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CN118906426B - A melt plasticizing extrusion control method and system - Google Patents

A melt plasticizing extrusion control method and system Download PDF

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Publication number
CN118906426B
CN118906426B CN202411390522.7A CN202411390522A CN118906426B CN 118906426 B CN118906426 B CN 118906426B CN 202411390522 A CN202411390522 A CN 202411390522A CN 118906426 B CN118906426 B CN 118906426B
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target
melting temperature
curve
interval
melting
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CN118906426A (en
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江庆国
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Nantong Younaite Plastic New Material Co ltd
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Nantong Younaite Plastic New Material Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/25Component parts, details or accessories; Auxiliary operations
    • B29C48/92Measuring, controlling or regulating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C2948/00Indexing scheme relating to extrusion moulding
    • B29C2948/92Measuring, controlling or regulating
    • B29C2948/92504Controlled parameter
    • B29C2948/92695Viscosity; Melt flow index [MFI]; Molecular weight
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C2948/00Indexing scheme relating to extrusion moulding
    • B29C2948/92Measuring, controlling or regulating
    • B29C2948/92504Controlled parameter
    • B29C2948/92704Temperature

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Extrusion Moulding Of Plastics Or The Like (AREA)

Abstract

The invention discloses a method and a system for controlling melt plasticizing extrusion, and relates to the technical field of plastic processing, wherein the method comprises the steps of monitoring plasticizing extrusion quality of a target product of a target extruder in a preset monitoring window, and generating an extrusion quality recording sequence; determining extrusion quality fluctuation factors, obtaining K heat change curves, generating a melting temperature interval of a target product, generating a target melting temperature interval, performing temperature monitoring to obtain a monitoring temperature set, determining a target melting temperature deviation value, performing control parameter configuration according to the target melting temperature deviation value to obtain a target control parameter set, and transmitting the target control parameter set to a control unit of a target extruder for parameter adjustment. The invention solves the technical problem of poor extrusion quality caused by inaccurate determination of the melting temperature interval of the product in the prior art, and achieves the technical effect of improving the accuracy of melting plasticizing extrusion control.

Description

Melt plasticizing extrusion control method and system
Technical Field
The invention relates to the technical field of plastic processing, in particular to a melting plasticizing extrusion control method and a melting plasticizing extrusion control system.
Background
In the production of plastic products, plasticization extrusion is a critical process. However, if the melting temperature interval of the product is not accurately determined at the time of plasticizing extrusion, poor extrusion quality may result. In addition, the unstable melting temperature also causes inconsistent extrusion speed, further affecting the dimensional accuracy and appearance quality of the product. Therefore, precise control of the melting temperature interval of the plastic is an important element in ensuring the quality of the extruded product. At present, when the melting plasticization extrusion control is performed, the melting temperature interval of a product is not accurately determined, and the extruder cannot be adaptively adjusted and controlled, so that the extrusion quality is poor.
Disclosure of Invention
The application provides a melting plasticizing extrusion control method and a melting plasticizing extrusion control system, which are used for solving the technical problem of poor extrusion quality caused by inaccurate determination of a product melting temperature interval in the prior art.
In view of the above, the present application provides a melt plasticizing extrusion control method and system.
In a first aspect of the present application, there is provided a melt plasticization extrusion control method, the method comprising:
Performing plasticizing extrusion quality monitoring of a target product of a target extruder in a preset monitoring window to generate an extrusion quality recording sequence;
Analyzing the extrusion quality record sequence based on a preset melting quality index, and determining an extrusion quality fluctuation factor according to an analysis result;
Carrying out melting temperature test on K product raw material samples by using a differential scanning calorimeter to obtain K heat change curves, and carrying out scattered point edge identification on the K heat change curves to generate a melting temperature interval of the target product;
correcting the melting temperature interval based on the extrusion quality fluctuation factor to generate a target melting temperature interval;
Continuously monitoring the temperature of a melting zone of the target extruder in a preset continuous monitoring window to obtain a monitoring temperature set;
Determining a target melting temperature deviation value based on the monitored temperature set and the target melting temperature interval, and performing control parameter configuration according to the target melting temperature deviation value to obtain a target control parameter set, wherein the target control parameter comprises heating temperature, heating time and melting pressure;
And transmitting the target control parameter set to a control unit of a target extruder for parameter adjustment.
In a second aspect of the present application, there is provided a melt plasticizing extrusion control system, the system comprising:
the extrusion quality record sequence generation module is used for executing plasticization extrusion quality monitoring of a target product of the target extruder in a preset monitoring window to generate an extrusion quality record sequence;
The extrusion quality fluctuation factor determining module is used for analyzing the extrusion quality record sequence based on a preset melting quality index and determining an extrusion quality fluctuation factor according to an analysis result;
The melting temperature interval generation module is used for carrying out melting temperature test on K product raw material samples by utilizing a differential scanning calorimeter to obtain K heat change curves, carrying out scattered point edge identification on the K heat change curves, and generating a melting temperature interval of the target product;
the target melting temperature interval generation module is used for correcting the melting temperature interval based on the extrusion quality fluctuation factor to generate a target melting temperature interval;
The monitoring temperature set obtaining module is used for continuously monitoring the temperature of the melting zone of the target extruder in a preset continuous monitoring window to obtain a monitoring temperature set;
The target control parameter set obtaining module is used for determining a target melting temperature deviation value based on the monitored temperature set and the target melting temperature interval, and carrying out control parameter configuration according to the target melting temperature deviation value to obtain a target control parameter set, wherein the target control parameter set comprises heating temperature, heating time and melting pressure;
and the parameter adjustment module is used for transmitting the target control parameter set to a control unit of the target extruder for parameter adjustment.
One or more technical schemes provided by the application have at least the following technical effects or advantages:
according to the application, plasticizing extrusion quality monitoring of a target product of a target extruder is performed in a preset monitoring window to generate an extrusion quality recording sequence, then the extrusion quality recording sequence is analyzed based on a preset melting quality index, extrusion quality fluctuation factors are determined according to analysis results, and then K raw material samples of the product are subjected to melting temperature testing by utilizing a differential scanning calorimeter to obtain K heat change curves, scattered point edge identification is performed on the K heat change curves to generate a melting temperature interval of the target product, the melting temperature interval is corrected based on the extrusion quality fluctuation factors to generate a target melting temperature interval, then the melting area of the target extruder is continuously subjected to temperature monitoring in the preset continuous monitoring window to obtain a monitoring temperature set, a target melting temperature deviation value is determined based on the monitoring temperature set and the target melting temperature interval, and a target control parameter set is obtained according to control parameter configuration of the target melting temperature deviation value, wherein the target control parameters comprise heating temperature, heating time and melting pressure, and then the target control parameter set is transmitted to a control unit of the target extruder for parameter adjustment. The technical effects of improving the control reliability of parameters and improving the quality of melt plasticization extrusion are achieved.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings required for the description of the embodiments will be briefly described below, and it is apparent that the drawings in the following description are only some embodiments of the present invention, and other drawings may be obtained according to these drawings without inventive effort for a person skilled in the art.
FIG. 1 is a schematic flow chart of a melt plasticizing extrusion control method according to an embodiment of the present application;
fig. 2 is a schematic structural diagram of a melt plasticizing extrusion control system according to an embodiment of the present application.
Reference numerals indicate that the extrusion quality record sequence generating module 11, the extrusion quality fluctuation factor determining module 12, the melting temperature interval generating module 13, the target melting temperature interval generating module 14, the monitoring temperature set obtaining module 15, the target control parameter set obtaining module 16 and the parameter adjusting module 17.
Detailed Description
The application provides a melting plasticizing extrusion control method and a melting plasticizing extrusion control system, which are used for solving the technical problem of poor extrusion quality caused by inaccurate determination of a product melting temperature interval in the prior art.
The technical solutions in the embodiments of the present application will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present application. It will be apparent that the described embodiments are only some, but not all, embodiments of the application. All other embodiments, which can be made by those skilled in the art based on the embodiments of the application without making any inventive effort, are intended to be within the scope of the application.
It should be noted that the terms "comprises" and "comprising" are intended to cover a non-exclusive inclusion, such that a process, method, system, article, or server that comprises a list of steps or elements is not necessarily limited to those steps or elements expressly listed or inherent to such process, method, article, or apparatus.
Example 1
As shown in fig. 1, the present application provides a melt plasticizing extrusion control method, wherein the method includes:
Step 100, performing plasticizing extrusion quality monitoring of a target product of a target extruder in a preset monitoring window to generate an extrusion quality recording sequence;
In one possible embodiment, in order to analyze the fluctuation degree of the quality of the product processed by the production of the target extruder, the processed product is subjected to plasticizing extrusion quality monitoring within a preset monitoring window, and key parameters and quality indexes are recorded in the monitoring process, so as to generate the extrusion quality recording sequence. The preset monitoring window is a monitoring time period set by a person skilled in the art, for example, a monitoring window is set from 10 th minute to 60 th minute after the extruder is started, and the extruder reaches a stable working state and continuously produces target products.
The monitoring equipment such as a temperature sensor, a pressure sensor and the like is arranged at key parts (such as an extruder head, a die and the like) of the extruder and is used for recording key parameters such as temperature, pressure and the like in the extrusion process in real time. And simultaneously, recording data such as melt index of the produced product, and arranging the recorded data according to time sequence to obtain the extrusion quality recording sequence. The technical effect of correcting the melting temperature interval for the actual production condition of the subsequent combined extruder and providing basic analysis data is achieved.
Step 200, analyzing the extrusion quality record sequence based on a preset melting quality index, and determining an extrusion quality fluctuation factor according to an analysis result;
Further, the preset melt quality index includes a melt index, a thermal stability, and a melt viscosity.
In one embodiment, the extrusion quality recording sequence is subjected to data extraction by taking the preset melt quality index as an index to obtain a melt index set, a thermal stability set and a melt viscosity set. And respectively carrying out variance calculation on the melt index set, the thermal stability set and the melt viscosity set, and taking calculation results as a melt index fluctuation factor, a thermal stability fluctuation factor and a melt viscosity fluctuation factor. The larger the variance, the greater the volatility of the corresponding index, the poorer the extruder production stability.
The melt index refers to the mass of the melt flowing out of the molten plastic in unit time of passing through the die head at a preset temperature and a preset load. The thermal stability is the ability of a plastic to retain its properties at high temperatures. The melt viscosity is the viscosity of the plastic in a molten state.
And carrying out weighted calculation on the melt index fluctuation factor, the thermal stability fluctuation factor and the melt viscosity fluctuation factor according to a weight ratio preset by a person skilled in the art, and taking a weighted calculation result as the extrusion quality fluctuation factor. The technical effect of quantifying the working stability of the extruder is achieved.
S300, carrying out melting temperature test on K product raw material samples by using a differential scanning calorimeter to obtain K heat change curves, and carrying out scattered point edge identification on the K heat change curves to generate a melting temperature interval of the target product;
Further, the melting temperature test is performed on K product raw material samples by using a differential scanning calorimeter to obtain K heat change curves, and step S300 of the embodiment of the present application further includes:
placing the K product raw material samples in an aluminum crucible, and placing the aluminum crucible in a sample frame of a differential scanning calorimeter for completing baseline calibration;
heating K raw material samples of the product according to a preset heating rate until reaching a preset heating temperature, and leading out a record curve of a differential scanning calorimeter to generate K initial heat change curves;
And traversing the K initial heat change curves to perform data cleaning, and determining the K heat change curves.
In one possible embodiment, in order to determine the melting temperature interval of the raw material of the target product in the extruder, K samples of the raw material of the product are first tested to determine the melting temperature interval that corresponds to the condition of the raw material itself. The differential scanning calorimeter is an instrument for measuring the temperature and heat flow relation related to the internal thermal transition of a material. The K product raw material samples are tested through the differential scanning calorimeter, so that accidental errors can be effectively avoided, and the analysis accuracy is improved. The K heat change curves reflect the melting crystallization conditions of K raw material samples of the product. And further, the scattered point edge recognition is carried out on the K heat change curves, so that the melting temperature interval of the raw materials meeting the batch of target products can be effectively determined.
In one embodiment, the K product raw material samples are placed in aluminum crucibles and the aluminum crucibles are placed in a sample holder of a differential scanning calorimeter that completes the baseline calibration, respectively. Alternatively, baseline calibration may be achieved by conducting a blank test on a differential scanning calorimeter using two empty crucibles under the same temperature conditions.
The preset temperature rise rate is the amplitude of the temperature rise per unit time set by a person skilled in the art. The preset heating temperature is a temperature value set by a person skilled in the art to be heated. Optionally, the K product raw material samples are heated at a preset heating rate, for example, 10 ℃ per minute or 20 ℃ per minute, until a preset heating temperature is reached, for example, from room temperature to 300 ℃. At this time, the recording curves of the differential scanning calorimeter are respectively derived, and K initial heat change curves are obtained. Optionally, filling missing values and break points in the K initial heat change curves, and removing the abnormal values by using a box diagram method, so that the K heat change curves after cleaning is obtained.
Further, step S300 of the embodiment of the present application further includes:
Carrying out alignment treatment on the K heat change curves based on the same time, numbering the K heat change curves according to the sequence of curve starting nodes, and generating K heat change curve numbers, wherein the K heat change curve numbers are in one-to-one correspondence with the K heat change curves;
Extracting a first curve starting point and a first curve ending point of the K heat change curves respectively, mapping the extraction results according to the K heat change curve numbers, and determining a first curve starting point sequence and a first curve ending point sequence, wherein the first curve starting point is a peak starting point of a melting peak of the heat change curve, and the first curve ending point is a peak ending point of the melting peak of the heat change curve;
and carrying out scattered point edge identification based on the first curve starting point sequence and the first curve ending point sequence, and generating the melting temperature interval.
Further, step S300 of the embodiment of the present application further includes:
Extracting intermediate values of K first curve starting points of the first curve starting point sequence to obtain first curve starting point intermediate values;
taking the intermediate value of the starting point of the first curve as the starting point, and determining a first identification temperature interval according to a preset edge identification step length;
Moving the first identification temperature interval to the left side of the left side end point and the right side of the right side end point according to a preset edge identification step length to obtain a second identification temperature interval;
judging whether the distribution density difference value of the first identification temperature interval and the second identification temperature interval meets a preset difference value threshold value, if so, carrying out average value processing on a plurality of first curve starting points in the first identification temperature interval to obtain an interval left end point;
extracting intermediate values of K first curve end points of the first curve end point sequence, and carrying out scattered point edge identification on the first curve end point sequence by taking the intermediate values of the first curve end points as starting points to obtain a right end point of a section;
And generating the melting temperature interval according to the left end point of the interval and the right end point of the interval.
Further, step S300 of the embodiment of the present application further includes:
if not, moving the second identification temperature interval to the left side of the left side end point and the right side of the right side end point according to a preset edge identification step length to obtain a third identification temperature interval;
Judging whether the distribution density difference value of the second identification temperature interval and the third identification temperature interval meets a preset difference value threshold value, if so, carrying out average value processing on a plurality of first curve starting points in the second identification temperature interval to obtain an interval left end point;
if not, carrying out scattered point edge recognition based on the third recognition temperature interval, and determining the left end point of the interval.
In one possible embodiment, the same time is a time when the test starts, and based on the same, the K thermal variation curves are aligned, and the K thermal variation curves are numbered according to the sequence of the curve start nodes, so as to generate K thermal variation curve numbers, where the K thermal variation curve numbers are in one-to-one correspondence with the K thermal variation curves.
The K heat change curves have peaks and valleys. The peak is a melting peak corresponding to the melting process of the plastic. And taking a peak starting point of a melting peak in the thermal variation curve as the first curve starting point and a peak ending point of the melting peak of the thermal variation curve as the first curve ending point.
And respectively extracting a first curve starting point and a first curve ending point from the K heat change curves, mapping the extraction results according to the numbers of the K heat change curves, and determining a first curve starting point sequence and a first curve ending point sequence. The first curve starting point sequence reflects the time series of the onset of melting of the K product raw material samples. The first curve end point sequence reflects the time series of the end of melting of K product raw material samples.
And extracting intermediate values of K first curve starting points of the first curve starting point sequence to obtain a first curve starting point intermediate value, and then determining a first identification temperature interval according to a preset edge identification step length by taking the first curve starting point intermediate value as a starting point. The preset edge identification step length is a temperature amplitude which is set by a person skilled in the art and is moved on one side during interval identification. And respectively moving preset edge recognition step sizes to two sides of the starting point by taking the middle value of the starting point of the first curve as the starting point according to the preset edge recognition step sizes to obtain two end points of the first recognition temperature interval. And obtaining a first distribution density of the first identification temperature interval by counting the number of the first curve starting points contained in the first identification temperature interval and comparing the counted result with the length of the first identification temperature interval. Wherein the first distribution density reflects a degree of intensity of a first curve start point of the distribution within the first identification temperature interval.
And further, moving the first identification temperature interval to the left side of the left side end point and the right side of the right side end point according to a preset edge identification step length to obtain a second identification temperature interval. A second distribution density of the second identified temperature interval is obtained based on the same principle as the first distribution density.
Judging whether the distribution density difference value (the difference value between the first distribution density and the second distribution density) between the first identification temperature interval and the second identification temperature interval meets a preset difference value threshold, if so, indicating that the first identification temperature interval can represent the temperature distribution condition of a first curve starting point sequence, and carrying out average value processing on a plurality of first curve starting points in the first identification temperature interval to obtain an interval left end point.
If not, moving the second identification temperature interval to the left side of the left side end point and the right side of the right side end point according to a preset edge identification step length to obtain a third identification temperature interval;
and determining a third distribution density of a third identification temperature interval based on the same acquisition principle as the first distribution density, further judging whether the distribution density difference between the second identification temperature interval and the third identification temperature interval meets a preset difference threshold, and if so, carrying out mean value processing on a plurality of first curve starting points in the second identification temperature interval to obtain an interval left end point. If not, carrying out scattered point edge recognition based on the third recognition temperature interval until the distribution density difference value of two adjacent recognition temperature intervals meets a preset difference value threshold, and determining the left end point of the interval.
And extracting intermediate values of K first curve end points of the first curve end point sequence based on the same acquisition principle as that of the left end point of the interval, and carrying out scattered point edge identification on the first curve end point sequence by taking the intermediate values of the first curve end points as starting points to acquire the right end point of the interval. And generating the melting temperature interval according to the left end point of the interval and the right end point of the interval.
Step 400, correcting the melting temperature interval based on the extrusion quality fluctuation factor to generate a target melting temperature interval;
in one possible embodiment, a target extrusion quality fluctuation factor (an extrusion product quality fluctuation condition of an extruder in a standard operation state) of the target product raw material is extracted, and a ratio of the extrusion quality fluctuation factor to the target extrusion quality fluctuation factor is used as a correction factor. And multiplying the correction factor by the melting temperature interval to obtain the target melting temperature interval. The aim of correcting the melting temperature interval according to the actual working fluctuation condition of the extruder is fulfilled.
Step 500, continuously monitoring the temperature of a melting zone of the target extruder in a preset continuous monitoring window to obtain a monitoring temperature set;
In one possible embodiment, the preset monitoring window is a monitoring period preset by a person skilled in the art. And monitoring the temperature of the melting area of the target extruder by using devices such as a thermocouple, a thermometer and the like, and reading monitoring data to obtain the monitoring temperature set. Wherein, the monitoring temperature set reflects the temperature change condition of the melting zone when the extruder actually works.
Step 600, determining a target melting temperature deviation value based on the monitored temperature set and the target melting temperature interval, and configuring control parameters according to the target melting temperature deviation value to obtain a target control parameter set, wherein the target control parameters comprise heating temperature, heating time and melting pressure;
And step S700, transmitting the target control parameter set to a control unit of a target extruder for parameter adjustment.
Further, determining a target melting temperature deviation value based on the monitored temperature set and the target melting temperature interval, and performing control parameter configuration according to the target melting temperature deviation value to obtain a target control parameter set, where step S600 further includes:
Traversing the monitoring temperature set to perform average value calculation, and determining a monitoring temperature average value;
Calculating a difference value between the monitored temperature average value and the central melting temperature of the target melting temperature interval, and determining the target melting temperature deviation value;
Constructing a control parameter configuration network layer;
and identifying the target melting temperature deviation value and the target extruder parameter range by utilizing the control parameter configuration network layer, and determining a target control parameter set.
In one possible embodiment, a target melting temperature deviation value is determined based on the monitored temperature set and the target melting temperature interval, and then a control parameter configuration is performed based on the target melting temperature deviation value to obtain a target control parameter set, wherein the target control parameter includes a heating temperature, a heating time and a melting pressure. And transmitting the target control parameter set to a control unit of a target extruder for parameter adjustment. The technical effects of performing control parameter configuration according to the actual conditions of the extruder and the actual melting temperature interval of the raw materials of the target product and improving the control accuracy are achieved.
In one embodiment, the monitored temperature set is traversed to perform a mean calculation to determine a monitored temperature mean. And further, calculating a difference value between the monitored temperature average value and the central melting temperature of the target melting temperature interval, and determining the target melting temperature deviation value. Wherein the target melting temperature deviation value is a temperature deviation value to be corrected. The control parameter configuration network layer is used for intelligently configuring extruder parameters according to the actual conditions of the extruder and the target melting temperature deviation value to be corrected.
Optionally, acquiring a plurality of sample melting temperature deviation values and a plurality of sample extruder parameter ranges, and a plurality of sample control parameter sets as training data, performing supervised training on a network layer constructed based on a convolutional neural network by using the training data, and learning a two-to-one mapping relation between the melting temperature deviation values and the extruder parameter ranges and the control parameter sets in training until model output reaches convergence, so as to obtain the control parameter configuration network layer after training is completed. And inputting the target melting temperature deviation value and the target extruder parameter range into a control parameter configuration network layer for identification, and determining a target control parameter set.
In summary, the embodiment of the application has at least the following technical effects:
According to the application, plasticizing extrusion quality monitoring of a target product of a target extruder is performed in a preset monitoring window to generate an extrusion quality record sequence, then an extrusion quality fluctuation factor is determined according to an analysis result to obtain K heat change curves, scattered point edge recognition is performed on the K heat change curves to generate a melting temperature interval of the target product, the melting temperature interval is corrected based on the extrusion quality fluctuation factor to generate a target melting temperature interval, a target for correcting the melting temperature interval according to the actual working state of the extruder is realized, then the melting area of the target extruder is continuously monitored in the preset continuous monitoring window to obtain a monitoring temperature set, a target melting temperature deviation value is determined based on the monitoring temperature set and the target melting temperature interval, control parameter configuration is performed according to the target melting temperature deviation value to obtain a target control parameter set, wherein the target control parameter set comprises heating temperature, heating time and melting pressure, and then the target control parameter set is transmitted to a control unit of the target extruder for parameter adjustment. The technical effects of improving the control accuracy of the extruder and improving the melt plasticizing extrusion quality are achieved.
Example two
Based on the same inventive concept as one of the melt plasticizing extrusion control methods in the foregoing embodiments, as shown in fig. 2, the present application provides a melt plasticizing extrusion control system, and the system and method embodiments in the embodiments of the present application are based on the same inventive concept. Wherein the system comprises:
the extrusion quality record sequence generation module 11 is used for performing plasticization extrusion quality monitoring of a target product of the target extruder in a preset monitoring window to generate an extrusion quality record sequence;
An extrusion quality fluctuation factor determination module 12, configured to analyze the extrusion quality record sequence based on a preset melt quality index, and determine an extrusion quality fluctuation factor according to an analysis result;
The melting temperature interval generating module 13 is configured to perform melting temperature test on K product raw material samples by using a differential scanning calorimeter to obtain K heat change curves, and perform scattered point edge recognition on the K heat change curves to generate a melting temperature interval of the target product;
A target melting temperature interval generation module 14 for correcting the melting temperature interval based on the extrusion quality fluctuation factor to generate a target melting temperature interval;
the monitoring temperature set obtaining module 15 is configured to continuously monitor the temperature of the melting zone of the target extruder in a preset continuous monitoring window, so as to obtain a monitoring temperature set;
a target control parameter set obtaining module 16, configured to determine a target melting temperature deviation value based on the monitored temperature set and the target melting temperature interval, and perform control parameter configuration according to the target melting temperature deviation value, so as to obtain a target control parameter set, where the target control parameter includes a heating temperature, a heating time, and a melting pressure;
And the parameter adjustment module 17 is used for transmitting the target control parameter set to a control unit of the target extruder for parameter adjustment.
Further, the preset melt quality index includes a melt index, a thermal stability, and a melt viscosity.
Further, the melting temperature interval generation module 13 is configured to perform the following steps:
placing the K product raw material samples in an aluminum crucible, and placing the aluminum crucible in a sample frame of a differential scanning calorimeter for completing baseline calibration;
heating K raw material samples of the product according to a preset heating rate until reaching a preset heating temperature, and leading out a record curve of a differential scanning calorimeter to generate K initial heat change curves;
And traversing the K initial heat change curves to perform data cleaning, and determining the K heat change curves.
Further, the melting temperature interval generation module 13 is configured to perform the following steps:
Carrying out alignment treatment on the K heat change curves based on the same time, numbering the K heat change curves according to the sequence of curve starting nodes, and generating K heat change curve numbers, wherein the K heat change curve numbers are in one-to-one correspondence with the K heat change curves;
Extracting a first curve starting point and a first curve ending point of the K heat change curves respectively, mapping the extraction results according to the K heat change curve numbers, and determining a first curve starting point sequence and a first curve ending point sequence, wherein the first curve starting point is a peak starting point of a melting peak of the heat change curve, and the first curve ending point is a peak ending point of the melting peak of the heat change curve;
and carrying out scattered point edge identification based on the first curve starting point sequence and the first curve ending point sequence, and generating the melting temperature interval.
Further, the melting temperature interval generation module 13 is configured to perform the following steps:
Extracting intermediate values of K first curve starting points of the first curve starting point sequence to obtain first curve starting point intermediate values;
taking the intermediate value of the starting point of the first curve as the starting point, and determining a first identification temperature interval according to a preset edge identification step length;
Moving the first identification temperature interval to the left side of the left side end point and the right side of the right side end point according to a preset edge identification step length to obtain a second identification temperature interval;
judging whether the distribution density difference value of the first identification temperature interval and the second identification temperature interval meets a preset difference value threshold value, if so, carrying out average value processing on a plurality of first curve starting points in the first identification temperature interval to obtain an interval left end point;
extracting intermediate values of K first curve end points of the first curve end point sequence, and carrying out scattered point edge identification on the first curve end point sequence by taking the intermediate values of the first curve end points as starting points to obtain a right end point of a section;
And generating the melting temperature interval according to the left end point of the interval and the right end point of the interval.
Further, the melting temperature interval generation module 13 is configured to perform the following steps:
if not, moving the second identification temperature interval to the left side of the left side end point and the right side of the right side end point according to a preset edge identification step length to obtain a third identification temperature interval;
Judging whether the distribution density difference value of the second identification temperature interval and the third identification temperature interval meets a preset difference value threshold value, if so, carrying out average value processing on a plurality of first curve starting points in the second identification temperature interval to obtain an interval left end point;
if not, carrying out scattered point edge recognition based on the third recognition temperature interval, and determining the left end point of the interval.
Further, the target control parameter set obtaining module 16 is configured to perform the following steps:
Traversing the monitoring temperature set to perform average value calculation, and determining a monitoring temperature average value;
Calculating a difference value between the monitored temperature average value and the central melting temperature of the target melting temperature interval, and determining the target melting temperature deviation value;
Constructing a control parameter configuration network layer;
and identifying the target melting temperature deviation value and the target extruder parameter range by utilizing the control parameter configuration network layer, and determining a target control parameter set.
It should be noted that the sequence of the embodiments of the present application is only for description, and does not represent the advantages and disadvantages of the embodiments. And the foregoing description has been directed to specific embodiments of this specification. In addition, the processes depicted in the accompanying figures do not necessarily require the particular order shown, or sequential order, to achieve desirable results. In some embodiments, multitasking and parallel processing are also possible or may be advantageous.
The foregoing description of the preferred embodiments of the application is not intended to limit the application to the precise form disclosed, and any such modifications, equivalents, and alternatives falling within the spirit and scope of the application are intended to be included within the scope of the application.
The specification and figures are merely exemplary illustrations of the present application and are considered to cover any and all modifications, variations, combinations, or equivalents that fall within the scope of the application. It will be apparent to those skilled in the art that various modifications and variations can be made to the present application without departing from the scope of the application. Thus, the present application is intended to include such modifications and alterations insofar as they come within the scope of the application or the equivalents thereof.

Claims (7)

1.一种熔融塑化挤出控制方法,其特征在于,所述方法包括:1. A melt plasticizing extrusion control method, characterized in that the method comprises: 在预设监测窗口内执行目标挤出机的目标产品的塑化挤出质量监测,生成挤出质量记录序列;Perform plasticizing extrusion quality monitoring of a target product of a target extruder within a preset monitoring window, and generate an extrusion quality record sequence; 基于预设熔融质量指标对所述挤出质量记录序列进行分析,根据分析结果确定挤出质量波动因子;Analyzing the extrusion quality record sequence based on a preset melting quality index, and determining an extrusion quality fluctuation factor according to the analysis result; 利用差示扫描量热仪对K个产品原材料样品进行熔融温度测试,获得K条热量变化曲线,并对所述K条热量变化曲线进行散点边缘识别,生成所述目标产品的熔融温度区间;Using a differential scanning calorimeter to test the melting temperature of K product raw material samples, obtaining K heat change curves, and performing scattered point edge recognition on the K heat change curves to generate the melting temperature range of the target product; 基于所述挤出质量波动因子对所述熔融温度区间进行修正,生成目标熔融温度区间;Correcting the melting temperature range based on the extrusion quality fluctuation factor to generate a target melting temperature range; 在预设持续监测窗口持续对所述目标挤出机的熔融区进行温度监测,获得监测温度集合;Continuously monitoring the temperature of the melting zone of the target extruder in a preset continuous monitoring window to obtain a monitoring temperature set; 基于所述监测温度集合与所述目标熔融温度区间确定目标熔融温度偏离值,根据所述目标熔融温度偏离值进行控制参数配置,获得目标控制参数集合,其中,所述目标控制参数包括加热温度、加热时间、熔融压力;Determining a target melting temperature deviation value based on the monitoring temperature set and the target melting temperature interval, configuring control parameters according to the target melting temperature deviation value, and obtaining a target control parameter set, wherein the target control parameters include heating temperature, heating time, and melting pressure; 将所述目标控制参数集合传输至目标挤出机的控制单元进行参数调整;Transmitting the target control parameter set to a control unit of a target extruder for parameter adjustment; 其中,生成所述目标产品的熔融温度区间,包括:Wherein, generating the melting temperature range of the target product includes: 基于同比时间对所述K条热量变化曲线进行对齐处理,并按照曲线开始节点的先后顺序对所述K条热量变化曲线进行编号,生成K个热量变化曲线编号,其中,所述K个热量变化曲线编号与K条热量变化曲线一一对应;Aligning the K heat change curves based on the same period of time, and numbering the K heat change curves according to the order of the start nodes of the curves to generate K heat change curve numbers, wherein the K heat change curve numbers correspond to the K heat change curves one by one; 分别对所述K条热量变化曲线进行第一曲线起点和第一曲线终点提取,并对提取结果按照所述K个热量变化曲线编号进行映射,确定第一曲线起点序列和第一曲线终点序列,其中,所述第一曲线起点为热量变化曲线的熔融峰的峰开始点,所述第一曲线终点为热量变化曲线的熔融峰的峰结束点;Extracting the first curve starting point and the first curve end point of the K heat change curves respectively, and mapping the extraction results according to the numbers of the K heat change curves to determine the first curve starting point sequence and the first curve end point sequence, wherein the first curve starting point is the peak start point of the melting peak of the heat change curve, and the first curve end point is the peak end point of the melting peak of the heat change curve; 基于所述第一曲线起点序列和所述第一曲线终点序列进行散点边缘识别,生成所述熔融温度区间。The melting temperature interval is generated by performing scattered point edge recognition based on the first curve starting point sequence and the first curve end point sequence. 2.如权利要求1所述的一种熔融塑化挤出控制方法,其特征在于,所述预设熔融质量指标包括熔融指数、热稳定性和熔体黏度。2. A melt plasticizing extrusion control method as described in claim 1, characterized in that the preset melt quality indicators include melt index, thermal stability and melt viscosity. 3.如权利要求1所述的一种熔融塑化挤出控制方法,其特征在于,利用差示扫描量热仪对K个产品原材料样品进行熔融温度测试,获得K条热量变化曲线,包括:3. A melt plasticizing extrusion control method according to claim 1, characterized in that K product raw material samples are subjected to melting temperature testing using a differential scanning calorimeter to obtain K heat change curves, comprising: 对所述K个产品原材料样品放置于铝制坩埚中,并将铝制坩埚放入完成基线校准的差示扫描量热仪的样品架中;The K product raw material samples are placed in an aluminum crucible, and the aluminum crucible is placed in a sample holder of a differential scanning calorimeter that has completed baseline calibration; 按照预设升温速率对K个产品原材料样品进行加热,直至达到预设加热温度,导出差示扫描量热仪的记录曲线,生成K条初始热量变化曲线;K product raw material samples are heated at a preset heating rate until a preset heating temperature is reached, and a recording curve of a differential scanning calorimeter is derived to generate K initial heat change curves; 遍历所述K条初始热量变化曲线进行数据清洗,确定K条热量变化曲线。The K initial heat change curves are traversed to perform data cleaning and determine K heat change curves. 4.如权利要求1所述的一种熔融塑化挤出控制方法,其特征在于,包括:4. A melt plasticizing extrusion control method according to claim 1, characterized in that it comprises: 对所述第一曲线起点序列的K个第一曲线起点进行中间值提取,获得第一曲线起点中间值;Extracting intermediate values of K first curve starting points in the first curve starting point sequence to obtain intermediate values of the first curve starting points; 以所述第一曲线起点中间值为起始点,按照预设边缘识别步长确定第一识别温度区间;Taking the middle value of the starting point of the first curve as the starting point, determining the first recognition temperature interval according to the preset edge recognition step length; 对所述第一识别温度区间按照预设边缘识别步长向左侧端点的左侧和右侧端点的右侧进行移动,获得第二识别温度区间;The first identified temperature interval is moved to the left of the left end point and to the right of the right end point according to a preset edge identification step length to obtain a second identified temperature interval; 判断所述第一识别温度区间和所述第二识别温度区间的分布密度差值是否满足预设差值阈值,若是,则对所述第一识别温度区间内的多个第一曲线起点进行均值处理,获得区间左端点;Determine whether the distribution density difference between the first identified temperature interval and the second identified temperature interval meets a preset difference threshold, and if so, perform mean processing on multiple first curve starting points in the first identified temperature interval to obtain the interval left endpoint; 对所述第一曲线终点序列的K个第一曲线终点进行中间值提取,并以第一曲线终点中间值为起始点,对所述第一曲线终点序列进行散点边缘识别,获得区间右端点;Extracting the middle value of K first curve endpoints of the first curve endpoint sequence, and using the middle value of the first curve endpoint as the starting point, performing scattered point edge recognition on the first curve endpoint sequence to obtain the right endpoint of the interval; 根据所述区间左端点和所述区间右端点,生成所述熔融温度区间。The melting temperature interval is generated according to the interval left endpoint and the interval right endpoint. 5.如权利要求4所述的一种熔融塑化挤出控制方法,其特征在于,包括:5. A melt plasticizing extrusion control method according to claim 4, characterized in that it comprises: 若否,则对所述第二识别温度区间按照预设边缘识别步长向左侧端点的左侧和右侧端点的右侧进行移动,获得第三识别温度区间;If not, the second identified temperature interval is moved to the left of the left end point and to the right of the right end point according to the preset edge identification step length to obtain a third identified temperature interval; 判断所述第二识别温度区间和所述第三识别温度区间的分布密度差值是否满足预设差值阈值,若是,则对所述第二识别温度区间内的多个第一曲线起点进行均值处理,获得区间左端点;Determine whether the distribution density difference between the second identification temperature interval and the third identification temperature interval meets a preset difference threshold, and if so, perform mean processing on multiple first curve starting points in the second identification temperature interval to obtain the interval left endpoint; 若否,则基于所述第三识别温度区间进行散点边缘识别,确定区间左端点。If not, scattered point edge recognition is performed based on the third identified temperature interval to determine the left endpoint of the interval. 6.如权利要求1所述的一种熔融塑化挤出控制方法,其特征在于,基于所述监测温度集合与所述目标熔融温度区间确定目标熔融温度偏离值,根据所述目标熔融温度偏离值进行控制参数配置,获得目标控制参数集合,包括:6. A melt plasticizing extrusion control method according to claim 1, characterized in that a target melt temperature deviation value is determined based on the monitoring temperature set and the target melt temperature interval, and a control parameter is configured according to the target melt temperature deviation value to obtain a target control parameter set, comprising: 遍历所述监测温度集合进行均值计算,确定监测温度均值;Traversing the monitoring temperature set to perform mean calculation and determine the mean of the monitoring temperatures; 将所述监测温度均值与所述目标熔融温度区间的中心熔融温度进行差值计算,确定所述目标熔融温度偏离值;Calculate the difference between the monitored temperature mean and the central melting temperature of the target melting temperature interval to determine the target melting temperature deviation value; 构建控制参数配置网络层;Construct control parameters to configure the network layer; 利用所述控制参数配置网络层对所述目标熔融温度偏离值和目标挤出机参数范围进行识别,确定目标控制参数集合。The control parameter configuration network layer is used to identify the target melt temperature deviation value and the target extruder parameter range, and determine a target control parameter set. 7.一种熔融塑化挤出控制系统,其特征在于,所述系统用于实施权利要求1-6任一项所述的一种熔融塑化挤出控制方法,所述系统包括:7. A melt-plasticizing extrusion control system, characterized in that the system is used to implement a melt-plasticizing extrusion control method according to any one of claims 1 to 6, and the system comprises: 挤出质量记录序列生成模块,用于在预设监测窗口内执行目标挤出机的目标产品的塑化挤出质量监测,生成挤出质量记录序列;An extrusion quality record sequence generation module is used to perform plasticizing extrusion quality monitoring of a target product of a target extruder within a preset monitoring window and generate an extrusion quality record sequence; 挤出质量波动因子确定模块,用于基于预设熔融质量指标对所述挤出质量记录序列进行分析,根据分析结果确定挤出质量波动因子;An extrusion quality fluctuation factor determination module, used for analyzing the extrusion quality record sequence based on a preset melting quality index, and determining the extrusion quality fluctuation factor according to the analysis result; 熔融温度区间生成模块,用于利用差示扫描量热仪对K个产品原材料样品进行熔融温度测试,获得K条热量变化曲线,并对所述K条热量变化曲线进行散点边缘识别,生成所述目标产品的熔融温度区间;A melting temperature interval generation module is used to perform melting temperature tests on K product raw material samples using a differential scanning calorimeter to obtain K heat change curves, and perform scattered point edge recognition on the K heat change curves to generate the melting temperature interval of the target product; 目标熔融温度区间生成模块,用于基于所述挤出质量波动因子对所述熔融温度区间进行修正,生成目标熔融温度区间;A target melting temperature interval generating module, used for correcting the melting temperature interval based on the extrusion quality fluctuation factor to generate a target melting temperature interval; 监测温度集合获得模块,用于在预设持续监测窗口持续对所述目标挤出机的熔融区进行温度监测,获得监测温度集合;A monitoring temperature set acquisition module, used for continuously monitoring the temperature of the melting zone of the target extruder in a preset continuous monitoring window to obtain a monitoring temperature set; 目标控制参数集合获得模块,用于基于所述监测温度集合与所述目标熔融温度区间确定目标熔融温度偏离值,根据所述目标熔融温度偏离值进行控制参数配置,获得目标控制参数集合,其中,所述目标控制参数包括加热温度、加热时间、熔融压力;a target control parameter set acquisition module, used to determine a target melting temperature deviation value based on the monitoring temperature set and the target melting temperature interval, configure control parameters according to the target melting temperature deviation value, and obtain a target control parameter set, wherein the target control parameters include heating temperature, heating time, and melting pressure; 参数调整模块,用于将所述目标控制参数集合传输至目标挤出机的控制单元进行参数调整。The parameter adjustment module is used to transmit the target control parameter set to the control unit of the target extruder for parameter adjustment.
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