltd. Registration number: Y2025980016527 |