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CN110055498B - Surface vapor deposition source and its production method, vapor deposition method, and vapor deposition device - Google Patents

Surface vapor deposition source and its production method, vapor deposition method, and vapor deposition device Download PDF

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CN110055498B
CN110055498B CN201810054822.6A CN201810054822A CN110055498B CN 110055498 B CN110055498 B CN 110055498B CN 201810054822 A CN201810054822 A CN 201810054822A CN 110055498 B CN110055498 B CN 110055498B
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evaporation
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王路
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BOE Technology Group Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/04Coating on selected surface areas, e.g. using masks
    • C23C14/042Coating on selected surface areas, e.g. using masks using masks
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/24Vacuum evaporation
    • C23C14/243Crucibles for source material
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/24Vacuum evaporation
    • C23C14/28Vacuum evaporation by wave energy or particle radiation
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K71/00Manufacture or treatment specially adapted for the organic devices covered by this subclass

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Abstract

本发明公开了一种面蒸镀源及其制作方法、蒸镀方法、蒸镀装置,涉及显示技术领域,所述面蒸镀源用于蒸镀待蒸镀材料,使其能够经过蒸镀掩膜版的开口在器件基板上形成薄膜,包括衬底,在所述衬底上设置有隔离墙结构,所述隔离墙结构在所述衬底上形成多个相互分隔的第一凹槽;所述第一凹槽用于承载待蒸镀材料;蒸镀时,所述蒸镀掩膜版的开口在所述衬底上的投影至少覆盖一个所述第一凹槽在衬底上的投影。所述面蒸镀源能够减小蒸镀掩膜版的开口区域外的阴影面积,有效提升蒸镀的精度,降低不同像素间的混色问题,进而减小像素尺寸,支撑更高分辨率的OLED显示产品。

Figure 201810054822

The invention discloses a surface evaporation source, a preparation method, an evaporation method and an evaporation device, and relates to the technical field of display. The opening of the stencil forms a thin film on the device substrate, which includes a substrate, and a partition wall structure is arranged on the substrate, and the partition wall structure forms a plurality of first grooves separated from each other on the substrate; The first groove is used to carry the material to be evaporated; during evaporation, the projection of the opening of the evaporation mask on the substrate at least covers the projection of the first groove on the substrate. The surface evaporation source can reduce the shadow area outside the opening area of the evaporation mask, effectively improve the precision of evaporation, and reduce the problem of color mixing between different pixels, thereby reducing the pixel size and supporting higher-resolution OLEDs Display products.

Figure 201810054822

Description

面蒸镀源及其制作方法、蒸镀方法、蒸镀装置Surface vapor deposition source and method for producing the same, vapor deposition method, and vapor deposition device

技术领域technical field

本发明涉及显示领域,尤其涉及面蒸镀源及其制作方法、蒸镀方法、蒸镀装置。The present invention relates to the field of display, and in particular, to a surface vapor deposition source and its manufacturing method, vapor deposition method and vapor deposition device.

背景技术Background technique

OLED(Organic Light Emitting Diode,有机电致发光二极管)显示面板具有自发光、响应速度快、轻薄、可制备柔性器件等优点。OLED (Organic Light Emitting Diode, organic electroluminescent diode) display panels have the advantages of self-luminescence, fast response speed, lightness and thinness, and flexible devices can be prepared.

蒸镀工艺是制备OLED显示面板的关键工序,在高精细的像素蒸镀中,会采用蒸镀掩膜版作为遮挡,蒸镀材料从蒸镀掩膜版开口蒸镀到对应的像素位置上,但目前由于采用点源和线源的方式,蒸镀源与背板之间会产生相对运动,导致掩膜版后面会出现蒸镀阴影区域,如果阴影区域过大,会导致像素的混色和色偏问题,为此减小阴影区域就可以有效提升蒸镀的精度,进而减小像素尺寸,支撑更高分辨率的OLED产品。The evaporation process is a key process in the preparation of OLED display panels. In high-precision pixel evaporation, an evaporation mask is used as a shield, and the evaporation material is evaporated from the opening of the evaporation mask to the corresponding pixel position. However, at present, due to the use of point sources and line sources, there will be relative motion between the evaporation source and the backplane, resulting in a shadow area of evaporation behind the mask. If the shadow area is too large, it will lead to pixel color mixing and color mixing. For this reason, reducing the shadow area can effectively improve the accuracy of evaporation, thereby reducing the pixel size and supporting higher-resolution OLED products.

同时,蒸镀装置方面,由于蒸镀源与器件基板间要保持比较大的距离,蒸镀装置腔室很高大,加工困难,并导致设备昂贵,抽真空时间长,进一步造成蒸镀工艺时间长。At the same time, in terms of the evaporation device, due to the relatively large distance between the evaporation source and the device substrate, the chamber of the evaporation device is very large, the processing is difficult, the equipment is expensive, the vacuuming time is long, and the evaporation process time is long. .

发明内容SUMMARY OF THE INVENTION

本发明的目的在于提供面蒸镀源及其制作方法、蒸镀方法、蒸镀装置,减小蒸镀的阴影区域,减小蒸镀装置体积,提高生产效率。The purpose of the present invention is to provide a surface vapor deposition source and its manufacturing method, vapor deposition method, and vapor deposition device, which can reduce the shadow area of vapor deposition, reduce the volume of the vapor deposition device, and improve production efficiency.

为了实现上述目的,本发明提供如下技术方案:In order to achieve the above object, the present invention provides the following technical solutions:

一种面蒸镀源,用于蒸镀待蒸镀材料,使其能够经过蒸镀掩膜版的开口在器件基板上形成薄膜,其特征在于,包括:A surface evaporation source is used for evaporating materials to be evaporated so that a thin film can be formed on a device substrate through an opening of an evaporation mask, and is characterized in that it includes:

衬底;substrate;

隔离墙结构,所述隔离墙结构设置在所述衬底上;a separation wall structure, the separation wall structure is arranged on the substrate;

其中,所述隔离墙结构在所述衬底上形成多个相互分隔的第一凹槽;Wherein, the isolation wall structure forms a plurality of mutually separated first grooves on the substrate;

所述第一凹槽用于承载待蒸镀材料;the first groove is used to carry the material to be evaporated;

所述第一凹槽被配置为,蒸镀时,所述蒸镀掩膜版的开口在所述衬底上的投影至少覆盖一个所述第一凹槽在衬底上的投影。The first groove is configured such that, during evaporation, the projection of the opening of the evaporation mask on the substrate at least covers a projection of the first groove on the substrate.

优选的,所述蒸镀掩膜版的开口在所述衬底上的投影覆盖N个所述第一凹槽在衬底上的投影,其中,N为正整数。Preferably, the projections of the openings of the evaporation mask on the substrate cover the projections of the N first grooves on the substrate, where N is a positive integer.

进一步的,至少部分所述第一凹槽在衬底上的投影与所述蒸镀掩膜版的开口在所述衬底上的投影完全重合。Further, the projection of at least part of the first groove on the substrate completely coincides with the projection of the opening of the evaporation mask on the substrate.

优选的,所述隔离墙结构的高度及所述第一凹槽的底面的特征尺寸为毫米或微米量级。Preferably, the height of the partition wall structure and the characteristic size of the bottom surface of the first groove are in the order of millimeters or micrometers.

进一步的,所述隔离墙结构的高度大于或等于10微米。Further, the height of the isolation wall structure is greater than or equal to 10 microns.

优选的,所述面蒸镀源包括蒸镀区和膜厚测试区;Preferably, the surface evaporation source includes an evaporation area and a film thickness test area;

所述蒸镀区用于蒸镀待蒸镀材料至器件基板;The evaporation area is used for evaporating the material to be evaporated to the device substrate;

所述膜厚测试区用于形成检测薄膜厚度所用的薄膜。The film thickness test area is used to form a thin film for detecting the thickness of the thin film.

优选的,所述衬底为透明的。Preferably, the substrate is transparent.

进一步的,所述第一凹槽的底部还设置有金属层;Further, the bottom of the first groove is also provided with a metal layer;

所述金属层的上表面到所述金属层的下表面的最大距离小于等于1微米;The maximum distance from the upper surface of the metal layer to the lower surface of the metal layer is less than or equal to 1 micron;

其中,所述金属层的上表面为所述金属层的远离所述第一凹槽的底面的表面;Wherein, the upper surface of the metal layer is the surface of the metal layer away from the bottom surface of the first groove;

所述金属层的下表面为所述金属层的与所述第一凹槽的底面相接触的表面。The lower surface of the metal layer is the surface of the metal layer that is in contact with the bottom surface of the first groove.

进一步的,所述金属层的上表面形成有表面微结构;Further, a surface microstructure is formed on the upper surface of the metal layer;

所述金属层与所述表面微结构为一体结构。The metal layer and the surface microstructure have an integral structure.

进一步的,所述表面微结构为栅格结构;Further, the surface microstructure is a grid structure;

所述栅格结构包括在所述金属层的上表面形成的多个第二凹槽;the grid structure includes a plurality of second grooves formed on the upper surface of the metal layer;

所述第二凹槽的深度为0.5-0.6微米,所述第二凹槽的底面到所述金属层的下表面的距离为0.4-0.5微米。The depth of the second groove is 0.5-0.6 μm, and the distance from the bottom surface of the second groove to the lower surface of the metal layer is 0.4-0.5 μm.

优选的,所述衬底与所述隔离墙结构为一体结构。Preferably, the substrate and the isolation wall structure are integral structures.

本发明还提供了一种面蒸镀源的制作方法,所述面蒸镀源用于蒸镀待蒸镀材料,使其能够经过蒸镀掩膜版的开口在器件基板上形成薄膜,其特征在于,包括:The present invention also provides a method for making a surface evaporation source, which is used for evaporating the material to be evaporated, so that a thin film can be formed on the device substrate through the opening of the evaporation mask, and its characteristics are: is, including:

提供一个衬底;provide a substrate;

在所述衬底上形成隔离墙结构;forming a separation wall structure on the substrate;

其中,所述隔离墙结构在所述衬底上形成多个相互分隔的第一凹槽;Wherein, the isolation wall structure forms a plurality of mutually separated first grooves on the substrate;

所述第一凹槽用于承载待蒸镀材料;the first groove is used to carry the material to be evaporated;

所述第一凹槽被配置为,蒸镀时,所述蒸镀掩膜版的开口在所述衬底上的投影至少覆盖一个所述第一凹槽在衬底上的投影。The first groove is configured such that, during evaporation, the projection of the opening of the evaporation mask on the substrate at least covers a projection of the first groove on the substrate.

进一步的,所述的面蒸镀源制作方法,还包括:Further, the method for making the surface evaporation source also includes:

在所述第一凹槽的底部形成金属层。A metal layer is formed at the bottom of the first groove.

进一步的,所述的面蒸镀源制作方法,还包括:Further, the method for making the surface evaporation source also includes:

刻蚀所述金属层的上表面形成表面微结构;etching the upper surface of the metal layer to form a surface microstructure;

其中,所述金属层的上表面为所述金属层的远离所述第一凹槽的底面的表面。Wherein, the upper surface of the metal layer is the surface of the metal layer that is away from the bottom surface of the first groove.

进一步的,所述刻蚀所述金属层的上表面的方法为干法刻蚀。Further, the method for etching the upper surface of the metal layer is dry etching.

优选的,在所述衬底上形成所述隔离墙结构的方法为刻蚀所述衬底形成所述隔离墙结构;Preferably, the method for forming the isolation wall structure on the substrate is to etch the substrate to form the isolation wall structure;

或者,在所述衬底上形成所述隔离墙结构的方法为在所述衬底上沉积隔离墙结构材料,刻蚀所述隔离墙结构材料形成所述隔离墙结构。Alternatively, the method for forming the isolation wall structure on the substrate is to deposit the isolation wall structure material on the substrate, and etch the isolation wall structure material to form the isolation wall structure.

本发明还提供了一种蒸镀方法,包括:The present invention also provides an evaporation method, comprising:

采用面蒸镀源蒸镀;Use surface evaporation source evaporation;

其中,所述面蒸镀源包括衬底;隔离墙结构,所述隔离墙结构设置在所述衬底上;所述隔离墙结构在所述衬底上形成多个相互分隔的第一凹槽;所述第一凹槽用于承载待蒸镀材料;所述第一凹槽被配置为,蒸镀时,所述蒸镀掩膜版的开口在所述衬底上的投影至少覆盖一个所述第一凹槽在衬底上的投影。Wherein, the surface evaporation source includes a substrate; a separation wall structure, the separation wall structure is arranged on the substrate; the separation wall structure forms a plurality of mutually separated first grooves on the substrate ; the first groove is used to carry the material to be evaporated; the first groove is configured such that during evaporation, the projection of the opening of the evaporation mask on the substrate at least covers one of the the projection of the first groove on the substrate.

优选的,所述蒸镀方法,还包括:Preferably, the evaporation method further includes:

在所述面蒸镀源的第一凹槽的开口侧设置器件基板;A device substrate is arranged on the opening side of the first groove of the surface evaporation source;

所述面蒸镀源和所述器件基板之间设置蒸镀掩膜版;An evaporation mask is arranged between the surface evaporation source and the device substrate;

将所述面蒸镀源与蒸镀掩膜版以及器件基板对位设置;aligning the surface evaporation source with the evaporation mask and the device substrate;

其中,所述面蒸镀源与所述蒸镀掩膜版之间的距离设置为毫米或微米量级;Wherein, the distance between the surface evaporation source and the evaporation mask is set to the order of millimeters or microns;

所述蒸镀掩膜版的开口在所述衬底上的投影覆盖N个所述第一凹槽在衬底上的投影,N为整数。The projections of the openings of the evaporation mask on the substrate cover the projections of the N first grooves on the substrate, where N is an integer.

进一步的,至少部分所述第一凹槽在衬底上的投影与所述蒸镀掩膜版的开口在所述衬底上的投影完全重合。Further, the projection of at least part of the first groove on the substrate completely coincides with the projection of the opening of the evaporation mask on the substrate.

优选的,所述蒸镀方法,还包括:Preferably, the evaporation method further includes:

向所述面蒸镀源的第一凹槽中填充待蒸镀材料;Filling the material to be evaporated into the first groove of the surface evaporation source;

向所述面蒸镀源的第一凹槽中填充待蒸镀材料后,去除所述面蒸镀源的隔离墙结构上方的待蒸镀材料。After the material to be evaporated is filled into the first groove of the surface evaporation source, the material to be evaporated above the isolation wall structure of the surface evaporation source is removed.

进一步的,向所述的面蒸镀源的第一凹槽中填充待蒸镀材料的方法为采用点或线蒸镀源蒸镀待蒸镀材料,使待蒸镀材料附着于所述面蒸镀源上。Further, the method of filling the first groove of the surface evaporation source with the material to be evaporated is to use a point or line evaporation source to evaporate the material to be evaporated, so that the material to be evaporated is attached to the surface evaporation. on the plating source.

进一步的,所述蒸镀方法,还包括:Further, the evaporation method also includes:

所述面蒸镀源的第一凹槽的开口向下设置,进行蒸镀。The opening of the first groove of the surface vapor deposition source is set downward for vapor deposition.

进一步的,去除所述面蒸镀源的隔离墙结构上方的待蒸镀材料的方法为采用激光倾斜照射去除所述隔离墙结构上方的待蒸镀材料;Further, the method for removing the material to be evaporated above the isolation wall structure of the surface evaporation source is to use laser oblique irradiation to remove the material to be evaporated above the isolation wall structure;

或者,去除所述面蒸镀源的隔离墙结构上方的待蒸镀材料的方法为通过粘附力强的薄膜材料,贴附在面蒸镀源上表面,将隔离墙结构上方的待蒸镀材料粘除;Alternatively, the method for removing the to-be-evaporated material above the partition wall structure of the surface evaporation source is to attach a film material with strong adhesion to the upper surface of the surface evaporation source, and remove the to-be-evaporated material above the partition wall structure. material sticking;

或者,去除所述面蒸镀源的隔离墙结构上方的待蒸镀材料的方法为利用真空吸附的方法,去除隔离墙结构上方的待蒸镀材料,通过控制真空部分和面蒸镀源的间隙,确保所述第一凹槽中的材料不被吸附走。Alternatively, the method for removing the material to be evaporated above the isolation wall structure of the surface evaporation source is to use a vacuum adsorption method to remove the material to be evaporated above the isolation wall structure, by controlling the gap between the vacuum part and the surface evaporation source. , to ensure that the material in the first groove is not adsorbed away.

优选的,所述蒸镀方法,还包括:Preferably, the evaporation method further includes:

加热所述面蒸镀源进行蒸镀;heating the surface evaporation source for evaporation;

其中,加热所述面蒸镀源的方法为采用面热源进行加热。Wherein, the method of heating the surface vapor deposition source is to use a surface heat source for heating.

优选的,加热所述面蒸镀源进行蒸镀;Preferably, heating the surface evaporation source for evaporation;

其中,加热所述面蒸镀源的方法为采用激光加热方式对面蒸镀源进行加热;Wherein, the method of heating the surface evaporation source is to heat the surface evaporation source by means of laser heating;

所述激光加热方式为采用激光照射所述面蒸镀源的选定区域,加热所述选定区域进行蒸镀。The laser heating method is to use a laser to irradiate a selected area of the surface vapor deposition source, and heat the selected area to perform vapor deposition.

本发明还提供了一种蒸镀装置,包括:The present invention also provides an evaporation device, comprising:

上述任一的面蒸镀源。Any of the above-mentioned surface vapor deposition sources.

附图说明Description of drawings

此处所说明的附图用来提供对本发明的进一步理解,构成本发明的一部分,本发明的示意性实施例及其说明用于解释本发明,并不构成对本发明的不当限定。在附图中:The accompanying drawings described herein are used to provide further understanding of the present invention and constitute a part of the present invention. The exemplary embodiments of the present invention and their descriptions are used to explain the present invention and do not constitute an improper limitation of the present invention. In the attached image:

图1为本发明实施例提供的面蒸镀源的结构示意图一;1 is a schematic structural diagram 1 of a surface evaporation source provided by an embodiment of the present invention;

图2为本发明实施例提供的一种面蒸镀源与蒸镀掩膜版、器件基板和膜厚仪的对应关系图一;FIG. 2 is a corresponding relationship diagram 1 of a surface evaporation source and an evaporation mask, a device substrate and a film thickness gauge provided by an embodiment of the present invention;

图3为本发明实施例提供的面蒸镀源的结构示意图二;3 is a second structural schematic diagram of a surface evaporation source provided by an embodiment of the present invention;

图4为本发明实施例提供的面蒸镀源的结构示意图三;4 is a third structural schematic diagram of a surface evaporation source provided by an embodiment of the present invention;

图5为本发明实施例提供的面蒸镀源的结构示意图四;FIG. 5 is a fourth schematic structural diagram of a surface evaporation source provided by an embodiment of the present invention;

图6为本发明实施例提供的采用点或线蒸镀源蒸镀,向面蒸镀源中填充待蒸镀材料的示意图;6 is a schematic diagram of filling the material to be evaporated into the surface evaporation source by using a point or line evaporation source for evaporation according to an embodiment of the present invention;

图7为本发明实施例提供的面蒸镀源的第一凹槽的开口向下的蒸镀方法的示意图;7 is a schematic diagram of an evaporation method in which the opening of the first groove of the surface evaporation source is downward according to an embodiment of the present invention;

图8为本发明实施例提供的采用激光倾斜照射去除隔离墙结构上方的待蒸镀材料的示意图。FIG. 8 is a schematic diagram of removing the material to be evaporated above the isolation wall structure by oblique laser irradiation according to an embodiment of the present invention.

附图标记:Reference number:

11-隔离墙结构, 12-第一凹槽,11-Separation wall structure, 12-First groove,

2-蒸镀掩膜版, 3-器件基板,2- Evaporation mask, 3- Device substrate,

4-膜厚仪, 5-金属层,4-Film thickness gauge, 5-Metal layer,

6-待蒸镀材料, 7-激光。6- Material to be evaporated, 7- Laser.

具体实施方式Detailed ways

为了进一步说明本发明实施例提供的面蒸镀源及其制作方法、蒸镀方法、蒸镀装置,下面结合说明书附图进行详细描述。In order to further illustrate the surface vapor deposition source and its manufacturing method, vapor deposition method, and vapor deposition device provided by the embodiments of the present invention, the following detailed description is given in conjunction with the accompanying drawings.

本发明实施例提供了一种面蒸镀源,用于蒸镀待蒸镀材料,使其能够经过蒸镀掩膜版的开口在器件基板上形成薄膜,如图1所示,包括:衬底,在所述衬底上设置有隔离墙结构11,所述隔离墙结构在所述衬底上形成多个相互分隔的第一凹槽12。蒸镀时,加热所述面蒸镀源,所述第一凹槽内的待蒸镀材料经过蒸镀掩膜版2的开口在器件基板3上形成薄膜。所述蒸镀掩膜版2的开口在所述衬底上的投影至少覆盖一个所述第一凹槽12在衬底上的投影。面蒸镀源,与点源和线源不同,蒸镀时不需要和器件基板形成相对运动,可以减少蒸镀掩膜版的开口区域外的阴影面积。进一步的,由于蒸镀掩膜版2的开口在衬底上的投影至少覆盖一个第一凹槽12,隔离墙结构11能够在蒸镀掩膜版的开口的范围内限制蒸镀时形成的蒸汽流的扩散,从而能够减小蒸镀掩膜版开口区域外的阴影面积,有效提升蒸镀的精度,降低不同像素间的混色问题,进而可以设计更小的像素尺寸,支撑更高分辨率的OLED显示产品。同时,本发明的面蒸镀源可更靠近蒸镀掩膜版和器件基板,减小面蒸镀源与蒸镀掩膜版和器件基板之间的距离,蒸镀装置的腔体可以大幅度降低高度,减小蒸镀装置腔室的体积,进而减少抽真空所需时间,减少蒸镀工艺时长。较小的蒸镀装置腔室的体积也可以减少沉积在器件基板范围外的材料的量,减少材料消耗。An embodiment of the present invention provides a surface evaporation source for evaporating materials to be evaporated so that a thin film can be formed on a device substrate through an opening of an evaporation mask, as shown in FIG. 1 , including: a substrate , a partition wall structure 11 is arranged on the substrate, and a plurality of mutually separated first grooves 12 are formed on the substrate by the partition wall structure. During evaporation, the surface evaporation source is heated, and the material to be evaporated in the first groove forms a thin film on the device substrate 3 through the opening of the evaporation mask 2 . The projection of the opening of the evaporation mask 2 on the substrate at least covers the projection of the first groove 12 on the substrate. Unlike point sources and line sources, surface vapor deposition sources do not need to form relative motion with the device substrate during vapor deposition, which can reduce the shadow area outside the opening area of the vapor deposition mask. Further, since the projection of the opening of the evaporation mask 2 on the substrate covers at least one first groove 12, the isolation wall structure 11 can limit the vapor formed during evaporation within the range of the opening of the evaporation mask. The diffusion of the flow can reduce the shadow area outside the opening area of the evaporation mask, effectively improve the accuracy of evaporation, and reduce the problem of color mixing between different pixels, so that a smaller pixel size can be designed to support higher resolution OLED display products. At the same time, the surface evaporation source of the present invention can be closer to the evaporation mask and the device substrate, reducing the distance between the surface evaporation source and the evaporation mask and the device substrate, and the cavity of the evaporation device can be greatly reduced. The height is reduced, the volume of the chamber of the evaporation device is reduced, the time required for vacuuming is reduced, and the duration of the evaporation process is reduced. The smaller volume of the vapor deposition apparatus chamber can also reduce the amount of material deposited outside the confines of the device substrate, reducing material consumption.

需要说明的是,此处的“衬底上”,可以指衬底上方,也可以指衬底的上部的部分。It should be noted that "on the substrate" here may refer to the upper part of the substrate, or may refer to the upper part of the substrate.

进一步的,所述蒸镀掩膜版的开口在所述衬底上的投影覆盖N个所述第一凹槽在衬底上的投影,其中,N为正整数。在蒸镀掩膜版开口范围的边缘正对的位置,存在隔离墙,能够限制边缘处的蒸汽流扩散,减小阴影区域。同时,蒸镀掩膜版开口范围内也存在若干隔离墙结构,能够进一步地把蒸汽流限制在固定的方向,更好地达到减小阴影区域的目的。Further, the projections of the openings of the evaporation mask on the substrate cover the projections of the N first grooves on the substrate, where N is a positive integer. At the position facing the edge of the opening range of the evaporation mask, there is a separation wall, which can limit the diffusion of the vapor flow at the edge and reduce the shadow area. At the same time, there are also several isolation wall structures within the opening range of the evaporation mask, which can further restrict the steam flow in a fixed direction and better achieve the purpose of reducing the shadow area.

进一步的,如图2所示,至少部分所述第一凹槽在衬底上的投影与所述蒸镀掩膜版的开口在所述衬底上的投影可以完全重合。即为,蒸镀时,面蒸镀源的第一凹槽可与蒸镀掩膜版的开口一一对应,隔离墙结构所在区域对应蒸镀掩膜版的遮挡区;或者有部分第一凹槽对应蒸镀掩膜版的遮挡区,其他第一凹槽与蒸镀掩膜版的开口一一对应。Further, as shown in FIG. 2 , the projection of at least part of the first groove on the substrate and the projection of the opening of the evaporation mask on the substrate may be completely coincident. That is, during evaporation, the first grooves of the surface evaporation source may correspond one-to-one with the openings of the evaporation mask, and the area where the isolation wall structure is located corresponds to the shielding area of the evaporation mask; or there may be part of the first recesses. The grooves correspond to the shielding areas of the evaporation mask, and the other first grooves correspond one-to-one with the openings of the evaporation mask.

图1中,隔离墙结构11的高度h及所述第一凹槽12的底面的特征尺寸w为毫米或微米量级。OLED显示面板子像素的尺寸一般为十几到几十微米,也即蒸镀掩膜版2的开口也为毫米或微米量级。第一凹槽开口较小,而隔离墙结构与较小的第一凹槽开口的特征尺寸相比具有一定的高度,能够精细地控制蒸镀时形成的蒸汽流的扩散。可减小蒸镀掩膜版开口区域外的阴影面积,有效提升蒸镀的精度。In FIG. 1 , the height h of the isolation wall structure 11 and the characteristic dimension w of the bottom surface of the first groove 12 are in the order of millimeters or micrometers. The size of the sub-pixels of the OLED display panel is generally ten to several tens of micrometers, that is, the opening of the evaporation mask 2 is also in the order of millimeters or micrometers. The opening of the first groove is small, and the isolation wall structure has a certain height compared with the characteristic size of the smaller opening of the first groove, which can finely control the diffusion of the vapor flow formed during evaporation. The shadow area outside the opening area of the evaporation mask can be reduced, and the precision of evaporation can be effectively improved.

进一步的,隔离墙结构11的高度h大于或等于10微米,保证隔离墙结构与第一凹槽的底面的特征尺寸相比具有一定高度,可有效限制蒸汽流扩散。Further, the height h of the isolation wall structure 11 is greater than or equal to 10 microns, which ensures that the isolation wall structure has a certain height compared with the characteristic size of the bottom surface of the first groove, which can effectively limit the diffusion of steam flow.

需要说明的是,本发明中所述的底面的特征尺寸是指底面上任一两点之间距离的最大值。本发明中所述的毫米或微米量级指小于等于10毫米大于等于0.1微米的尺寸范围中的任一数值。It should be noted that the characteristic size of the bottom surface described in the present invention refers to the maximum value of the distance between any two points on the bottom surface. The millimeter or micrometer scale mentioned in the present invention refers to any value in the size range of 10 millimeters or less and greater than or equal to 0.1 micrometers.

优选的,如图3所示,面蒸镀源包括蒸镀区A和膜厚测试区B。蒸镀时,所述蒸镀区A对应器件基板3设置,用来蒸镀待蒸镀材料至器件基板3。所述膜厚测试区B对应设置膜厚仪4,用来在膜厚仪探头上形成检测薄膜厚度所用的薄膜,进而检测薄膜的厚度。Preferably, as shown in FIG. 3 , the surface evaporation source includes an evaporation area A and a film thickness test area B. During vapor deposition, the vapor deposition area A is disposed corresponding to the device substrate 3 for vapor deposition of the material to be vapor deposited onto the device substrate 3 . The film thickness test area B is correspondingly provided with a film thickness gauge 4, which is used to form a thin film for detecting the thickness of the thin film on the probe of the film thickness gauge, so as to detect the thickness of the thin film.

优选的,所述衬底为透明的。采用激光加热衬底时,激光可穿过衬底加热待加热部分。具体的,衬底可以为高透过率玻璃基板,在激光透射过程中,吸收少,激光能量损失小,更多的激光能量能够用于加热。Preferably, the substrate is transparent. When a laser is used to heat the substrate, the laser can pass through the substrate to heat the portion to be heated. Specifically, the substrate can be a glass substrate with high transmittance. During the laser transmission process, the absorption is small, the loss of laser energy is small, and more laser energy can be used for heating.

进一步的,如图4所示,第一凹槽的底部还设置有金属层5。采用激光加热方式加热面蒸镀源时,激光穿过透明的衬底,被金属层吸收,产生热量加热面蒸镀源。Further, as shown in FIG. 4 , the bottom of the first groove is further provided with a metal layer 5 . When the surface evaporation source is heated by the laser heating method, the laser passes through the transparent substrate and is absorbed by the metal layer to generate heat to heat the surface evaporation source.

进一步的,所述金属层的上表面到所述金属层的下表面的最大距离小于等于1微米;Further, the maximum distance from the upper surface of the metal layer to the lower surface of the metal layer is less than or equal to 1 micron;

其中,所述金属层的上表面为所述金属层的远离所述第一凹槽的底面的表面;Wherein, the upper surface of the metal layer is the surface of the metal layer away from the bottom surface of the first groove;

所述金属层的下表面为所述金属层的与所述第一凹槽的底面相接触的表面。The lower surface of the metal layer is the surface of the metal layer that is in contact with the bottom surface of the first groove.

进一步的,如图5所示,金属层的上表面还可以具有表面微结构,表面微结构由刻蚀金属层表面直接形成,金属层与所述表面微结构为一体结构。制作表面微结构的目的是增加面蒸镀源与待蒸镀材料的接触面积,使热量快速传导。具体的,表面微结构可以为栅格结构,所述栅格结构形成多个第二凹槽。栅格结构的尺寸可以根据面蒸镀源的第一凹槽的尺寸及要填充的待蒸镀材料的量综合考虑。例如,第二凹槽的深度可以为0.5-0.6微米,第二凹槽的底面到金属层的下表面的距离为0.4-0.5微米,总厚度在1微米以内。由于一般蒸镀材料需要的厚度在0.2um以下,这样的微栅格可满足蒸镀材料的厚度要求。使用的金属材料包括Ti,Al等金属或其合金等。Further, as shown in FIG. 5 , the upper surface of the metal layer may also have a surface microstructure, the surface microstructure is directly formed by etching the surface of the metal layer, and the metal layer and the surface microstructure are integrated into a structure. The purpose of making the surface microstructure is to increase the contact area between the surface evaporation source and the material to be evaporated, so that the heat can be conducted quickly. Specifically, the surface microstructure may be a grid structure, and the grid structure forms a plurality of second grooves. The size of the grid structure can be comprehensively considered according to the size of the first groove of the surface evaporation source and the amount of the material to be evaporated to be filled. For example, the depth of the second groove may be 0.5-0.6 μm, the distance from the bottom surface of the second groove to the lower surface of the metal layer is 0.4-0.5 μm, and the total thickness is within 1 μm. Since the thickness required by the general evaporation material is below 0.2um, such a microgrid can meet the thickness requirements of the evaporation material. The metal materials used include Ti, Al and other metals or their alloys and the like.

本发明实施例还提供了一种面蒸镀源的制作方法,所述面蒸镀源用于蒸镀待蒸镀材料,使其能够经过蒸镀掩膜版的开口在器件基板上形成薄膜,其特征在于,包括:The embodiment of the present invention also provides a method for making a surface evaporation source, wherein the surface evaporation source is used for evaporating a material to be evaporated, so that a thin film can be formed on a device substrate through an opening of an evaporation mask, It is characterized in that it includes:

提供一个衬底;provide a substrate;

在所述衬底上形成隔离墙结构;forming a separation wall structure on the substrate;

其中,所述隔离墙结构在所述衬底上形成多个相互分隔的第一凹槽;Wherein, the isolation wall structure forms a plurality of mutually separated first grooves on the substrate;

所述第一凹槽用于承载待蒸镀材料;the first groove is used to carry the material to be evaporated;

所述第一凹槽被配置为,蒸镀时,所述蒸镀掩膜版的开口在所述衬底上的投影至少覆盖一个所述第一凹槽在衬底上的投影。The first groove is configured such that, during evaporation, the projection of the opening of the evaporation mask on the substrate at least covers a projection of the first groove on the substrate.

优选的,在所述衬底上形成所述隔离墙结构的方法为刻蚀所述衬底形成所述隔离墙结构;Preferably, the method for forming the isolation wall structure on the substrate is to etch the substrate to form the isolation wall structure;

或者,在所述衬底上形成所述隔离墙结构的方法为在所述衬底上沉积隔离墙结构材料,刻蚀隔离墙结构材料形成所述隔离墙结构。Alternatively, the method for forming the isolation wall structure on the substrate is to deposit the isolation wall structure material on the substrate, and etch the isolation wall structure material to form the isolation wall structure.

以上两种方式,可根据实际需求具体选择。The above two methods can be selected according to actual needs.

进一步的,所述的面蒸镀源制作方法,还包括:Further, the method for making the surface evaporation source also includes:

在所述第一凹槽的底部形成金属层。A metal layer is formed at the bottom of the first groove.

进一步的,所述的面蒸镀源制作方法,还包括:Further, the method for making the surface evaporation source also includes:

刻蚀所述金属层的上表面形成表面微结构;etching the upper surface of the metal layer to form a surface microstructure;

其中,所述金属层的上表面为所述金属层的远离所述第一凹槽的底面的表面。对应形成第一凹槽的方式不同,形成金属层的方式和工艺步骤可以不同,例如:Wherein, the upper surface of the metal layer is the surface of the metal layer that is away from the bottom surface of the first groove. Correspondingly, the method of forming the first groove is different, and the method and process steps of forming the metal layer can be different, for example:

形成金属层的方法可以为,先形成第一凹槽,之后沉积金属层,图案化去除不需要的金属层部分,并且,刻蚀第一凹槽的底部的金属层上表面形成表面微结构。The method of forming the metal layer may be: firstly forming the first groove, then depositing the metal layer, patterning to remove the unnecessary metal layer part, and etching the upper surface of the metal layer at the bottom of the first groove to form the surface microstructure.

形成金属层的方法还可以为,在衬底上沉积金属层,图案化去除不需要的金属层部分,并且,刻蚀金属层上表面形成表面微结构。之后沉积隔离墙结构材料。刻蚀所述隔离墙结构材料形成隔离墙结构,所述隔离墙结构在所述衬底上形成多个相互分隔的第一凹槽。刻蚀后,形成的第一凹槽底部为带有表面微结构的金属层。The method of forming the metal layer can also be: depositing the metal layer on the substrate, patterning to remove unnecessary parts of the metal layer, and etching the upper surface of the metal layer to form a surface microstructure. The wall structure material is then deposited. The isolation wall structure material is etched to form an isolation wall structure, and the isolation wall structure forms a plurality of mutually separated first grooves on the substrate. After etching, the bottom of the first groove formed is a metal layer with surface microstructures.

其中,所述刻蚀所述金属层的上表面的方法为干法刻蚀。采用干法刻蚀相比于湿法刻蚀,可更容易实现在金属层表面形成表面微结构的同时不刻蚀穿金属层。Wherein, the method for etching the upper surface of the metal layer is dry etching. Compared with wet etching, dry etching can more easily achieve the formation of surface microstructures on the surface of the metal layer without etching through the metal layer.

本发明的实施方式还提供了一种蒸镀方法,包括:Embodiments of the present invention also provide an evaporation method, comprising:

S1:向上述的面蒸镀源的第一凹槽中填充待蒸镀材料;S1: Fill the material to be evaporated into the first groove of the above-mentioned surface evaporation source;

S2:在面蒸镀源的第一凹槽的开口侧设置器件基板;S2: disposing a device substrate on the opening side of the first groove of the surface evaporation source;

S3:所述面蒸镀源和所述器件基板之间设置蒸镀掩膜版;S3: an evaporation mask is arranged between the surface evaporation source and the device substrate;

S4:将所述面蒸镀源与蒸镀掩膜版以及器件基板对位设置;S4: aligning the surface evaporation source with the evaporation mask and the device substrate;

S5:加热面蒸镀源进行蒸镀,蒸镀在高真空环境下进行。S5: Vapor deposition is performed by heating the surface vapor deposition source, and the vapor deposition is performed in a high vacuum environment.

其中,所述面蒸镀源包括衬底;隔离墙结构,所述隔离墙结构设置在所述衬底上;所述隔离墙结构在所述衬底上形成多个相互分隔的第一凹槽;所述第一凹槽用于承载待蒸镀材料;所述第一凹槽被配置为,蒸镀时,所述蒸镀掩膜版的开口在所述衬底上的投影至少覆盖一个所述第一凹槽在衬底上的投影。Wherein, the surface evaporation source includes a substrate; a separation wall structure, the separation wall structure is arranged on the substrate; the separation wall structure forms a plurality of mutually separated first grooves on the substrate ; the first groove is used to carry the material to be evaporated; the first groove is configured such that during evaporation, the projection of the opening of the evaporation mask on the substrate at least covers one of the the projection of the first groove on the substrate.

所述蒸镀掩膜版的开口在所述衬底上的投影可以覆盖N个所述第一凹槽在衬底上的投影,N为整数。The projections of the openings of the evaporation mask on the substrate may cover the projections of the N first grooves on the substrate, where N is an integer.

进一步的,至少部分所述第一凹槽在衬底上的投影与所述蒸镀掩膜版的开口在所述衬底上的投影完全重合。Further, the projection of at least part of the first groove on the substrate completely coincides with the projection of the opening of the evaporation mask on the substrate.

优选的,如图1所示,所述面蒸镀源与所述蒸镀掩膜版之间的距离d设置为毫米或微米量级。其中,面蒸镀源与蒸镀掩膜版之间的距离d为面蒸镀源的隔离墙结构的上表面与蒸镀掩膜版的下表面之间的距离。蒸镀中,蒸汽流的扩散虽然受到了面蒸镀源的隔离墙结构的限制,保持在一定的范围内,然而如果面蒸镀源与蒸镀掩膜版之间的距离过远,对蒸汽流的限制效果就会显著下降。将面蒸镀源与蒸镀掩膜版之间的距离设置为毫米或微米量级,保证了面蒸镀源对蒸汽流的限制效果能够更好的发挥,减小蒸镀掩膜版开口区域外的阴影面积,有效提升蒸镀的精度,降低不同像素间的混色问题,进而可以设计更小的像素尺寸,支撑更高分辨率的OLED显示产品。同时,本发明的面蒸镀源更靠近蒸镀掩膜版和器件基板,蒸镀装置的腔体可以大幅度降低高度,减小蒸镀装置腔室的体积,进而减少抽真空所需时间,减少蒸镀工艺时长。较小的蒸镀装置腔室的体积也可以减少沉积在器件基板范围外的材料的量,减少材料消耗。Preferably, as shown in FIG. 1 , the distance d between the surface evaporation source and the evaporation mask is set to the order of millimeters or micrometers. The distance d between the surface evaporation source and the evaporation mask is the distance between the upper surface of the partition wall structure of the surface evaporation source and the lower surface of the evaporation mask. In vapor deposition, although the diffusion of vapor flow is limited by the isolation wall structure of the surface vapor deposition source and kept within a certain range, if the distance between the surface vapor deposition source and the vapor deposition mask is too far, the vapor The effect of restricting the flow is significantly reduced. The distance between the surface evaporation source and the evaporation mask is set to the order of millimeters or microns to ensure that the surface evaporation source can better limit the steam flow and reduce the opening area of the evaporation mask. The external shadow area can effectively improve the accuracy of evaporation and reduce the problem of color mixing between different pixels, so that a smaller pixel size can be designed to support higher-resolution OLED display products. At the same time, the surface evaporation source of the present invention is closer to the evaporation mask and the device substrate, the height of the cavity of the evaporation device can be greatly reduced, the volume of the cavity of the evaporation device can be reduced, and the time required for vacuuming can be reduced. Reduce the evaporation process time. The smaller volume of the vapor deposition apparatus chamber can also reduce the amount of material deposited outside the confines of the device substrate, reducing material consumption.

其中,面蒸镀源可包括蒸镀区和膜厚测试区。蒸镀区对应设置所述器件基板,将待蒸镀材料通过蒸镀掩膜版的开口蒸镀到器件基板上;膜厚测试区对应设置膜厚仪,用来监测蒸镀的薄膜厚度。Wherein, the surface evaporation source may include an evaporation area and a film thickness test area. The device substrate is correspondingly arranged in the evaporation area, and the material to be evaporated is evaporated onto the device substrate through the opening of the evaporation mask; the film thickness test area is correspondingly arranged with a film thickness meter to monitor the thickness of the evaporated film.

进一步的,如图6所示,向面蒸镀源的第一凹槽中填充待蒸镀材料的方法为采用点或线蒸镀源蒸镀待蒸镀材料,使待蒸镀材料6附着于所述面蒸镀源上。附着于面蒸镀源上的待蒸镀材料的厚度可根据实际需求进行调节。同时,蒸镀过程中,保持蒸镀速度一致,点或线蒸镀源移动速度匀速,这种向面蒸镀源中填充待蒸镀材料的方法保证了各个第一凹槽中待蒸镀材料的厚度的均匀性,有利于使用面蒸镀源进行蒸镀时得到均匀致密的薄膜。并且,蒸镀待蒸镀材料附着于所述面蒸镀源上相当于一次材料升华提纯,有助于提高使用面蒸镀源蒸镀得到的薄膜的材料纯度,进而改善蒸镀制备的器件的性能。现有技术所采用的点或线蒸镀源,为了蒸镀薄膜的均匀性,需要使蒸镀源和器件基板保持一定的距离。本实施例所述蒸镀源,由于各个第一凹槽中待蒸镀材料的厚度是均匀的,保证了面蒸镀源各个凹槽的蒸镀速度均匀。在保证均匀性的同时,可以使面蒸镀源非常靠近蒸镀掩膜版和器件基板设置,距离可以为毫米或微米量级。由于OLED显示用蒸镀掩膜版的开口也为毫米或微米量级,隔离墙结构能够精确控制蒸镀时形成的蒸汽流的扩散,可减小蒸镀掩膜版开口区域外的阴影面积,有效提升蒸镀的精度,降低不同像素间的混色问题,进而减小像素尺寸,支撑更高分辨率的OLED显示产品。并且,由于面蒸镀源可更靠近蒸镀掩膜版和器件基板设置,距离可以为毫米或微米量级,蒸镀装置的腔体可以大幅度降低高度,减小蒸镀装置腔室的体积,进而减少抽真空所需时间,减少蒸镀工艺时长。较小的蒸镀装置腔室的体积也可以减少沉积在器件基板范围外的材料的量,减少材料消耗。Further, as shown in FIG. 6 , the method of filling the material to be evaporated into the first groove facing the evaporation source is to use a point or line evaporation source to evaporate the material to be evaporated, so that the material to be evaporated 6 is attached to the evaporation source. on the surface evaporation source. The thickness of the material to be evaporated attached to the surface evaporation source can be adjusted according to actual needs. At the same time, during the evaporation process, the evaporation speed is kept the same, and the moving speed of the point or line evaporation source is uniform. This method of filling the material to be evaporated into the surface evaporation source ensures that the material to be evaporated in each first groove is The uniformity of the thickness is beneficial to obtain a uniform and dense film when using a surface vapor deposition source for vapor deposition. In addition, the deposition of the material to be evaporated on the surface evaporation source is equivalent to a sublimation purification of the material, which helps to improve the material purity of the thin film evaporated by using the surface evaporation source, thereby improving the quality of the device prepared by evaporation. performance. The point or line vapor deposition source used in the prior art needs to keep a certain distance between the vapor deposition source and the device substrate for the uniformity of the vapor deposition film. In the evaporation source described in this embodiment, since the thickness of the material to be evaporated in each of the first grooves is uniform, it is ensured that the evaporation speed of each groove of the surface evaporation source is uniform. While ensuring uniformity, the surface evaporation source can be placed very close to the evaporation mask and the device substrate, and the distance can be on the order of millimeters or micrometers. Since the opening of the evaporation mask for OLED display is also in the order of millimeters or microns, the isolation wall structure can precisely control the diffusion of the vapor flow formed during evaporation, which can reduce the shadow area outside the opening area of the evaporation mask. Effectively improve the accuracy of evaporation, reduce the problem of color mixing between different pixels, and then reduce the pixel size to support higher-resolution OLED display products. Moreover, since the surface evaporation source can be set closer to the evaporation mask and the device substrate, the distance can be in the order of millimeters or microns, the height of the cavity of the evaporation device can be greatly reduced, and the volume of the cavity of the evaporation device can be reduced. , thereby reducing the time required for vacuuming and reducing the duration of the evaporation process. The smaller volume of the vapor deposition apparatus chamber can also reduce the amount of material deposited outside the confines of the device substrate, reducing material consumption.

采用上述方式将待蒸镀材料填充到面蒸镀源的第一凹槽中的情况下,去除面蒸镀源的隔离墙结构上方的待蒸镀材料后,如图7所示,可将面蒸镀源的第一凹槽的开口向下设置,进行蒸镀。待蒸镀材料6以薄膜的形式附着于面蒸镀源上,因此,待蒸镀材料6在之后的整个设置及蒸镀过程中不会掉落。蒸镀掩膜版2和器件基板3依次设置于面蒸镀源下方。蒸镀时,产生的蒸汽气流向下通过蒸镀掩膜版2的开口,蒸镀到器件基板上。方向向下的蒸汽气流,结合面蒸镀源的隔离墙结构对蒸汽气流方向的限制,相比于面蒸镀源的凹槽的开口向上设置的情况,可进一步减小蒸镀掩膜版开口区域外的阴影面积,有效提升蒸镀的精度。When the material to be evaporated is filled into the first groove of the surface evaporation source in the above manner, after removing the material to be evaporated above the isolation wall structure of the surface evaporation source, as shown in FIG. 7 , the surface The opening of the first groove of the evaporation source is set downward, and evaporation is performed. The material to be evaporated 6 is attached to the surface evaporation source in the form of a thin film, so the material to be evaporated 6 will not fall off during the entire setting and evaporation process thereafter. The evaporation mask 2 and the device substrate 3 are sequentially arranged below the surface evaporation source. During vapor deposition, the generated vapor flows downward through the openings of the vapor deposition mask 2 and is vapor deposited onto the device substrate. The downward steam flow, combined with the restriction of the steam flow direction by the partition wall structure of the surface evaporation source, can further reduce the opening of the evaporation mask compared to the case where the opening of the groove of the surface evaporation source is set upward. The shadow area outside the area can effectively improve the accuracy of evaporation.

需要说明的是,这里的“第一凹槽的开口向下”中的“向下”是指沿重力方向向下。It should be noted that the "downward" in "the opening of the first groove is downward" here refers to downward in the direction of gravity.

并且,在上述实施例中,去除面蒸镀源的隔离墙结构上方的待蒸镀材料的方式可以根据实际需要进行选择,包括但不限于下面三种:Moreover, in the above embodiment, the method of removing the material to be evaporated above the isolation wall structure of the surface evaporation source can be selected according to actual needs, including but not limited to the following three:

去除面蒸镀源的隔离墙结构上方的待蒸镀材料的方式一,如图8所示,可以为采用激光7倾斜照射去除面蒸镀源的隔离墙结构上方的待蒸镀材料。采用倾斜一定角度的激光扫描整个面蒸镀源,激光只能照射到隔离墙结构上方而无法照射到第一凹槽底部,因此,隔离墙结构上方的待蒸镀材料被去除,第一凹槽中的材料得以保留。具体的扫描激光角度可以根据面蒸镀源的第一凹槽的具体尺寸进行选择,例如,扫描激光与面蒸镀源平面的法线方向的夹角为70-80度。The first method of removing the material to be evaporated above the partition wall structure of the surface vapor deposition source, as shown in FIG. 8 , may be to use the laser 7 to irradiate obliquely to remove the material to be evaporated above the partition wall structure of the surface evaporation source. The entire surface of the evaporation source is scanned by a laser inclined at a certain angle. The laser can only be irradiated on the top of the isolation wall structure and cannot be irradiated to the bottom of the first groove. Therefore, the material to be evaporated above the isolation wall structure is removed, and the first groove material is preserved. The specific scanning laser angle can be selected according to the specific size of the first groove of the surface evaporation source, for example, the angle between the scanning laser and the normal direction of the surface evaporation source plane is 70-80 degrees.

去除面蒸镀源的隔离墙结构上方的待蒸镀材料的方式二,可以为通过粘附力强的薄膜材料,贴附在面蒸镀源上表面,将面蒸镀源的隔离墙结构上方的待蒸镀材料粘除。The second method of removing the material to be evaporated above the isolation wall structure of the surface evaporation source can be to attach a film material with strong adhesion to the upper surface of the surface evaporation source, and place the surface evaporation source above the isolation wall structure. The material to be evaporated is removed.

去除面蒸镀源的隔离墙结构上方的待蒸镀材料的方式三,可以为利用真空吸附的方法,去除面蒸镀源的隔离墙结构上方的待蒸镀材料,通过控制真空部分和面蒸镀源的间隙,确保第一凹槽中的材料不被吸附走。The third method of removing the material to be evaporated above the isolation wall structure of the surface evaporation source may be to use a vacuum adsorption method to remove the material to be evaporated above the isolation wall structure of the surface evaporation source, and by controlling the vacuum part and surface evaporation The gap between the plating source ensures that the material in the first groove is not adsorbed away.

加热面蒸镀源蒸镀的方法,可选的,可以为采用面热源对面蒸镀源进行加热。The method for heating the surface vapor deposition source for vapor deposition, optionally, may be to use a surface heat source to heat the surface vapor deposition source.

加热面蒸镀源蒸镀的方法还可以为采用激光扫描的方式对面蒸镀源进行加热。激光扫描的速度和强度是确定的,这样可以确保蒸镀的均一性。The method of heating the surface vapor deposition source for vapor deposition may also be to heat the surface vapor deposition source by means of laser scanning. The speed and intensity of the laser scanning is determined, which ensures uniformity of evaporation.

其中,采用激光加热的方法,可采用激光扫描选定区域,进行精准蒸镀。由于激光非常好的方向性,激光照射的区域可以精确控制。因此,可以通过控制照射区域的范围,加热部分面蒸镀源,蒸镀部分第一凹槽内的待蒸镀材料。配合上述面蒸镀源的隔离墙结构对蒸汽流的控制,无需配合蒸镀掩膜版即可蒸镀得到图案化的薄膜。并且,可通过控制激光的强度,扫描速度等,控制加热速率,可以以不同的蒸镀速率,得到不同厚度的薄膜。Among them, the method of laser heating can be used to scan the selected area by laser for precise evaporation. Due to the very good directionality of the laser, the area irradiated by the laser can be precisely controlled. Therefore, by controlling the range of the irradiation area, part of the surface evaporation source can be heated, and part of the material to be evaporated in the first groove can be evaporated. In combination with the control of the vapor flow by the isolation wall structure of the above-mentioned surface vapor deposition source, a patterned thin film can be obtained by vapor deposition without matching with an vapor deposition mask. In addition, the heating rate can be controlled by controlling the intensity of the laser, scanning speed, etc., and films with different thicknesses can be obtained at different evaporation rates.

在上述实施方式的描述中,具体特征、结构、材料或者特点可以在任何的一个或多个实施例或示例中以合适的方式结合。In the foregoing description of the embodiments, the particular features, structures, materials or characteristics may be combined in any suitable manner in any one or more of the embodiments or examples.

以上所述,仅为本发明的具体实施方式,但本发明的保护范围并不局限于此,任何熟悉本技术领域的技术人员在本发明揭露的技术范围内,可轻易想到变化或替换,都应涵盖在本发明的保护范围之内。因此,本发明的保护范围应以所述权利要求的保护范围为准。The above are only specific embodiments of the present invention, but the protection scope of the present invention is not limited thereto. Any person skilled in the art can easily think of changes or substitutions within the technical scope disclosed by the present invention. should be included within the protection scope of the present invention. Therefore, the protection scope of the present invention should be based on the protection scope of the claims.

Claims (21)

1. The utility model provides a face coating by vaporization source for the coating by vaporization treats coating by vaporization material, makes its opening that can pass through the coating by vaporization mask version form the film on the device substrate, its characterized in that includes:
a substrate, the substrate being transparent;
the isolation wall structure is fixedly arranged on the substrate;
the isolation wall structure forms a plurality of first grooves which are separated from each other on the substrate; the height of the isolation wall structure and the characteristic dimension of the bottom surface of the first groove are any numerical value in the dimension range of being less than or equal to 10 millimeters and greater than or equal to 0.1 micrometer; the first groove is used for bearing a material to be evaporated; the first grooves are configured in such a way that the projection of one opening of the evaporation mask on the substrate covers the projection of N first grooves on the substrate during evaporation, wherein N is a positive integer;
the metal layer is arranged at the bottom of the first groove; the maximum distance from the upper surface of the metal layer to the lower surface of the metal layer is less than or equal to 1 micrometer; the upper surface of the metal layer is the surface of the metal layer, which is far away from the bottom surface of the first groove; the lower surface of the metal layer is a surface of the metal layer which is in contact with the bottom surface of the first groove.
2. The surface evaporation source according to claim 1, wherein the projection of at least part of the first recess on the substrate is completely coincident with the projection of the opening of the evaporation mask on the substrate.
3. The surface evaporation source according to claim 1, wherein the height of the partition wall structure is greater than or equal to 10 μm.
4. The source of claim 1, wherein the source comprises an evaporation zone and a film thickness test zone;
the evaporation area is used for evaporating a material to be evaporated to the device substrate;
the film thickness test area is used for forming a film for detecting the thickness of the film.
5. The source of claim 1, wherein the metal layer has a surface microstructure formed on an upper surface thereof;
the metal layer and the surface microstructure are of an integral structure.
6. The surface evaporation source according to claim 5, wherein the surface microstructure is a grid structure;
the grid structure includes a plurality of second grooves formed on an upper surface of the metal layer;
the depth of the second groove is 0.5-0.6 microns, and the distance from the bottom surface of the second groove to the lower surface of the metal layer is 0.4-0.5 microns.
7. The surface evaporation source according to claim 1, wherein the substrate and the isolation wall structure are of a unitary structure.
8. A method for manufacturing a surface evaporation source, which is used for evaporating a material to be evaporated so that the material can form a thin film on a device substrate through an opening of an evaporation mask, is characterized by comprising the following steps of:
providing a substrate, wherein the substrate is transparent;
forming an isolation wall structure on the substrate;
the isolation wall structure forms a plurality of first grooves which are separated from each other on the substrate; the height of the isolation wall structure and the characteristic dimension of the bottom surface of the first groove are any numerical value in the dimension range of being less than or equal to 10 millimeters and greater than or equal to 0.1 micrometer; the first groove is used for bearing a material to be evaporated; the first grooves are configured in such a way that the projection of one opening of the evaporation mask on the substrate covers the projection of N first grooves on the substrate during evaporation, wherein N is a positive integer;
forming a metal layer at the bottom of the first groove; the maximum distance from the upper surface of the metal layer to the lower surface of the metal layer is less than or equal to 1 micrometer; the upper surface of the metal layer is the surface of the bottom surface, far away from the first groove, of the metal layer; the lower surface of the metal layer is a surface of the metal layer which is in contact with the bottom surface of the first groove.
9. The method of claim 8, further comprising:
etching the upper surface of the metal layer to form a surface microstructure;
the upper surface of the metal layer is the surface of the bottom surface, far away from the first groove, of the metal layer.
10. The method of claim 9, wherein the etching the upper surface of the metal layer is dry etching.
11. The method of claim 9, wherein the method comprises:
the method for forming the isolation wall structure on the substrate comprises the steps of etching the substrate to form the isolation wall structure;
or, the method for forming the isolation wall structure on the substrate is to deposit an isolation wall structure material on the substrate and etch the isolation wall structure material to form the isolation wall structure.
12. An evaporation method, comprising:
adopting a surface evaporation source for evaporation;
the surface evaporation source is used for evaporating a material to be evaporated, so that the material can form a thin film on the device substrate through an opening of an evaporation mask, and the surface evaporation source comprises a substrate which is transparent; the isolation wall structure is fixedly arranged on the substrate; the isolation wall structure forms a plurality of first grooves which are separated from each other on the substrate; the height of the isolation wall structure and the characteristic dimension of the bottom surface of the first groove are any numerical value in a dimension range of being less than or equal to 10 millimeters and greater than or equal to 0.1 micrometer; the first groove is used for bearing a material to be evaporated; the first grooves are configured in such a way that the projection of one opening of the evaporation mask on the substrate covers the projection of N first grooves on the substrate during evaporation, wherein N is a positive integer; the metal layer is arranged at the bottom of the first groove; the maximum distance from the upper surface of the metal layer to the lower surface of the metal layer is less than or equal to 1 micrometer; the upper surface of the metal layer is the surface of the metal layer, which is far away from the bottom surface of the first groove; the lower surface of the metal layer is a surface of the metal layer which is in contact with the bottom surface of the first groove.
13. The vapor deposition method according to claim 12, further comprising:
arranging a device substrate on the opening side of the first groove of the surface evaporation source;
an evaporation mask is arranged between the surface evaporation source and the device substrate;
aligning the surface evaporation source with an evaporation mask plate and a device substrate;
wherein, the distance between the surface evaporation source and the evaporation mask is set to be millimeter or micron magnitude.
14. A vapor deposition method according to claim 13, wherein a projection of at least part of the first recess on the substrate completely coincides with a projection of the opening of the vapor deposition mask on the substrate.
15. A vapor deposition method according to claim 12, further comprising:
filling a material to be evaporated into the first groove of the surface evaporation source;
and after filling a material to be evaporated in the first groove of the surface evaporation source, removing the material to be evaporated above the isolation wall structure of the surface evaporation source.
16. A deposition method according to claim 15, wherein the first groove of the surface deposition source is filled with a material to be deposited by a dot or line deposition source, and the material to be deposited is attached to the surface deposition source.
17. A vapor deposition method according to claim 16, further comprising:
and an opening of the first groove of the surface evaporation source is arranged downwards for evaporation.
18. A vapor deposition method according to claim 15, wherein:
the method for removing the material to be evaporated above the isolation wall structure of the surface evaporation source comprises the steps of removing the material to be evaporated above the isolation wall structure by oblique laser irradiation;
or, the method for removing the material to be evaporated above the isolation wall structure of the surface evaporation source is to stick and remove the material to be evaporated above the isolation wall structure by attaching the film material with strong adhesive force to the upper surface of the surface evaporation source;
or, the method for removing the material to be evaporated above the isolation wall structure of the surface evaporation source is a method of removing the material to be evaporated above the isolation wall structure by using vacuum adsorption, and the material in the first groove is ensured not to be adsorbed away by controlling the gap between the vacuum part and the surface evaporation source.
19. A vapor deposition method according to claim 12, further comprising:
heating the surface evaporation source for evaporation;
the method for heating the surface evaporation source adopts a surface heat source for heating.
20. A vapor deposition method according to claim 12, further comprising:
heating the surface evaporation source for evaporation;
the method for heating the surface evaporation source comprises the steps of heating the surface evaporation source in a laser heating mode;
the laser heating mode is to irradiate a selected area of the surface evaporation source by laser and heat the selected area for evaporation.
21. An evaporation apparatus, comprising:
the surface evaporation source according to any one of claims 1 to 7.
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CN112397674B (en) * 2019-08-19 2022-04-12 京东方科技集团股份有限公司 Manufacturing method of display substrate and mask plate assembly
CN115287603B (en) * 2022-08-02 2023-09-12 广东广纳芯科技有限公司 Vapor deposition method
CN115312608B (en) * 2022-08-26 2025-04-15 三一硅能(株洲)有限公司 Passivation contact structure, solar cell and preparation method
CN116162894B (en) * 2023-02-28 2024-09-10 京东方科技集团股份有限公司 Mask plate and manufacturing method thereof
CN116377394A (en) * 2023-04-04 2023-07-04 上海天马微电子有限公司 Evaporation device, evaporation method and organic light emitting display panel

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101078104A (en) * 2006-05-23 2007-11-28 株式会社细美事 Linear evaporator for manufacturing organic light emitting device using numerous crucibles
CN102959121A (en) * 2010-08-30 2013-03-06 夏普株式会社 Vapor deposition method, vapor deposition device, and organic el display device
CN105283576B (en) * 2013-06-11 2017-03-08 夏普株式会社 Limiting plate unit, vapor deposition unit, and vapor deposition device
CN106835028A (en) * 2017-03-10 2017-06-13 京东方科技集团股份有限公司 A kind of vapor deposition source, vapor deposition device and vapor deposition method
CN107425144A (en) * 2017-08-21 2017-12-01 江苏集萃有机光电技术研究所有限公司 The preparation method of OLED evaporation sources, evaporated device and oled panel pel array

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101078104A (en) * 2006-05-23 2007-11-28 株式会社细美事 Linear evaporator for manufacturing organic light emitting device using numerous crucibles
CN102959121A (en) * 2010-08-30 2013-03-06 夏普株式会社 Vapor deposition method, vapor deposition device, and organic el display device
CN105283576B (en) * 2013-06-11 2017-03-08 夏普株式会社 Limiting plate unit, vapor deposition unit, and vapor deposition device
CN107083531A (en) * 2013-06-11 2017-08-22 夏普株式会社 Limit Slab element and deposition unit and evaporation coating device
CN106835028A (en) * 2017-03-10 2017-06-13 京东方科技集团股份有限公司 A kind of vapor deposition source, vapor deposition device and vapor deposition method
CN107425144A (en) * 2017-08-21 2017-12-01 江苏集萃有机光电技术研究所有限公司 The preparation method of OLED evaporation sources, evaporated device and oled panel pel array

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