CN116439243A - Spinosad cockroach killing bait and preparation method thereof - Google Patents
Spinosad cockroach killing bait and preparation method thereof Download PDFInfo
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Abstract
本发明涉及一种多杀菌素杀蟑饵剂及其制备方法，包括如下百分含量的各原料：多杀菌素2％；糖类0.10.3％；口感添加剂115％；香精0.10.5％；填充剂余量。所述糖类采用阿斯巴甜。所述口感添加剂包括滑石粉、单双甘油脂肪酸酯中的一种或几种。所述填充剂采用熟黄豆饼粉。本发明绿色、环保、可降解，不易吸潮结块，能够诱导蟑螂食用。The invention relates to a spinosyn cockroach-killing bait and a preparation method thereof, which comprises the following raw materials in percentage content: 2% spinosyn; 0.10.3% sugar; 115% mouthfeel additive; 0.10.5% essence; Filler balance. Described sugar adopts aspartame. The taste additive includes one or more of talcum powder and mono-diglyceride fatty acid esters. The filler is cooked soybean cake powder. The invention is green, environment-friendly, degradable, not easy to absorb moisture and agglomerate, and can induce cockroaches to eat.
Description
技术领域technical field
本发明涉及生物农药技术领域，具体涉及一种多杀菌素杀蟑饵剂及其制备方法。The invention relates to the technical field of biological pesticides, in particular to a spinosad cockroach-killing bait and a preparation method thereof.
背景技术Background technique
蟑螂是家居常见昆虫，繁殖力强，取食品种复杂。蟑螂进食时，边吃、边吐、边排泄，导致污染食物，传播疾病，因此对于蟑螂的防治工作不能松懈。市售灭蟑药的杀虫成分大致包括吡虫啉，乙酰甲胺磷，氟虫腈，氟蚁腙，毒死蜱，呋虫胺，菊酯类，硼酸及PFDNV昆虫病毒等，相当一部分品种已经产生了抗性，为保护公众卫生健康，研发新品种的杀蟑剂势在必行。Cockroaches are common household insects with strong fecundity and complex food species. When cockroaches eat, they eat, vomit, and excrete, resulting in food contamination and disease transmission. Therefore, the prevention and control of cockroaches cannot be slack. The insecticidal ingredients of commercially available cockroach medicines generally include imidacloprid, acephate, fipronil, hydrazone, chlorpyrifos, dinotefuran, pyrethroids, boric acid and PFDNV insect virus, etc., and a considerable number of varieties have produced anti- In order to protect public health, it is imperative to develop new types of cockicides.
杀蟑螂剂需要需要克服的技术问题在于高效、低毒，不能在居室内引发难闻的气味和较高的农药残留；同时需要对蟑螂产生足够的吸引力，保证合适的取食率并保证活性原料药进入蟑螂体内后能够有足够的剂量以便杀死蟑螂。The technical problem that needs to be overcome by the cockroach killer is high efficiency, low toxicity, and can not cause unpleasant smell and high pesticide residue in the living room; at the same time, it needs to be attractive enough to cockroaches to ensure a suitable feeding rate and ensure activity After the raw material drug enters the cockroach body, it can have a sufficient dose to kill the cockroach.
多杀霉素又名多杀菌素(Spinosad)是在多刺甘蔗多孢菌(Saccharopolysporaspinosa)发酵液中提取的一种大环内酯类无公害高效生物杀虫剂，因其具有杀虫谱广、杀虫活性高、可降解，对益虫及哺乳动物相比其他农药安全的特性，已经逐渐在农药界开发使用。然而，在利用其制备杀蟑饵剂时，却由于其具有陈腐泥土的气味，被蟑螂所不喜，因此，研发一种多杀菌素杀蟑饵剂及其制备方法，能够引诱蟑螂食用多杀菌素显得至关重要。Spinosad, also known as spinosad (Spinosad), is a macrolide pollution-free and high-efficiency biopesticide extracted from the fermentation broth of Saccharopolysporaspinosa, because it has a wide insecticidal spectrum. , high insecticidal activity, degradable, and safe for beneficial insects and mammals compared to other pesticides, it has been gradually developed and used in the pesticide industry. However, when using it to prepare cockroach-killing bait, it is disliked by cockroaches because it has the smell of stale soil. Therefore, a kind of spinosad cockroach-killing bait and its preparation method are developed, which can lure cockroaches to eat multi-killing bait. element appears to be crucial.
发明内容Contents of the invention
本发明的目的在于克服现有技术的缺陷，提供了一种多杀菌素杀蟑饵剂及其制备方法，其绿色、环保、可降解，不易吸潮结块，能够诱导蟑螂食用。The purpose of the present invention is to overcome the defects of the prior art, and provide a spinosad cockroach-killing bait and a preparation method thereof, which is green, environmentally friendly, degradable, not easy to absorb moisture and agglomerate, and can induce cockroaches to eat.
为了实现上述目的，本发明采取的技术方案如下：In order to achieve the above object, the technical scheme that the present invention takes is as follows:
技术方案一：Technical solution one:
一种多杀菌素杀蟑饵剂，包括多杀菌素、糖类、口感添加剂、香精、填充剂；进一步的所述糖类优选自阿斯巴甜。A spinosad cockroach-killing bait, comprising spinosad, sugars, mouthfeel additives, flavors, and fillers; further, the sugars are preferably selected from aspartame.
进一步的，一种多杀菌素杀蟑饵剂，包括如下百分含量的各原料：Further, a spinosad cockroach-killing bait comprises the following raw materials in percentages:
进一步的，所述口感添加剂包括滑石粉、单双甘油脂肪酸酯中的一种或几种；优选的所述口感添加剂选自滑石粉、单双甘油脂肪酸酯或其组合；更优选的所述口感添加剂选自滑石粉和单双甘油脂肪酸酯的组合，且滑石粉和单双甘油脂肪酸酯的质量比为1525∶1。Further, the mouthfeel additive includes one or more of talcum powder, mono-diglyceride fatty acid ester; preferably the mouthfeel additive is selected from talcum powder, mono-diglyceride fatty acid ester or a combination thereof; more preferably all The taste additive is selected from the combination of talc powder and mono-diglyceride fatty acid ester, and the mass ratio of talc powder and mono-diglyceride fatty acid ester is 1525:1.
进一步的，所述香精采用奶味香精。Further, the essence adopts milk essence.
进一步的，所述填充剂采用熟黄豆饼粉。Further, the filler is cooked soybean cake powder.
进一步的，一种多杀菌素杀蟑饵剂，包括如下百分含量的各原料：Further, a spinosad cockroach-killing bait comprises the following raw materials in percentages:
技术方案二：Technical solution two:
一种所述多杀菌素杀蟑饵剂的制备方法，包括如下步骤：A preparation method of the spinosyn cockroach bait, comprising the steps of:
按比例称取各成分，混合并搅拌均匀后，置于超微气流粉碎机中粉碎，出料后继续搅拌至均匀，任选的过筛，即得多杀菌素杀蟑饵剂。The components are weighed in proportion, mixed and stirred uniformly, placed in an ultra-fine airflow pulverizer, pulverized, continuously stirred until uniform after discharging, and optionally sieved to obtain the multibactin cockroach-killing bait.
进一步的，采用超微气流粉碎机粉碎至粒径小于等于3微米。Further, it is pulverized to a particle size of less than or equal to 3 microns by using an ultrafine airflow pulverizer.
与现有技术相比，本发明所取得的有益效果如下：Compared with prior art, the beneficial effect that the present invention obtains is as follows:
本发明以多杀菌素作为杀蟑的有效药物成分，其杀虫谱广、杀虫活性高、可降解，对益虫及哺乳动物相比其他农药安全；本发明以阿斯巴甜代替传统糖类，使杀蟑饵剂不易吸潮结块。The present invention uses spinosad as an effective drug ingredient for killing cockroaches, which has a wide insecticidal spectrum, high insecticidal activity, and is degradable, and is safer for beneficial insects and mammals than other pesticides; the present invention uses aspartame to replace traditional sugars , so that the cockroach bait is not easy to absorb moisture and agglomerate.
滑石粉和单双甘油脂肪酸酯在食品和医药领域主要用作润滑剂，本发明通过添加滑石粉增加杀蟑饵剂的口柔滑感，并通过添加单双甘油脂肪酸酯改善其口感。Talcum powder and mono-diglyceride fatty acid esters are mainly used as lubricants in the food and medical fields. The present invention increases the mouthfeel of the cockroach-killing bait by adding talcum powder, and improves its mouthfeel by adding mono-diglyceride fatty acid esters.
本发明通过使用奶味香精使杀蟑饵剂具有浓厚的奶香味，能够掩盖多杀菌素本身的陈腐泥土的味道，本发明以熟黄豆饼作为填充剂，其散发的香味为大多数动物所喜爱，能够提高蟑螂的取食率。The invention makes the cockroach-killing bait have a strong milk flavor by using milk flavor essence, which can cover up the stale soil taste of spinosad itself. The invention uses cooked soybean cake as a filler, and its fragrance is loved by most animals , can increase the feeding rate of cockroaches.
具体实施方式Detailed ways
以下结合实施例对本发明进行进一步详细的叙述。Below in conjunction with embodiment the present invention is described in further detail.
在本发明中，In the present invention,
多杀菌素(含量99.1％)：陕西睿明德生物科技有限公司；Spinosyn (content 99.1%): Shaanxi Ruimingde Biotechnology Co., Ltd.;
吡虫啉原药(含量98.5％)：上海嘉利康生物科技有限公司；Technical imidacloprid (content 98.5%): Shanghai Jialikang Biotechnology Co., Ltd.;
氟蚁腙原药(含量95.2％)：济宁中坚化工有限公司；The original drug of hydrazone (content 95.2%): Jining Zhongjian Chemical Co., Ltd.;
其他辅料均为市售常规产品。Other auxiliary materials are commercially available conventional products.
实施例1Example 1
一种多杀菌素杀蟑饵剂，包括如下百分重量的各原料：A spinosad cockroach-killing bait comprises the following raw materials in percentage by weight:
上述多杀菌素杀蟑饵剂的制备方法，包括如下步骤：The preparation method of above-mentioned spinosyn cockroach bait comprises the following steps:
按比例称取各原料，混合并搅拌均匀后，置于超微气流粉碎机中粉碎至粒径小于等于3微米，出料后继续搅拌至均匀，即得多杀菌素杀蟑饵剂。其中，所述超微气流粉碎机(湖南创未来机电设备，QLF-50)的处理量为0.05-0.5kg/h，进料粒度为100-200目。Weigh each raw material in proportion, mix and stir evenly, place in an ultrafine jet mill and pulverize until the particle size is less than or equal to 3 microns, and continue stirring until uniform after discharging, that is, the multibactin cockroach-killing bait. Wherein, the processing capacity of the ultra-fine jet mill (Hunan Chuangfuli Electromechanical Equipment, QLF-50) is 0.05-0.5kg/h, and the feed particle size is 100-200 mesh.
实施例2Example 2
一种多杀菌素杀蟑饵剂，包括如下百分重量的各原料：A spinosad cockroach-killing bait comprises the following raw materials in percentage by weight:
上述多杀菌素杀蟑饵剂的制备方法包括的步骤，同实施例1。The steps included in the preparation method of the above spinosad cockroach bait are the same as in Example 1.
实施例3Example 3
一种多杀菌素杀蟑饵剂，包括如下百分重量的各原料：A spinosad cockroach-killing bait comprises the following raw materials in percentage by weight:
上述多杀菌素杀蟑饵剂的制备方法包括的步骤，同实施例1。The steps included in the preparation method of the above spinosad cockroach bait are the same as in Example 1.
对比例1Comparative example 1
一种吡虫啉杀蟑饵剂，包括如下百分重量的各原料：A kind of imidacloprid cockroach-killing bait, comprises each raw material of following percentage by weight:
上述吡虫啉杀蟑饵剂的制备方法，包括如下步骤：The preparation method of above-mentioned imidacloprid cockroach bait comprises the following steps:
按比例称取各原料，混合并搅拌均匀后，置于超微气流粉碎机中粉碎至粒径小于等于3微米，出料继续搅拌至均匀，即得吡虫啉杀蟑饵剂。其中，所述超微气流粉碎机(湖南创未来机电设备，QLF-50)的处理量为0.05-0.5kg/h，进料粒度为100-200目。The raw materials are weighed in proportion, mixed and stirred evenly, placed in an ultra-fine jet mill and pulverized until the particle size is less than or equal to 3 microns, and the discharged material is continuously stirred until uniform, and the imidacloprid cockroach-killing bait is obtained. Wherein, the processing capacity of the ultra-fine jet mill (Hunan Chuangfuli Electromechanical Equipment, QLF-50) is 0.05-0.5kg/h, and the feed particle size is 100-200 mesh.
对比例2Comparative example 2
一种氟蚁腙杀蟑饵剂，包括如下百分重量的各原料：A kind of hydrazone cockroach-killing bait, comprises each raw material of following percentage by weight:
上述氟蚁腙杀蟑饵剂的制备方法，包括如下步骤：The preparation method of above-mentioned hydrazone cockroach-killing bait comprises the following steps:
按比例称取各原料，混合并搅拌均匀后，置于超微气流粉碎机中粉碎至粒径小于等于3微米，出料后继续搅拌至均匀，即得氟蚁腙杀蟑饵剂。其中，所述超微气流粉碎机(湖南创未来机电设备，QLF-50)的处理量为0.05-0.5kg/h，进料粒度为100-200目。Weigh each raw material in proportion, mix and stir evenly, place in an ultrafine jet mill and pulverize until the particle size is less than or equal to 3 microns, continue stirring until uniform after discharging, and obtain hydrazone cockroach-killing bait. Wherein, the processing capacity of the ultra-fine jet mill (Hunan Chuangfuli Electromechanical Equipment, QLF-50) is 0.05-0.5kg/h, and the feed particle size is 100-200 mesh.
对比例3Comparative example 3
一种多杀菌素杀蟑饵剂，包括如下百分重量的各原料：A spinosad cockroach-killing bait comprises the following raw materials in percentage by weight:
上述多杀菌素杀蟑饵剂制备方法包括如下步骤：The above-mentioned spinosyn cockroach-killing bait preparation method comprises the following steps:
按比例称取各原料，混合并搅拌均匀后，置于超微气流粉碎机中粉碎至粒径小于等于3微米，出料后继续搅拌至均匀，即得多杀菌素杀蟑饵剂。其中，所述超微气流粉碎机(湖南创未来机电设备，QLF-50)的处理量为0.05-0.5kg/h，进料粒度为100-200目。Weigh each raw material in proportion, mix and stir evenly, place in an ultrafine jet mill and pulverize until the particle size is less than or equal to 3 microns, and continue stirring until uniform after discharging, that is, the multibactin cockroach-killing bait. Wherein, the processing capacity of the ultra-fine jet mill (Hunan Chuangfuli Electromechanical Equipment, QLF-50) is 0.05-0.5kg/h, and the feed particle size is 100-200 mesh.
对比例4Comparative example 4
一种多杀菌素杀蟑饵剂，包括如下百分重量的各原料：A spinosad cockroach-killing bait comprises the following raw materials in percentage by weight:
上述多杀菌素杀蟑饵剂制备方法包括如下步骤：The above-mentioned spinosyn cockroach-killing bait preparation method comprises the following steps:
按比例称取各原料，混合并搅拌均匀后，置于超微气流粉碎机中粉碎至粒径小于等于3微米，出料后继续搅拌至均匀，即得多杀菌素杀蟑饵剂。其中，所述超微气流粉碎机(湖南创未来机电设备，QLF-50)的处理量为0.05-0.5kg/h，进料粒度为100-200目。Weigh each raw material in proportion, mix and stir evenly, place in an ultrafine jet mill and pulverize until the particle size is less than or equal to 3 microns, and continue stirring until uniform after discharging, that is, the multibactin cockroach-killing bait. Wherein, the processing capacity of the ultra-fine jet mill (Hunan Chuangfuli Electromechanical Equipment, QLF-50) is 0.05-0.5kg/h, and the feed particle size is 100-200 mesh.
效果例1：Effect example 1:
将实施例1以及各对比例的杀蟑饵剂进行蟑螂灭杀试验；The cockroach killing bait of embodiment 1 and each comparative ratio is carried out cockroach extermination test;
准备供试美洲大蠊500只，随机分成5组，每组100只，自由取食。Prepare 500 Periplaneta americana for testing, randomly divide them into 5 groups, 100 in each group, and feed freely.
试验组：给食实施例1制备的杀蟑饵剂；对比一组：给食对比例1制备的杀蟑饵剂；对比二组：给食对比例2制备的杀蟑饵剂；对比三组：给食对比例3制备的杀蟑饵剂；对比四组：给食对比例4制备的杀蟑饵剂；5组供试蟑螂分别投放于5个22m2房间中，5个房间的布局及培养皿位置均一样，每个房间均放置木板格栅，并按每个房间21g杀蟑饵剂放置到各组房间的两个培养皿中，且在每个房间再放置两个盛蟑螂饲料的培养皿，同时在每个培养皿旁放置一个盛放有吸水纱布团的培养皿关闭门窗，并计时。每天检查并记录死亡虫数，连续观察至投饵后7d。Test group: feed the cockroach-killing bait prepared in Example 1; comparison group: feed the cockroach-killing bait prepared in Comparative Example 1; compare two groups: feed the cockroach-killing bait prepared in Comparative Example 2; compare three groups : feed the cockroach-killing bait that comparative example 3 prepares; Contrast four groups: feed the cockroach-killing bait that comparative example 4 prepares; 5 groups of test cockroaches are put in 5 22m respectively in the room, layout and cultivation of 5 rooms The positions of the dishes are all the same, each room is placed with a wooden grid, and 21g of cockroach-killing baits are placed in two culture dishes in each group of rooms according to each room, and two culture dishes containing cockroach feed are placed in each room. At the same time, place a Petri dish filled with absorbent gauze next to each Petri dish, close the door and window, and time it. Check and record the number of dead insects every day, and observe continuously until 7 days after feeding.
实验结果：Experimental results:
试验组于给药10-15小时观察到蟑螂有中毒症状，48小时蟑螂死亡率为88％，72小时蟑螂死亡率为100％；In the test group, cockroaches were observed to have poisoning symptoms after 10-15 hours of administration, and the cockroach mortality rate was 88% at 48 hours, and 100% at 72 hours;
对比一组于给药后20小时未见蟑螂死亡，48小时蟑螂死亡75％，72小时蟑螂死亡87％。In the comparison group, no cockroaches died 20 hours after the administration, 75% of the cockroaches died in 48 hours, and 87% of the cockroaches died in 72 hours.
对比二组于给药后20小时未见蟑螂死亡，48小时蟑螂死亡72％，72小时蟑螂死亡89％。Compared with the two groups, no cockroaches died 20 hours after administration, 72% of cockroaches died in 48 hours, and 89% of cockroaches died in 72 hours.
对比三组于给药后20小时未见蟑螂死亡，48小时蟑螂死亡67％，72小时蟑螂死亡73％。Comparing the three groups, no cockroaches died in 20 hours after administration, 67% of cockroaches died in 48 hours, and 73% of cockroaches died in 72 hours.
对比四组于给药后20小时未见蟑螂死亡，48小时蟑螂死亡62％，72小时蟑螂死亡77％。Compared with the four groups, no cockroaches died 20 hours after the administration, 62% of the cockroaches died in 48 hours, and 77% of the cockroaches died in 72 hours.
以上所述实施方式仅为本发明的优选实施例，而并非本发明可行实施的穷举。对于本领域一般技术人员而言，在不背离本发明原理和精神的前提下对其所作出的任何显而易见的改动，都应当被认为包含在本发明的权利要求保护范围之内。The implementation manners described above are only preferred embodiments of the present invention, rather than an exhaustive list of feasible implementations of the present invention. For those skilled in the art, any obvious changes made without departing from the principle and spirit of the present invention should be considered to be included in the protection scope of the claims of the present invention.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| US20110117153A1 (en) * | 2008-03-27 | 2011-05-19 | Christine Kritikou | Spinosyn bait formulations for the control of cockroaches and methods of using the same |
| CN102715196A (en) * | 2011-03-29 | 2012-10-10 | 广州市泰祥白蚁防治工程有限公司 | Bait of cockroach biological pesticide |
| CN106665627A (en) * | 2016-12-28 | 2017-05-17 | 北京贝达化工股份有限公司 | Cockroach attractant, preparation method of cockroach attractant and cockroach bait |
| CN109793014A (en) * | 2019-02-21 | 2019-05-24 | 江西生成卫生用品有限公司 | A kind of high-efficient low toxicity insecticide and preparation method thereof |
| CN111296478A (en) * | 2018-12-10 | 2020-06-19 | 江苏功成生物科技有限公司 | Boric acid-containing insecticidal composition and application thereof |
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| CN103039451B (en) * | 2012-12-21 | 2015-03-18 | 广东省农业科学院植物保护研究所 | Powder type blattaria bait |
| CN103907628A (en) * | 2014-03-31 | 2014-07-09 | 马瑞 | Cockroach prevention and control agent |
| CN105746576A (en) * | 2016-05-05 | 2016-07-13 | 刘凯 | Cockroach killing medicinal powder |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| US20110117153A1 (en) * | 2008-03-27 | 2011-05-19 | Christine Kritikou | Spinosyn bait formulations for the control of cockroaches and methods of using the same |
| CN102715196A (en) * | 2011-03-29 | 2012-10-10 | 广州市泰祥白蚁防治工程有限公司 | Bait of cockroach biological pesticide |
| CN106665627A (en) * | 2016-12-28 | 2017-05-17 | 北京贝达化工股份有限公司 | Cockroach attractant, preparation method of cockroach attractant and cockroach bait |
| CN111296478A (en) * | 2018-12-10 | 2020-06-19 | 江苏功成生物科技有限公司 | Boric acid-containing insecticidal composition and application thereof |
| CN109793014A (en) * | 2019-02-21 | 2019-05-24 | 江西生成卫生用品有限公司 | A kind of high-efficient low toxicity insecticide and preparation method thereof |
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