CN103614950A - Electronic component packing paper and preparation method thereof - Google Patents
Electronic component packing paper and preparation method thereof Download PDFInfo
- Publication number
- CN103614950A CN103614950A CN201310612943.5A CN201310612943A CN103614950A CN 103614950 A CN103614950 A CN 103614950A CN 201310612943 A CN201310612943 A CN 201310612943A CN 103614950 A CN103614950 A CN 103614950A
- Authority
- CN
- China
- Prior art keywords
- preparation
- electronic component
- paper
- pulp
- softwood pulp
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 238000012856 packing Methods 0.000 title abstract 6
- 238000007731 hot pressing Methods 0.000 claims abstract description 23
- 229920000742 Cotton Polymers 0.000 claims abstract description 21
- 239000011122 softwood Substances 0.000 claims abstract description 20
- 229920002472 Starch Polymers 0.000 claims abstract description 10
- 125000002091 cationic group Chemical group 0.000 claims abstract description 10
- 238000009413 insulation Methods 0.000 claims abstract description 10
- 235000019698 starch Nutrition 0.000 claims abstract description 10
- 239000008107 starch Substances 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 9
- 238000005507 spraying Methods 0.000 claims abstract description 5
- 239000000126 substance Substances 0.000 claims abstract description 4
- 239000003973 paint Substances 0.000 claims abstract description 3
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 claims description 18
- 238000010009 beating Methods 0.000 claims description 12
- 239000007921 spray Substances 0.000 claims description 12
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 11
- 229910021653 sulphate ion Inorganic materials 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 10
- 238000004806 packaging method and process Methods 0.000 claims description 10
- 235000011037 adipic acid Nutrition 0.000 claims description 9
- 239000001361 adipic acid Substances 0.000 claims description 9
- 229920002635 polyurethane Polymers 0.000 claims description 8
- 239000004814 polyurethane Substances 0.000 claims description 8
- 239000002966 varnish Substances 0.000 claims description 8
- 230000009172 bursting Effects 0.000 claims description 7
- 239000004952 Polyamide Substances 0.000 claims description 6
- 230000004907 flux Effects 0.000 claims description 6
- 239000011268 mixed slurry Substances 0.000 claims description 6
- 229920002647 polyamide Polymers 0.000 claims description 6
- LRWZZZWJMFNZIK-UHFFFAOYSA-N 2-chloro-3-methyloxirane Chemical compound CC1OC1Cl LRWZZZWJMFNZIK-UHFFFAOYSA-N 0.000 claims description 4
- VILCJCGEZXAXTO-UHFFFAOYSA-N 2,2,2-tetramine Chemical compound NCCNCCNCCN VILCJCGEZXAXTO-UHFFFAOYSA-N 0.000 claims description 3
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 3
- 239000012153 distilled water Substances 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 229920000642 polymer Polymers 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 230000002194 synthesizing effect Effects 0.000 claims description 3
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 claims description 3
- 229960001124 trientine Drugs 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000011248 coating agent Substances 0.000 claims description 2
- 238000000576 coating method Methods 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 5
- -1 Alkyl Ketene Dimer Chemical compound 0.000 abstract description 2
- 239000000654 additive Substances 0.000 abstract description 2
- 229920000090 poly(aryl ether) Polymers 0.000 abstract 2
- 238000002955 isolation Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 239000000758 substrate Substances 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 239000005022 packaging material Substances 0.000 description 3
- 239000000835 fiber Substances 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229920003656 Daiamid® Polymers 0.000 description 1
- 241000192783 Hakea sericea Species 0.000 description 1
- 241000218652 Larix Species 0.000 description 1
- 235000005590 Larix decidua Nutrition 0.000 description 1
- 241000351396 Picea asperata Species 0.000 description 1
- 235000011615 Pinus koraiensis Nutrition 0.000 description 1
- 240000007263 Pinus koraiensis Species 0.000 description 1
- 235000011609 Pinus massoniana Nutrition 0.000 description 1
- 241000018650 Pinus massoniana Species 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000002688 persistence Effects 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
Landscapes
- Paper (AREA)
Abstract
The invention discloses an electronic component packing paper. The electronic component packing paper has a density of 50-60g/m<2>, a thickness of 0.21-0.28mm, a tensile strength of 2.15-2.50kN/m, a breakage resistance of 90.4-107.3kPa, a tear resistance of 190-215mN, a resistance of 1.5*1011-3.7*1011 Ohm/cm and a good insulation effect. A preparation method of the electronic component packing paper comprises the steps of mixing softwood pulp with cotton pulp, adding PAE (Polyarylether), AKD (Alkyl Ketene Dimer) and cationic starch as chemical additives, forming paper through a wet papermaking process and then spraying an isolation paint layer on the surface of the paper, subsequently, carrying out hot pressing and preparing the electronic component packing paper with good insulation effect. The electronic component packing paper is simple in preparation process, good in paper flexibility, easy to pack, good in insulation effect and capable of protecting the electronic component fully.
Description
Technical field
The invention belongs to pulp technology for making paper, particularly a kind of electronic component packaging paper using and preparation method thereof.
Background technology
Along with the fast development of electronics industry, electronic circuit board integrated level is more and more higher, and the high density of electronic devices and components on motherboard is, the compactness of wiring, the even extensive employing of surface-adhered type element all easily cause electrostatic damage circuit board.Studies have found that the integrated circuit breaking down has 1st/3rd, is punctured by static discharge.Electronics industry is badly in need of having the packaging material of anti-static function.
Early stage antistatic packaging material adopts completion method, graphite or metal fibre is mixed in plastics, forms the wire netting of conduction in plastics inner.The metal web forming on this ambroin can provide goodish shielding when low frequency (< 100MHz), and when frequency higher (100～1000MHz), the inductive effect of the telegram in reply circulation flow path forming due to fiber web, its shield effectiveness reduces gradually.Therefore,, at the external coated and inner interpolation of material antistatic additive, the packaging material that reach electrostatic dissipation and shielding object by chemical technology more and more come into one's own.
Summary of the invention
In order to overcome the shortcoming of above-mentioned prior art, the object of the present invention is to provide a kind of electronic component packaging paper using and preparation method thereof, after adding PAE, AKD and cationic starch after utilizing bleached sulphate softwood pulp and cotton pulp to mix, prepare paper-based substrate, on paper substrate, spray polyurethane insulating varnish by hot-pressing processing, the electronic component packaging paper tensile strength of preparation is large, bursting strength, tearability are all higher, and insulation effect is good.
To achieve these goals, the technical solution used in the present invention is:
An electronic component packaging paper using is quantitatively 50～60g/m
2, thickness is 0.21～0.28mm, and tensile strength is 2.15～2.50kN/m, and bursting strength is 90.4～107.3kPa, and tearability is 190～215mN, resistance is 1.5 * 10
11～3.7 * 10
11Ω/cm.
The present invention provides the preparation method of described electronic component packaging paper using simultaneously, softwood pulp and cotton pulp are mixed, adding daiamid epoxy chloropropane (PAE), alkyl ketene dimer (AKD) and cationic starch is chemical assistant, after wet papermaking process becomes paper at its surface spraying insulation enamelled coating, then by making after hot-pressing processing.
Described softwood pulp is bleached sulphate softwood pulp, and making beating is to 30～40 ° of SR; Cotton pulp is commodity cotton pulp, and making beating is to 50～60 ° of SR.
After described softwood pulp and cotton pulp mix, the percentage by weight of softwood pulp is 80%～90%, the percentage by weight 10%～20% of cotton pulp.
The addition of described PAE, AKD and cationic starch is respectively 0.2%, 0.2% and 1% of mixed slurry gross weight.
The insulated paint of described surface spraying is polyurethane insulating varnish, and spray flux accounts for into 5%～10% of paper gross weight.
The condition of described hot-pressing processing is 105 ℃ of hot pressing temperatures, hot pressing time 20～30min.
Needlebush of the present invention can adopt as masson pine, larch, Korean pine, dragon spruce etc.
The preparation process of described PAE is: the ratio that is 1: 1.5: 1.02 in molar ratio by adipic acid, triethylene tetramine and p-methyl benzenesulfonic acid mixes, controlling temperature is 150～175 ℃, successive reaction synthesizing polyamides performed polymer, in synthetic polyamide prepolymer aggressiveness, add distilled water, after being cooled to 40 ℃, add methacrylic acid, its addition is 10% of adipic acid, after stirring, under constant voltage, drip epoxychloropropane, dripping quantity is 1.5 times of adipic acid, heating and thermal insulation regulates cessation reaction between pH value to 3～5 to make when viscosity reaches 100～150mPas.
Compared with prior art, the invention has the beneficial effects as follows:
(1) the electronic component packaging paper paper substrate making adopts wet papermaking process preparation, and technical maturity is convenient.
(2) both are in conjunction with tight after hot pressing on paper substrate, to spray polyurethane insulating varnish, and insulation effect persistence is better.In preparation process, cotton fiber accounts for major part, and the electronic component packaging paper making is soft, easy to use.
The specific embodiment
Below in conjunction with embodiment, describe embodiments of the present invention in detail.
Embodiment 1:
By bleached sulphate softwood pulp beating degree to 30 ° SR, commodity cotton pulp beating degree to 50 ° SR, mixes both, and bleached sulphate softwood pulp accounts for mixture total weight amount 80%, and commodity cotton pulp accounts for mixture total weight amount 20%; Add PAE, AKD and cationic starch, adding proportion is respectively 0.2%, 0.2% and 1% of mixed slurry gross weight; Through wet papermaking process, become paper rear surface spray polyurethane insulating varnish, spray flux accounts for into 5% of paper gross weight; Then through hot-pressing processing, 105 ℃ of hot pressing temperatures, hot pressing time 20min, gets product.
Gained finished product is quantitative 50～54g/m after measured
2, thickness 0.21～0.24mm, tensile strength 2.15～2.21kN/m, bursting strength 90.4～103.3kPa, tearability 197～210mN, resistance 1.5 * 10
11Ω/cm.
Embodiment 2:
By bleached sulphate softwood pulp beating degree to 40 ° SR, commodity cotton pulp beating degree to 60 ° SR, mixes both, and bleached sulphate softwood pulp accounts for mixture total weight amount 90%, and commodity cotton pulp accounts for mixture total weight amount 10%; Add PAE, AKD and cationic starch, adding proportion is respectively 0.2%, 0.2% and 1% of mixed slurry gross weight; Through wet papermaking process, become paper rear surface spray polyurethane insulating varnish, spray flux accounts for into 5% of paper gross weight; Then through hot-pressing processing, 105 ℃ of hot pressing temperatures, hot pressing time 30min, gets product.
Gained finished product is quantitative 53～56g/m after measured
2, thickness 0.21～0.25mm, tensile strength 2.19～2.37kN/m, bursting strength 95.4～101.3kPa, tearability 190～206mN, resistance 1.8 * 10
11Ω/cm.
Embodiment 3:
By bleached sulphate softwood pulp beating degree to 35 ° SR, commodity cotton pulp beating degree to 55 ° SR, mixes both, and bleached sulphate softwood pulp accounts for mixture total weight amount 80%, and commodity cotton pulp accounts for mixture total weight amount 20%; Add PAE, AKD and cationic starch, adding proportion is respectively 0.2%, 0.2% and 1% of mixed slurry gross weight; Through wet papermaking process, become paper rear surface spray polyurethane insulating varnish, spray flux accounts for into 10% of paper gross weight; Then through hot-pressing processing, 105 ℃ of hot pressing temperatures, hot pressing time 25min, gets product.
Gained finished product is quantitative 55～60g/m after measured
2, thickness 0.25～0.28mm, tensile strength 2.19～2.44kN/m, bursting strength 95.4～106.3kPa, tearability 197～215mN, resistance 3.6 * 10
11Ω/cm.
Embodiment 4:
By bleached sulphate softwood pulp beating degree to 30 ° SR, commodity cotton pulp beating degree to 60 ° SR, mixes both, and bleached sulphate softwood pulp accounts for mixture total weight amount 80%, and commodity cotton pulp accounts for mixture total weight amount 20%; Add PAE, AKD and cationic starch, adding proportion is respectively 0.2%, 0.2% and 1% of mixed slurry gross weight; Through wet papermaking process, become paper rear surface spray polyurethane insulating varnish, spray flux accounts for into 10% of paper gross weight; Then through hot-pressing processing, 105 ℃ of hot pressing temperatures, hot pressing time 20min, gets product.
Gained finished product is quantitative 55～60g/m after measured
2, thickness 0.25～0.28mm, tensile strength 2.19～2.44kN/m, bursting strength 95.4～106.3kPa, tearability 197～215mN, resistance 3.6 * 10
11Ω/cm.
Wherein in the present embodiment, the preparation process of described PAE is: the ratio that is 1: 1.5: 1.02 in molar ratio by adipic acid, triethylene tetramine and p-methyl benzenesulfonic acid mixes, controlling temperature is 175 ℃, successive reaction synthesizing polyamides performed polymer, in synthetic polyamide prepolymer aggressiveness, add distilled water, after being cooled to 40 ℃, add methacrylic acid, its addition is 10% of adipic acid, after stirring, under constant voltage, drip epoxychloropropane, dripping quantity is 1.5 times of adipic acid, heating and thermal insulation regulates pH value to 5 cessation reaction to make when viscosity reaches 150mPas.
Claims (8)
1. an electronic component packaging paper using, is characterized in that, is quantitatively 50～60g/m
2, thickness is 0.21～0.28mm, and tensile strength is 2.15～2.50kN/m, and bursting strength is 90.4～107.3kPa, and tearability is 190～215mN, resistance is 1.5 * 10
11～3.7 * 10
11Ω/cm.
2. the preparation method of electronic component packaging paper using according to claim 1, it is characterized in that, softwood pulp and cotton pulp are mixed, and adding PAE, AKD and cationic starch is chemical assistant, after wet papermaking process becomes paper at its surface spraying insulation enamelled coating, then by making after hot-pressing processing.
3. preparation method according to claim 2, is characterized in that, described softwood pulp is bleached sulphate softwood pulp, and making beating is to 30～40 ° of SR; Cotton pulp is commodity cotton pulp, and making beating is to 50～60 ° of SR.
4. according to preparation method described in claim 2 or 3, it is characterized in that, after described softwood pulp and cotton pulp mix, the percentage by weight of softwood pulp is 80%～90%, the percentage by weight 10%～20% of cotton pulp.
5. preparation method according to claim 4, is characterized in that, the addition of described PAE, AKD and cationic starch is respectively 0.2%, 0.2% and 1% of mixed slurry gross weight.
6. preparation method according to claim 4, is characterized in that, the insulated paint of described surface spraying is polyurethane insulating varnish, and spray flux accounts for into 5%～10% of paper gross weight.
7. preparation method according to claim 4, is characterized in that, the hot pressing condition of employing is 105 ℃ of hot pressing temperatures, hot pressing time 20～30min.
8. preparation method according to claim 4, it is characterized in that, the preparation process of described PAE is: by adipic acid, triethylene tetramine and p-methyl benzenesulfonic acid are that the ratio of 1: 1.5: 1.02 mixes in molar ratio, controlling temperature is 150～175 ℃, successive reaction synthesizing polyamides performed polymer, in synthetic polyamide prepolymer aggressiveness, add distilled water, after being cooled to 40 ℃, add methacrylic acid, its addition is 10% of adipic acid, after stirring, under constant voltage, drip epoxychloropropane, dripping quantity is 1.5 times of adipic acid, heating and thermal insulation, when reaching 100～150mPas, viscosity regulate cessation reaction between pH value to 3～5 to make.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310612943.5A CN103614950B (en) | 2013-11-26 | 2013-11-26 | A kind of electronic component packaging paper using and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310612943.5A CN103614950B (en) | 2013-11-26 | 2013-11-26 | A kind of electronic component packaging paper using and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103614950A true CN103614950A (en) | 2014-03-05 |
| CN103614950B CN103614950B (en) | 2016-01-13 |
Family
ID=50165665
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310612943.5A Active CN103614950B (en) | 2013-11-26 | 2013-11-26 | A kind of electronic component packaging paper using and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103614950B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105648825A (en) * | 2016-01-07 | 2016-06-08 | 仙鹤股份有限公司 | Cotton paper for conveying electronic element and producing process of cotton paper |
| CN106835811A (en) * | 2017-03-06 | 2017-06-13 | 陕西科技大学 | A kind of polyamine epichlorohydrin resin self-crosslinking polyester fiber paper and preparation method thereof |
| CN111663353A (en) * | 2020-05-15 | 2020-09-15 | 仙鹤股份有限公司 | High-flexibility cotton paper and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0482631A1 (en) * | 1990-10-26 | 1992-04-29 | Mitsubishi Paper Mills, Ltd. | Process for producing alkaline paper |
| JPH04180059A (en) * | 1990-11-15 | 1992-06-26 | Mitsubishi Paper Mills Ltd | Production of paper for photographic printing paper |
| WO1997035068A1 (en) * | 1996-03-21 | 1997-09-25 | Betzdearborn Inc. | Paper size and paper sizing process |
| US20040118538A1 (en) * | 2002-07-15 | 2004-06-24 | Ralph Cilevitz | Novel paper having low lint and/or anti-static |
| JP4377423B2 (en) * | 2007-05-30 | 2009-12-02 | 大王製紙株式会社 | Production method of conductive / rust-proof paper |
-
2013
- 2013-11-26 CN CN201310612943.5A patent/CN103614950B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0482631A1 (en) * | 1990-10-26 | 1992-04-29 | Mitsubishi Paper Mills, Ltd. | Process for producing alkaline paper |
| JPH04180059A (en) * | 1990-11-15 | 1992-06-26 | Mitsubishi Paper Mills Ltd | Production of paper for photographic printing paper |
| WO1997035068A1 (en) * | 1996-03-21 | 1997-09-25 | Betzdearborn Inc. | Paper size and paper sizing process |
| US20040118538A1 (en) * | 2002-07-15 | 2004-06-24 | Ralph Cilevitz | Novel paper having low lint and/or anti-static |
| JP4377423B2 (en) * | 2007-05-30 | 2009-12-02 | 大王製紙株式会社 | Production method of conductive / rust-proof paper |
Non-Patent Citations (1)
| Title |
|---|
| 吴芳: ""聚酰胺环氧氯丙烷的合成、改性及在造纸上得应用"", 《中国学位论文全文数据库》, 22 December 2010 (2010-12-22), pages 19 - 30 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105648825A (en) * | 2016-01-07 | 2016-06-08 | 仙鹤股份有限公司 | Cotton paper for conveying electronic element and producing process of cotton paper |
| CN106835811A (en) * | 2017-03-06 | 2017-06-13 | 陕西科技大学 | A kind of polyamine epichlorohydrin resin self-crosslinking polyester fiber paper and preparation method thereof |
| CN111663353A (en) * | 2020-05-15 | 2020-09-15 | 仙鹤股份有限公司 | High-flexibility cotton paper and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103614950B (en) | 2016-01-13 |
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Address after: 324400 No. 37 Jinxing Road, Longyou Industrial Zone, Longyou County, Quzhou, Zhejiang Applicant after: ZHEJIANG JINCHANG SPECIALTY PAPER CO., LTD. Address before: 324400 No. 37 Jinxing Road, Longyou Industrial Zone, Longyou County, Quzhou, Zhejiang Applicant before: Zhejiang Jinchang Paper Industry Co., Ltd. |
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Effective date of registration: 20210305 Address after: No.5, Maosheng Road, industrial park, Longyou County, Quzhou City, Zhejiang Province 324400 Patentee after: ZHEJIANG JINZE PAPER TECHNOLOGY Co.,Ltd. Address before: No. 37, Jinxing Avenue, Longyou Industrial Zone, Longyou County, Quzhou City, Zhejiang Province 324400 Patentee before: ZHEJIANG JINCHANG SPECIALTY PAPER Co.,Ltd. |