CN114720853A - Failure analysis method for laminated chip packaging product - Google Patents
Failure analysis method for laminated chip packaging product Download PDFInfo
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- G01R31/00—Arrangements for testing electric properties; Arrangements for locating electric faults; Arrangements for electrical testing characterised by what is being tested not provided for elsewhere
- G01R31/28—Testing of electronic circuits, e.g. by signal tracer
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- G01R31/00—Arrangements for testing electric properties; Arrangements for locating electric faults; Arrangements for electrical testing characterised by what is being tested not provided for elsewhere
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Abstract
Description
技术领域technical field
本发明属于芯片封装失效分析技术领域,具体涉及一种叠层芯片封装产品失效分析方法。The invention belongs to the technical field of chip packaging failure analysis, and in particular relates to a failure analysis method for stacked chip packaging products.
背景技术Background technique
在叠层芯片封装产品失效分析中,对芯片尺寸长宽比值较大,芯片厚度较薄的叠层芯片封装产品,通常采用P-Lapping磨抛剥离方法分析每层芯片失效缘由,该方法存在耗时较长的问题,且随着芯片厚度的减小,P-Lapping磨抛剥离要求越高,该方法中人为造成芯片破损的风险性越大;现有技术中,部分研究者采用酸/碱煮方法实现全开封,该方法存在与塑封料发生剧烈的化学反应,造成芯片受力不均,芯片破损,如图9所示,且存在由于芯片结构的复杂性、材质的多样性(如砷化镓/氮化硅),酸或碱会侵蚀芯片,干扰失效分析结论的准确性。因此,亟需一种针对叠层芯片封装产品新的失效分析方法来弥补现有技术的不足。In the failure analysis of laminated chip packaging products, for laminated chip packaging products with large chip size aspect ratio and thin chip thickness, the P-Lapping grinding and polishing method is usually used to analyze the failure cause of each layer of chips. In addition, as the thickness of the chip decreases, the higher the requirements for P-Lapping grinding and polishing, the greater the risk of artificially causing chip damage in this method; in the prior art, some researchers use acid/alkali The boiling method achieves full opening. This method has a violent chemical reaction with the plastic sealing compound, resulting in uneven stress on the chip and damage to the chip, as shown in Figure 9, and due to the complexity of the chip structure and the diversity of materials (such as arsenic gallium nitride/silicon nitride), acids or bases will corrode the chip and interfere with the accuracy of failure analysis conclusions. Therefore, there is an urgent need for a new failure analysis method for stacked chip packaging products to make up for the deficiencies of the prior art.
发明内容SUMMARY OF THE INVENTION
本发明的目的在于针对上述现有技术中的问题,提供一种叠层芯片封装产品失效分析方法,使得芯片在无化学腐蚀或人为破损等二次破坏作用下,实现观察和分析芯片失效原因。The purpose of the present invention is to solve the above problems in the prior art, and provide a method for analyzing the failure of laminated chip packaging products, so that the chip can observe and analyze the failure cause of the chip without secondary damage such as chemical corrosion or artificial damage.
为达到上述目的,本发明采用的技术方案是:To achieve the above object, the technical scheme adopted in the present invention is:
一种叠层芯片封装产品失效分析方法,包括将塑封后的叠层芯片封装产品放置于加热设备中;设定温度曲线并加热烘烤,烘烤预设时间后,将叠层芯片封装产品取出,分离出各层芯片,进行芯片异常判断分析。A method for analyzing the failure of a laminated chip package product, comprising placing the plastic-encapsulated laminated chip package product in a heating device; setting a temperature curve and heating and baking, and after baking for a preset time, the laminated chip package product is taken out , separate the chips of each layer, and conduct chip abnormality judgment and analysis.
进一步的,在所述叠层芯片封装产品放置于加热设备中时,首先将所述叠层芯片封装产品放置在托盘上,放置时,将叠层芯片封装产品的塑封面朝上;然后,将所述托盘置于加热设备的恒温区。Further, when the stacked chip package product is placed in the heating device, first place the stacked chip package product on the tray, and when placing, turn the plastic surface of the stacked chip package product upward; then, place the stacked chip package product on the tray. The tray is placed in the constant temperature zone of the heating device.
进一步的,所述温度曲线设置为升温段、保温段和降温段;在升温段,叠层芯片封装产品温度随加热设备温度的升高而逐渐增加;在降温段,叠层芯片封装产品温度随加热设备温度的降低而逐渐降低。Further, the temperature curve is set to a heating section, a heat preservation section and a cooling section; in the heating section, the temperature of the laminated chip package product gradually increases with the increase of the temperature of the heating equipment; in the cooling section, the temperature of the laminated chip package product increases with the increase of the temperature. The temperature of the heating equipment decreases gradually.
进一步的,在所述升温段,升温斜率≤30℃/min;在保温段,温度保持在500~805℃,保温时间为2~4h;在降温段,降温斜率≤30℃/min。Further, in the heating section, the heating slope is ≤30°C/min; in the holding section, the temperature is maintained at 500-805°C, and the holding time is 2-4 hours; in the cooling section, the cooling slope is ≤30°C/min.
进一步的,当叠层芯片封装产品芯片长宽比>1,或叠层层数≥四层,或芯片厚度≤100μm,或芯片之间粘结材料热膨胀系数与芯片热膨胀系数比值≥50时,在所述叠层芯片封装产品放置于加热设备前,进行叠层芯片封装产品塑封材料的预处理。Further, when the aspect ratio of the laminated chip package product is greater than 1, or the number of laminated layers is greater than or equal to four layers, or the thickness of the chip is less than or equal to 100 μm, or the ratio of the thermal expansion coefficient of the bonding material between the chips to the thermal expansion coefficient of the chip is greater than or equal to 50, the Before the stacked chip package product is placed in the heating device, pretreatment of the plastic sealing material of the stacked chip package product is performed.
进一步的,所述预处理包括以下步骤:Further, the preprocessing includes the following steps:
步骤1:将叠层芯片封装产品采用化学法或物理法进行塑封材料的去除;Step 1: Use chemical or physical methods to remove the plastic packaging material for the laminated chip packaging product;
步骤2:然后采用清洗或气枪吹的方式去除塑封材料残屑,若发现未清洗干净,返回步骤1;Step 2: Then use cleaning or air gun blowing to remove the plastic sealing material residue. If it is found that it is not cleaned, go back to
步骤3:烘烤干燥即可。Step 3: Bake and dry.
进一步的,所述步骤1中将叠层芯片封装产品进行塑封材料去除前,预先进行封装产品预烘烤;所述物理法为采用激光开封机进行塑封材料的去除;化学法为采用酸、碱或有机溶解剂进行塑封材料的去除。Further, in the
进一步的,所述步骤2中清洗采用丙酮、水、水、丙酮依次清洗的方式。Further, the cleaning in the
进一步的,所述步骤3中烘烤干燥为气枪吹干或在加热设备中烘烤。Further, the baking and drying in the
进一步的,所述酸为发烟硝酸或浓硫酸,所述碱为氢氧化钾,所述有机溶解剂为树脂溶解剂。Further, the acid is fuming nitric acid or concentrated sulfuric acid, the alkali is potassium hydroxide, and the organic dissolving agent is a resin dissolving agent.
与现有技术相比,本发明具有以下有益效果:Compared with the prior art, the present invention has the following beneficial effects:
本发明基于材料热膨胀性及有机物分解机理,通过高温碳化分解有机物,使得在无化学腐蚀或人为破损等二次破坏作用下,提取芯片并进行异常分析和判断。本发明所采用的技术方案是利用叠层芯片封装产品芯片之间粘结剂,如粘片胶/贴片胶/DAF/塑封料等有机物碳化分解温度来使除芯片外的有机物碳化分解,利用芯片上下面物质热膨胀性使芯片在最小影响下还原塑封前芯片原始状貌,从而进行芯片异常判断,实验证明针对不同封装产品可以采取烘烤法实现芯片原始异常失效分析。Based on the thermal expansion of materials and the decomposition mechanism of organic matter, the invention decomposes organic matter through high temperature carbonization, so that chips can be extracted and abnormal analysis and judgment are performed without secondary damage such as chemical corrosion or artificial damage. The technical scheme adopted in the present invention is to use the adhesive between the chips of the laminated chip package product, such as the carbonization and decomposition temperature of organic matter such as adhesive/patch glue/DAF/plastic encapsulation material, to carbonize and decompose the organic matter other than the chips. The thermal expansion of the material above and below the chip enables the chip to restore the original appearance of the chip before plastic packaging with minimal influence, so as to judge the abnormality of the chip.
进一步的,通过将温度曲线设置为升温段、保温段和降温段,使得高温碳化分解有机物时,减小了有机物迅速热膨胀对芯片造成破损的风险。Further, by setting the temperature curve into a heating section, a heat preservation section and a cooling section, the risk of damage to the chip caused by rapid thermal expansion of the organic matter is reduced when the organic matter is decomposed by high temperature carbonization.
进一步的,通过对芯片长宽比>1,或叠层层数≥四层,或芯片厚度≤100μm,或芯片之间粘结材料热膨胀系数与芯片热膨胀系数比值≥50的叠层芯片封装产品进行塑封材料预处理,由于上述情况下叠层芯片封装产品自身抗弯强度较低,进行预处理可以降低热膨胀系数差异对芯片的拉压应力,进一步降低了芯片破损风险。Further, through the chip length-width ratio > 1, or the number of laminated layers ≥ four layers, or the chip thickness ≤ 100 μm, or the ratio of the thermal expansion coefficient of the bonding material between the chips to the chip thermal expansion coefficient ≥ 50. In the pretreatment of plastic packaging materials, due to the low bending strength of the laminated chip packaging product itself in the above situation, pretreatment can reduce the tensile and compressive stress of the chip caused by the difference in thermal expansion coefficient, and further reduce the risk of chip damage.
附图说明Description of drawings
图1是加热设备示意图;Fig. 1 is the schematic diagram of heating equipment;
图2是温度曲线设置图;Figure 2 is a temperature curve setting diagram;
图3是基板类封装产品图;Figure 3 is a diagram of a substrate package product;
图4是框架类封装产品图;Figure 4 is a diagram of a frame package product;
图5是基板类多层平齐堆叠封装产品图;Figure 5 is a product diagram of a substrate-type multi-layer flush stack packaging product;
图6是基板类多层错开堆叠封装产品图;Figure 6 is a product diagram of a substrate-type multi-layer staggered stack packaging product;
图7是基板类和框架类封装产品芯片分离效果图;Figure 7 is the effect diagram of chip separation of substrate type and frame type package products;
图8是基板类多层平齐和错开堆叠封装产品芯片分离效果图;Figure 8 is a diagram showing the effect of chip separation of substrate-based multilayer flush and staggered stack packaging products;
图9是基板类多层平齐堆叠封装产品采用酸煮方法芯片破损效果图;FIG. 9 is a diagram showing the chip damage effect of the substrate-type multi-layer flush stack packaging product using the acid boiling method;
其中:1-锡球;2-基板;3-粘片胶/贴片胶/DAF;4-芯片;5-塑封料;6-金属衬底;7-框架;9-加热设备舱门;10-加热区;11-恒温区。Among them: 1-solder ball; 2-substrate; 3-adhesive/SMD adhesive/DAF; 4-chip; 5-plastic compound; 6-metal substrate; 7-frame; 9-heating equipment door; 10 - Heating zone; 11- Constant temperature zone.
具体实施方式Detailed ways
为了使本发明所述的内容更加便于理解,下面结合附图对本发明针对叠层芯片封装产品失效分析的方法做进一步详细描述,但是本发明不仅限于此。In order to make the content of the present invention easier to understand, the method for failure analysis of stacked chip packaging products of the present invention will be described in further detail below with reference to the accompanying drawings, but the present invention is not limited thereto.
一种叠层芯片封装产品失效分析方法,包括将塑封后的叠层芯片封装产品放置于加热设备中,如图1所示,加热设备包括壳体,壳体上设置加热设备舱门9,壳体内设置加热区10,加热区10内设有恒温区11;在叠层芯片封装产品放置于加热设备中时,首先将叠层芯片封装产品放置在托盘上,放置时,将叠层芯片封装产品的塑封面朝上;然后,将托盘置于加热设备的恒温区11;然后设置温度曲线并加热烘烤,烘烤预设时间后,将产品取出,分离出各层芯片,进行芯片异常判断分析。优选的,温度曲线设置为升温段、保温段和降温段;在升温段,叠层芯片封装产品温度随加热设备温度8的升高而逐渐增加;在降温段,叠层芯片封装产品温度随加热设备温度的降低而逐渐降低;优选的,在升温段,升温斜率≤30℃/min;在保温段,温度保持在500~805℃,保温时间为2~4h;在降温段,降温斜率≤30℃/min。A method for failure analysis of a laminated chip package product, comprising placing the plastic-encapsulated laminated chip package product in a heating device, as shown in FIG. A
当叠层芯片封装产品芯片长宽比>1,或叠层层数≥四层,或芯片厚度≤100μm,或芯片之间粘结材料热膨胀系数与芯片热膨胀系数比值≥50时,在叠层芯片封装产品放置于加热设备前,进行叠层芯片封装产品塑封材料的预处理。When the aspect ratio of the laminated chip package product is greater than 1, or the number of laminated layers is greater than or equal to four layers, or the thickness of the chip is less than or equal to 100 μm, or the ratio of the thermal expansion coefficient of the bonding material between the chips to the thermal expansion coefficient of the chip is greater than or equal to 50, the laminated chip Before the packaged product is placed in the heating equipment, the pretreatment of the plastic sealing material of the stacked chip packaged product is performed.
预处理包括以下步骤:Preprocessing includes the following steps:
步骤1:将叠层芯片封装产品采用化学法或物理法进行塑封材料的去除;优选的,在进行塑封材料去除前,预先进行封装产品预烘烤;物理法为采用激光开封机进行塑封材料的去除;化学法为采用酸、碱或有机溶解剂进行塑封材料的去除,优选的,酸采用发烟硝酸或浓硫酸,碱采用氢氧化钾,有机溶解剂采用树脂溶解剂。Step 1: Use a chemical method or a physical method to remove the plastic packaging material of the laminated chip packaging product; preferably, before removing the plastic packaging material, pre-bake the packaging product in advance; the physical method is to use a laser unsealing machine to remove the plastic packaging material. Removal; chemical method is to use acid, alkali or organic dissolving agent to remove the plastic sealing material, preferably, the acid is fuming nitric acid or concentrated sulfuric acid, the alkali is potassium hydroxide, and the organic dissolving agent is resin dissolving agent.
步骤2:然后采用清洗或气枪吹的方式去除塑封材料残屑,优选的,清洗采用丙酮、水、水、丙酮依次清洗的方式。若发现未清洗干净,返回步骤1;Step 2: Then, the plastic sealing material residue is removed by cleaning or air gun blowing. Preferably, cleaning is performed by acetone, water, water, and acetone in sequence. If it is found that it is not cleaned, go back to
步骤3:烘烤干燥即可,烘烤干燥优选气枪吹干或在加热设备中烘烤。Step 3: Bake and dry, preferably air gun drying or baking in heating equipment.
下面以基板类封装产品、框架类封装产品、基板类多层平齐堆叠封装产品以及基板类多层错开堆叠封装产品为例详细说明本发明的失效分析方法。Hereinafter, the failure analysis method of the present invention will be described in detail by taking substrate-type package products, frame-type package products, substrate-type multi-layer flush-stack package products, and substrate-type multi-layer staggered-stack package products as examples.
图3所示为基板类封装产品,该产品包括基板2、锡球1,基板2的上表面由下到上依次设置粘片胶/贴片胶/DAF3、芯片4、粘片胶/贴片胶/DAF 3以及芯片4,整体通过塑封料5包裹,该产品芯片长宽比大于1,叠层层数为2。如图4所示为框架类封装产品,该产品包括框架7、金属衬底6,金属衬底6的上表面由下到上依次设置粘片胶/贴片胶/DAF3、芯片4、粘片胶/贴片胶/DAF 3以及芯片4,整体通过塑封料5包裹,该产品芯片长宽比大于1,叠层层数为2。Figure 3 shows a substrate package product, which includes a
在针对上述封装产品进行失效分析时,首先选取基板类封装产品样品1#和样品2#;选取框架类封装产品样品3#和样品4#,将样品1#、样品2#、样品3#和样品4#分别放置于加热设备中烘烤,在放置于加热设备中时,首先将上述样品放置在托盘上,放置时,将样品的塑封面朝上;然后,将托盘置于加热设备的恒温区11;加热时,温度曲线设置为:以10℃/min的速度从室温匀速升温至500℃,在500℃保持120min,然后以10℃/min的速度匀速降温至室温,如图2所示;在升温段,样品温度随加热设备温度的升高而逐渐增加;在降温段,样品温度随加热设备温度的降低而逐渐降低。待烘烤结束后,将各样品取出,分离出各层芯片,进行芯片异常判断分析。In the failure analysis of the above packaged products, firstly select
图7为样品1#、样品2#、样品3#和样品4#各层芯片分离结果,图7中1、2代表各样品第一层和第二层分离的芯片。可见,本发明实施例提供的失效分析方法基于材料热膨胀性及有机物分解机理,通过高温碳化分解有机物,使得在无化学腐蚀或人为破损等二次破坏作用下,能实现完好分离出各层芯片,分离出的芯片无崩边、崩角、裂片等现象。Figure 7 shows the chip separation results of
如图5所示为基板类多层平齐堆叠封装产品,该产品包括基板2、锡球1,基板2的上表面由下到上依次设置粘片胶/贴片胶/DAF 3、芯片4、粘片胶/贴片胶/DAF 3、芯片4、粘片胶/贴片胶/DAF 3、芯片4、粘片胶/贴片胶/DAF 3、芯片4,基板2上部整体通过塑封料5包裹,该产品的叠层层数为4。图6所示为基板类多层错开堆叠封装产品,该产品包括基板2、锡球1,基板2的上表面设置粘片胶/贴片胶/DAF 3,粘片胶/贴片胶/DAF 3上设置芯片4,芯片4上部交错设置两个叠层,叠层包括粘片胶/贴片胶/DAF 3和粘片胶/贴片胶/DAF 3上部设置的芯片4,基板2上部整体通过塑封料5包裹,该产品的叠层层数为4。图5和图6所示产品芯片之间粘结材料热膨胀系数与芯片热膨胀系数比值为66.7。上述产品失效分析方法包括以下步骤:As shown in Figure 5, it is a substrate-type multi-layer flush stacking package product. The product includes a
步骤一:首先选取基板类多层平齐堆叠封装产品样品1#、样品2#、样品3#以及样品4#;选取基板类多层错开堆叠封装产品样品5#、样品6#、样品7#和样品8#;将上述样品在60~130℃下预烘烤,采用浓硫酸将塑封料5去除;Step 1: First,
步骤二:采用丙酮-水-水-丙酮依次清洗方式清洗除去塑封料5,并观察芯片上方塑封料5是否清洗干净,若发现未清洗干净,返回步骤1;Step 2: Use the acetone-water-water-acetone cleaning method to clean and remove the
步骤三:在60~130℃下烘烤上述样品直至除去样品内部大部分水汽;Step 3: Bake the above sample at 60-130°C until most of the water vapor inside the sample is removed;
步骤四:将各样品放置于加热设备中烘烤,在放置于加热设备中时,首先将各样品放置在托盘上,放置时,将各样品的塑封面朝上;然后,将托盘置于加热设备的恒温区11,设置加热设备的温度曲线,温度曲线设置为升温段、保温段和降温段;在升温段,样品三和样品四温度随加热设备温度的升高而逐渐增加;在降温段,样品三和样品四温度随加热设备温度的降低而逐渐降低。如图2所示,温度曲线设置为:以10℃/min的速度从室温匀速升温至500℃,在500℃保持120min,然后以10℃/min的速度匀速降温至室温;Step 4: Place each sample in a heating device for baking. When placing it in the heating device, first place each sample on a tray, and place the plastic surface of each sample upward; then, place the tray on the heating device. In the
步骤五:待烘烤结束后,将各样品取出,分离出各层芯片,进行芯片异常判断分析。Step 5: After the baking is finished, each sample is taken out, the chips of each layer are separated, and the abnormality judgment and analysis of the chips are carried out.
图8为基板类多层平齐堆叠封装产品样品1#、样品2#、样品3#和样品4#,以及基板类多层错开堆叠封装产品样品5#、样品6#、样品7#和样品8#各层芯片分离结果。本发明实施例图5所示的基板类多层平齐堆叠封装产品以及图6所示的基板类多层错开堆叠封装产品叠层层数为4,图8中1、2、3、4代表各样品第一层、第二层、第三层以及第四层分离的芯片,芯片之间粘结材料热膨胀系数与芯片热膨胀系数比值为66.7,两个产品的自身抗弯强度较低,失效分析方法中首先进行了塑封材料预处理,可以降低热膨胀系数差异对芯片的拉压应力,进一步降低了芯片破损风险。从图8中可见,该方法能完好分离出各层芯片,且分离出的芯片无崩边、崩角、裂片等现象。Figure 8 shows the substrate-type multi-layer flush stack
然而,示例实施方式能够以多种形式实施,且不应被理解为限于在此阐述的实施方式,本领域的普通技术人员在本发明的启示下,在不脱离本发明宗旨和权利要求所保护的范围情况下,还可以做出很多形式,这些均属于本发明的保护范围之内。However, the example embodiments can be implemented in various forms, and should not be construed as limited to the embodiments set forth herein, those of ordinary skill in the art, under the inspiration of the present invention, without departing from the spirit of the present invention and the protection of the claims In the case of the scope of the present invention, many forms can also be made, which all fall within the protection scope of the present invention.
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