CN110840791B - Lip color cosmetic product and preparation method thereof - Google Patents
Lip color cosmetic product and preparation method thereof Download PDFInfo
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- CN110840791B CN110840791B CN201911237930.8A CN201911237930A CN110840791B CN 110840791 B CN110840791 B CN 110840791B CN 201911237930 A CN201911237930 A CN 201911237930A CN 110840791 B CN110840791 B CN 110840791B
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- color cosmetic
- lip color
- mica
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 131
- 238000002360 preparation method Methods 0.000 title claims abstract description 59
- 238000004519 manufacturing process Methods 0.000 title description 2
- 239000010445 mica Substances 0.000 claims abstract description 131
- 229910052618 mica group Inorganic materials 0.000 claims abstract description 131
- VQCBHWLJZDBHOS-UHFFFAOYSA-N erbium(iii) oxide Chemical compound O=[Er]O[Er]=O VQCBHWLJZDBHOS-UHFFFAOYSA-N 0.000 claims abstract description 74
- 239000000049 pigment Substances 0.000 claims abstract description 66
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 62
- 244000179291 Mahonia aquifolium Species 0.000 claims abstract description 49
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 claims abstract description 48
- SIWVEOZUMHYXCS-UHFFFAOYSA-N oxo(oxoyttriooxy)yttrium Chemical compound O=[Y]O[Y]=O SIWVEOZUMHYXCS-UHFFFAOYSA-N 0.000 claims abstract description 41
- RVGRUAULSDPKGF-UHFFFAOYSA-N Poloxamer Chemical compound C1CO1.CC1CO1 RVGRUAULSDPKGF-UHFFFAOYSA-N 0.000 claims abstract description 36
- 239000003921 oil Substances 0.000 claims abstract description 36
- 235000019198 oils Nutrition 0.000 claims abstract description 36
- 229960000502 poloxamer Drugs 0.000 claims abstract description 36
- 229920001983 poloxamer Polymers 0.000 claims abstract description 36
- 239000001100 (2S)-5,7-dihydroxy-2-(3-hydroxy-4-methoxyphenyl)chroman-4-one Substances 0.000 claims abstract description 29
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims abstract description 29
- 108010073771 Soybean Proteins Proteins 0.000 claims abstract description 29
- REZZEXDLIUJMMS-UHFFFAOYSA-M dimethyldioctadecylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCCCC[N+](C)(C)CCCCCCCCCCCCCCCCCC REZZEXDLIUJMMS-UHFFFAOYSA-M 0.000 claims abstract description 29
- AIONOLUJZLIMTK-AWEZNQCLSA-N hesperetin Chemical compound C1=C(O)C(OC)=CC=C1[C@H]1OC2=CC(O)=CC(O)=C2C(=O)C1 AIONOLUJZLIMTK-AWEZNQCLSA-N 0.000 claims abstract description 29
- 229960001587 hesperetin Drugs 0.000 claims abstract description 29
- AIONOLUJZLIMTK-UHFFFAOYSA-N hesperetin Natural products C1=C(O)C(OC)=CC=C1C1OC2=CC(O)=CC(O)=C2C(=O)C1 AIONOLUJZLIMTK-UHFFFAOYSA-N 0.000 claims abstract description 29
- 235000010209 hesperetin Nutrition 0.000 claims abstract description 29
- FTODBIPDTXRIGS-UHFFFAOYSA-N homoeriodictyol Natural products C1=C(O)C(OC)=CC(C2OC3=CC(O)=CC(O)=C3C(=O)C2)=C1 FTODBIPDTXRIGS-UHFFFAOYSA-N 0.000 claims abstract description 29
- 229910052700 potassium Inorganic materials 0.000 claims abstract description 29
- 239000011591 potassium Substances 0.000 claims abstract description 29
- 235000019710 soybean protein Nutrition 0.000 claims abstract description 26
- 244000183685 Citrus aurantium Species 0.000 claims abstract description 24
- 235000007716 Citrus aurantium Nutrition 0.000 claims abstract description 24
- SHBUUTHKGIVMJT-UHFFFAOYSA-N Hydroxystearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OO SHBUUTHKGIVMJT-UHFFFAOYSA-N 0.000 claims abstract description 24
- 235000019482 Palm oil Nutrition 0.000 claims abstract description 24
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 24
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims abstract description 24
- 235000012000 cholesterol Nutrition 0.000 claims abstract description 24
- 229940072106 hydroxystearate Drugs 0.000 claims abstract description 24
- 239000002540 palm oil Substances 0.000 claims abstract description 24
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 24
- 235000002906 tartaric acid Nutrition 0.000 claims abstract description 24
- 239000011975 tartaric acid Substances 0.000 claims abstract description 24
- TXBCBTDQIULDIA-UHFFFAOYSA-N 2-[[3-hydroxy-2,2-bis(hydroxymethyl)propoxy]methyl]-2-(hydroxymethyl)propane-1,3-diol Chemical compound OCC(CO)(CO)COCC(CO)(CO)CO TXBCBTDQIULDIA-UHFFFAOYSA-N 0.000 claims abstract description 21
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 21
- 229930006000 Sucrose Natural products 0.000 claims abstract description 21
- 229960004793 sucrose Drugs 0.000 claims abstract description 21
- OYZZJAQBPGMCDN-UHFFFAOYSA-N 18,18,18-trihydroxyoctadecanoic acid Chemical compound OC(=O)CCCCCCCCCCCCCCCCC(O)(O)O OYZZJAQBPGMCDN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000047 product Substances 0.000 claims description 119
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 36
- 238000001035 drying Methods 0.000 claims description 35
- QZXSMBBFBXPQHI-UHFFFAOYSA-N N-(dodecanoyl)ethanolamine Chemical compound CCCCCCCCCCCC(=O)NCCO QZXSMBBFBXPQHI-UHFFFAOYSA-N 0.000 claims description 28
- 238000010438 heat treatment Methods 0.000 claims description 24
- 239000000706 filtrate Substances 0.000 claims description 18
- 238000001914 filtration Methods 0.000 claims description 18
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 18
- 239000000843 powder Substances 0.000 claims description 18
- 238000002156 mixing Methods 0.000 claims description 17
- 238000001238 wet grinding Methods 0.000 claims description 16
- 206010015150 Erythema Diseases 0.000 claims description 15
- 235000009754 Vitis X bourquina Nutrition 0.000 claims description 15
- 235000012333 Vitis X labruscana Nutrition 0.000 claims description 15
- 235000014787 Vitis vinifera Nutrition 0.000 claims description 15
- 238000003756 stirring Methods 0.000 claims description 15
- 239000000463 material Substances 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 9
- XKMYWNHZAQUEPY-YZGJEOKZSA-N [(3s,8s,9s,10r,13r,14s,17r)-10,13-dimethyl-17-[(2r)-6-methylheptan-2-yl]-2,3,4,7,8,9,11,12,14,15,16,17-dodecahydro-1h-cyclopenta[a]phenanthren-3-yl] 12-hydroxyoctadecanoate Chemical compound C([C@@H]12)C[C@]3(C)[C@@H]([C@H](C)CCCC(C)C)CC[C@H]3[C@@H]1CC=C1[C@]2(C)CC[C@H](OC(=O)CCCCCCCCCCC(O)CCCCCC)C1 XKMYWNHZAQUEPY-YZGJEOKZSA-N 0.000 claims description 7
- 229940072104 cholesteryl hydroxystearate Drugs 0.000 claims description 7
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 5
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 3
- 240000004153 Hibiscus sabdariffa Species 0.000 claims description 3
- 235000001018 Hibiscus sabdariffa Nutrition 0.000 claims description 3
- 240000000249 Morus alba Species 0.000 claims description 3
- 235000008708 Morus alba Nutrition 0.000 claims description 3
- 240000001890 Ribes hudsonianum Species 0.000 claims description 3
- 235000016954 Ribes hudsonianum Nutrition 0.000 claims description 3
- 235000001466 Ribes nigrum Nutrition 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims description 3
- 235000016911 Ribes sativum Nutrition 0.000 claims description 2
- 235000002355 Ribes spicatum Nutrition 0.000 claims description 2
- 244000281209 Ribes triste Species 0.000 claims description 2
- 235000016897 Ribes triste Nutrition 0.000 claims description 2
- 240000006365 Vitis vinifera Species 0.000 claims 1
- 244000060011 Cocos nucifera Species 0.000 abstract 1
- 235000013162 Cocos nucifera Nutrition 0.000 abstract 1
- 235000014113 dietary fatty acids Nutrition 0.000 abstract 1
- 229930195729 fatty acid Natural products 0.000 abstract 1
- 239000000194 fatty acid Substances 0.000 abstract 1
- 150000004665 fatty acids Chemical class 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 25
- 241000219095 Vitis Species 0.000 description 14
- 210000003491 skin Anatomy 0.000 description 12
- 239000006185 dispersion Substances 0.000 description 8
- 238000001514 detection method Methods 0.000 description 7
- 230000000694 effects Effects 0.000 description 6
- 238000011156 evaluation Methods 0.000 description 5
- 239000005720 sucrose Substances 0.000 description 5
- 230000003064 anti-oxidating effect Effects 0.000 description 4
- 239000002932 luster Substances 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 230000001953 sensory effect Effects 0.000 description 4
- 235000019605 sweet taste sensations Nutrition 0.000 description 4
- 241000894006 Bacteria Species 0.000 description 3
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 3
- 229910052787 antimony Inorganic materials 0.000 description 3
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 3
- 229910052785 arsenic Inorganic materials 0.000 description 3
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 3
- 229910052793 cadmium Inorganic materials 0.000 description 3
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 3
- 229910052804 chromium Inorganic materials 0.000 description 3
- 239000011651 chromium Substances 0.000 description 3
- 229910001385 heavy metal Inorganic materials 0.000 description 3
- 230000003020 moisturizing effect Effects 0.000 description 3
- 229940001941 soy protein Drugs 0.000 description 3
- 241001391944 Commicarpus scandens Species 0.000 description 2
- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 2
- 241000589517 Pseudomonas aeruginosa Species 0.000 description 2
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 2
- 241000191967 Staphylococcus aureus Species 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 238000005452 bending Methods 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 230000006870 function Effects 0.000 description 2
- 125000001165 hydrophobic group Chemical group 0.000 description 2
- 230000000215 hyperchromic effect Effects 0.000 description 2
- 230000000813 microbial effect Effects 0.000 description 2
- 230000035699 permeability Effects 0.000 description 2
- 230000005501 phase interface Effects 0.000 description 2
- 230000002195 synergetic effect Effects 0.000 description 2
- SUSVAMTWXQCZSA-UHFFFAOYSA-N C(CCCCCCCCC(O)(O)O)CCCCCCCC(=O)OCC(CO)(CO)CO Chemical compound C(CCCCCCCCC(O)(O)O)CCCCCCCC(=O)OCC(CO)(CO)CO SUSVAMTWXQCZSA-UHFFFAOYSA-N 0.000 description 1
- 235000019542 Cured Meats Nutrition 0.000 description 1
- 229920000832 Cutin Polymers 0.000 description 1
- 206010040844 Skin exfoliation Diseases 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000035618 desquamation Effects 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 210000003780 hair follicle Anatomy 0.000 description 1
- 238000001095 inductively coupled plasma mass spectrometry Methods 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 230000002906 microbiologic effect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 210000003079 salivary gland Anatomy 0.000 description 1
- 210000001732 sebaceous gland Anatomy 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/85—Polyesters
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
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- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
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- Mycology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to the technical field of cosmetics, and provides a lip color cosmetic product and a preparation method thereof. The lip color cosmetic product comprises the following components in parts by weight: 1-10 parts of natural pigment, 2-15 parts of bitter orange peel oil, 5-10 parts of modified mica, 3-8 parts of poloxamer, 1-5 parts of polyethylene glycol, 0.5-2 parts of palm oil, 0.5-2 parts of cane sugar, 0.5-2 parts of tartaric acid, 2-5 parts of dipentaerythritol tri-hydroxystearate, 2-5 parts of cholesterol hydroxystearate, 0.1-0.5 part of hesperetin, 0.8-2.5 parts of mahonia stem extract, 0.5-1.5 parts of abietyl hydrolyzed soybean protein potassium, 0.5-1.5 parts of dioctadecyl dimethyl ammonium chloride and 0.5-1.5 parts of coconut fatty acid monoethanolamide, wherein the modified mica comprises the following components in parts by weight: 2.5-10 parts of mica, 0.2-0.5 part of yttrium oxide, 0.2-0.5 part of erbium oxide and 3-8 parts of water. Through above-mentioned technical scheme, solved among the prior art lip makeup product and moistened the degree poorly, the problem that lip skin is dry desquamate easily after using.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and relates to a lip color cosmetic product and a preparation method thereof.
Background
Unlike other skin regions, the skin of the lips is the weakest part of the human skin and is vulnerable to the external environment, which accelerates the aging process. The lip skin has thin cutin, no accessory organs such as hair follicles and sebaceous glands, and a plurality of salivary glands are distributed in the cuticle, the cuticle and the granular layer are thin, and the granular melanin is less than that of the common skin. The lip color cosmetic product can not only trace lips and endow the lips with gorgeous color, brightness and aesthetic feeling, but also play a role in protecting the lips, so the lip color cosmetic product is popular with vast women.
Lip color cosmetics on the market at present are various in color number and variety and rich in color, and are necessary beauty cosmetics for girls. However, the lips on which lipstick is applied tend to dry due to the user's work for a long time. Therefore, the existing lip color cosmetic products have the problems of poor moisturizing degree and easy dryness and desquamation of lip skin after long-term use.
Disclosure of Invention
The invention provides a lip color cosmetic product and a preparation method thereof, and solves the problems that the lip color cosmetic product in the prior art is poor in moistening degree and the skin of lips is easy to dry and peel after use.
The technical scheme of the invention is realized as follows:
the lip color cosmetic product comprises the following components in parts by weight:
1-10 parts of natural pigment, 2-15 parts of bitter orange peel oil, 5-10 parts of modified mica, 3-8 parts of poloxamer, 1-5 parts of polyethylene glycol, 0.5-2 parts of palm oil, 0.5-2 parts of cane sugar, 0.5-2 parts of tartaric acid, 2-5 parts of dipentaerythritol tri-hydroxystearate, 2-5 parts of cholesterol hydroxystearate, 0.1-0.5 part of hesperetin, 0.8-2.5 parts of mahonia stem extract, 0.5-1.5 parts of abietyl hydrolyzed soybean protein potassium, 0.5-1.5 parts of dioctadecyl dimethyl ammonium chloride, 0.5-1.5 parts of coconut monoethanolamide,
the modified mica comprises the following components in parts by weight: 2.5-10 parts of mica, 0.2-0.5 part of yttrium oxide, 0.2-0.5 part of erbium oxide and 3-8 parts of water.
As a further technical scheme, the paint comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxystearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride, 1 part of coconut monoethanolamide,
the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water.
As a further technical scheme, the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain the modified mica.
As a further technical scheme, the natural pigment comprises one or more of grape skin red, roselle red, mulberry red and blackcurrant red.
As a further technical scheme, the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract.
The invention also provides a preparation method of the lip color cosmetic product, which comprises the following steps:
s1, weighing the components according to the formula of the lip color cosmetic product for later use;
s2, adding poloxamer into water 2 times of the weight of the poloxamer, heating to 65-80 ℃, adding natural pigment, and dissolving to obtain a natural pigment solution;
s3, heating bitter orange peel oil, palm oil, poly pentaerythritol tri-polyhydroxy stearate and cholesterol hydroxy stearate to 80-85 ℃, stirring until the materials are completely dissolved to obtain an oil phase,
s4, slowly adding the oil phase obtained in the step S3 into the natural pigment solution obtained in the step S2, adding polyethylene glycol, potassium abietyl hydrolyzed soybean protein, dioctadecyl dimethyl ammonium chloride and coconut monoethanolamide, and uniformly stirring and dispersing to obtain a primary mixed material;
s5, adding the modified mica, tartaric acid, hesperetin and the mahonia stem extract into the primary mixed material obtained in the step S4, and uniformly stirring and dispersing to obtain the lip color cosmetic product.
As a further technical proposal, the stirring speed in the step S3 is 200 r/min.
As a further technical proposal, the stirring speed in the step S4 is 800 r/min.
As a further technical proposal, the stirring speed in the step S5 is 500 r/min.
The working principle and the beneficial effects of the invention are as follows:
1. according to the invention, the specific formula and the preparation method are compatible, so that the prepared lip color cosmetic product is smooth and uniform in texture, smooth in surface, strict in color and luster, moderate in hardness and not prone to bending and breaking.
2. According to the invention, the yttrium oxide and the oxidized bait are adopted to modify the mica, and then the modified mica is added into the lip color cosmetic product, so that the hardness, the color and the texture of the lip color cosmetic product can be obviously improved. The yttrium oxide and the oxidized bait are adopted to modify mica, the obtained modified mica has good colorability and crystal transparency, and when the modified mica is added into a lip color cosmetic product, the modified mica has good hyperchromic and color-retaining effects on natural pigments, so that the prepared lip color cosmetic product is strict, uniform and full in color. The addition of the modified mica promotes the dispersion of the pigment in the lip color cosmetic product, so that the components in the lip color cosmetic product are dispersed more uniformly, the lip color cosmetic product is smooth in texture and moderate in hardness, and the lip color cosmetic product is not easy to break in the using process.
3. According to the invention, the poloxamer is added into the lip color cosmetic product, so that the color and the wettability of the lip color cosmetic product can be obviously improved. The water solubility of the natural pigment is poor, and the poloxamer is added, so that the dispersion of the natural pigment in water is promoted in the process of preparing the natural pigment solution, and when the oil phase is slowly added into the natural pigment solution, the hydrophilic group and the hydrophobic group in the poloxamer molecule respectively interact with the natural pigment solution and the oil phase, so that the compatibility of the natural pigment solution and the oil phase interface is changed, the dispersion of the natural pigment in the lip color cosmetic product is further promoted, the color of the lip color cosmetic product is more uniform and full, the poloxamer has good hydrophilicity, and the lip color cosmetic product has a better moisturizing effect.
4. According to the invention, the mahonia stem extract and the hesperetin are added into the lip color cosmetic product, so that the smell of the lip color cosmetic product can be obviously improved. The mahonia stem extract is also compatible with hesperetin, so that the prepared lip color cosmetic product has light sweet taste and is popular with consumers. The mahonia stem extract also has a good antioxidation effect, and is added into a lip color cosmetic product to endow the lip color cosmetic product with an antioxidation function, so that the lip skin is better protected, and the practicability is stronger.
5. In the invention, the pentaerythritol tri-hydroxystearate and the cholesteryl hydroxystearate are added into the lip color cosmetic product, so that the texture and the moisture of the lip color cosmetic product can be obviously improved. The mutual compatibility of the polypentaerythritol tri-polyhydroxy stearate and the cholesterol hydroxy stearate can obviously improve the surface tension among various constituent phases in the lip color cosmetic product to form a uniform and stable dispersion system, so that the lip color cosmetic product has smooth and uniform texture; the mutual compatibility of the poly pentaerythritol tri-polyhydroxy stearate and the cholesterol hydroxy stearate can efficiently keep moisture, and has good skin moistening effect, thereby improving the moistening degree of the lip color cosmetic product.
6. In the invention, the potassium abietyl hydrolyzed soy protein, the dioctadecyl dimethyl ammonium chloride and the coconut monoethanolamide are added into the lip color cosmetic product, so that the wettability and the hardness of the lip color cosmetic product can be obviously improved. The potassium abietyl hydrolyzed soybean protein, the dioctadecyl dimethyl ammonium chloride and the coconut monoethanolamide have synergistic effect and strong permeability, and can effectively promote the absorption of active ingredients, thereby improving the wettability of the lip color cosmetic product, and the lip color cosmetic product is compatible with other components in the formula, thereby obviously improving the hardness of the lip color cosmetic product.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The lip color cosmetic product comprises the following components in parts by weight:
1 part of natural pigment, 2 parts of bitter orange peel oil, 5 parts of modified mica, 3 parts of poloxamer, 1 part of polyethylene glycol, 0.5 part of palm oil, 0.5 part of cane sugar, 0.5 part of tartaric acid, 2 parts of dipentaerythritol tri-polyhydroxy stearate, 2 parts of cholesterol hydroxy stearate, 0.1 part of hesperetin, 0.8 part of mahonia stem extract, 0.5 part of potassium abietyl hydrolyzed soybean protein, 0.5 part of dioctadecyl dimethyl ammonium chloride and 0.5 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method comprises the following steps:
s1, weighing the components according to the formula for later use;
s2, adding poloxamer into water 2 times of the weight of the poloxamer, heating to 65-80 ℃, adding natural pigment, and dissolving to obtain a natural pigment solution;
s3, heating bitter orange peel oil, palm oil, poly pentaerythritol tri-polyhydroxy stearate and cholesterol hydroxy stearate to 80-85 ℃, stirring at the speed of 200r/min until the materials are completely dissolved to obtain an oil phase,
s4, slowly adding the oil phase obtained in the step S3 into the natural pigment solution obtained in the step S2, adding polyethylene glycol, potassium abietyl hydrolyzed soybean protein, dioctadecyl dimethyl ammonium chloride and coconut monoethanolamide, and uniformly stirring and dispersing at the speed of 800r/min to obtain a primary mixed material;
s5, adding the modified mica, tartaric acid, hesperetin and the mahonia stem extract into the primary mixed material obtained in the step S4, and stirring and dispersing uniformly at the speed of 500r/min to obtain the lip color cosmetic product.
Example 2
The lip color cosmetic product comprises the following components in parts by weight:
10 parts of natural pigment, 15 parts of bitter orange peel oil, 10 parts of modified mica, 8 parts of poloxamer, 5 parts of polyethylene glycol, 2 parts of palm oil, 2 parts of sucrose, 2 parts of tartaric acid, 5 parts of dipentaerythritol tri-polyhydroxystearate, 5 parts of cholesterol hydroxystearate, 0.5 part of hesperetin, 2.5 parts of mahonia stem extract, 1.5 parts of potassium abietyl hydrolyzed soybean protein, 1.5 parts of dioctadecyl dimethyl ammonium chloride and 1.5 parts of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as that of example 1.
Example 3
The lip color cosmetic product comprises the following components in parts by weight:
3 parts of natural pigment, 6 parts of bitter orange peel oil, 6 parts of modified mica, 4 parts of poloxamer, 2 parts of polyethylene glycol, 1.2 parts of palm oil, 1 part of sucrose, 1 part of tartaric acid, 3 parts of dipentaerythritol tri-hydroxystearate, 3 parts of cholesterol hydroxystearate, 0.2 part of hesperetin, 1.3 parts of mahonia stem extract, 0.8 part of potassium abietyl hydrolyzed soybean protein, 0.8 part of dioctadecyl dimethyl ammonium chloride and 0.8 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating and concentrating the filtrate, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as that of example 1.
Example 4
The lip color cosmetic product comprises the following components in parts by weight:
7 parts of natural pigment, 10 parts of bitter orange peel oil, 8 parts of modified mica, 6 parts of poloxamer, 4 parts of polyethylene glycol, 1.5 parts of palm oil, 1.5 parts of cane sugar, 1.5 parts of tartaric acid, 4 parts of dipentaerythritol tri-hydroxystearate, 4 parts of cholesteryl hydroxystearate, 0.4 part of hesperetin, 2.1 parts of mahonia stem extract, 1.2 parts of potassium abietyl hydrolyzed soybean protein, 1.2 parts of dioctadecyl dimethyl ammonium chloride and 1.2 parts of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as that of example 1.
Example 5
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxy stearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wetly grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as that of example 1.
Example 6
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxy stearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 2.5 parts of mica, 0.2 part of yttrium oxide, 0.2 part of erbium oxide and 3 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating and concentrating the filtrate, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as that of example 1.
Example 7
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxy stearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 10 parts of mica, 0.5 part of yttrium oxide, 0.5 part of erbium oxide and 8 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as example 1.
Example 8
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxy stearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is roselle red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as that of example 1.
Example 9
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxy stearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is mulberry red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as that of example 1.
Example 10
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxy stearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is blackcurrant red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as example 1.
Comparative example 1
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-hydroxystearate, 3 parts of cholesteryl hydroxystearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of abietyl hydrolyzed soybean protein potassium, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as the example 1 except that mica is added and modified mica is not added in the step S5.
Comparative example 2
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of sucrose, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-hydroxystearate, 3 parts of cholesterol hydroxystearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as example 1 except that poloxamer is not added in step S2.
Comparative example 3
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxy stearate, 0.3 part of hesperetin, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as example 1 except that the mahonia stem extract is not added in step S5.
Comparative example 4
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of sucrose, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesterol hydroxystearate, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
the preparation method is the same as the example 1 except that no hesperetin is added in the step S5.
Comparative example 5
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of sucrose, 1.3 parts of tartaric acid, 0.3 part of hesperetin, 1.6 parts of a mahonia stem extract, 1 part of abietyl hydrolyzed soybean protein potassium, 1 part of dioctadecyl dimethyl ammonium chloride and 1 part of coconut monoethanolamide;
the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
in the preparation method, no dipentaerythritol tri-polyhydroxystearate or cholesteryl hydroxystearate is added in step S3, and the rest steps are the same as in example 1.
Comparative example 6
The lip color cosmetic product comprises the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxystearate, 3 parts of cholesterol hydroxystearate, 0.3 part of hesperetin and 1.6 parts of mahonia stem extract;
wherein the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water, wherein the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica; the natural pigment is grape skin red; the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract;
in the preparation method, step S4 does not add abietyl hydrolyzed soybean protein potassium, dioctadecyl dimethyl ammonium chloride and coconut monoethanolamide, and the rest steps are the same as in example 1.
The lip color cosmetic products prepared in examples 1-10 and comparative examples 1-6 were subjected to the following performance tests:
1. and (3) microbial detection: items such as total bacteria, total mold/yeast, heat-resistant coliform, staphylococcus aureus and pseudomonas aeruginosa in the sample are detected according to the method specified in technical specifications for cosmetic safety (2015), and the detection results are shown in the following table:
TABLE 1 results of microbiological examination of lip color cosmetic products prepared in examples 1-10 and comparative examples 1-6
Note: in the above table, indicates no detection, and indicates no detection.
The data in table 1 show that the total number of bacteria in the mask liquid products of examples 1 to 7 and comparative examples 7 to 12 is less than 10/mL, the total number of mold/yeast is less than 10/mL, heat-resistant coliform bacteria, staphylococcus aureus and pseudomonas aeruginosa are not detected, and the microbial test result shows that the products meet the requirements of technical cosmetic safety specifications (2015 edition), which indicates that the lip color cosmetic products prepared by the invention are safe and reliable.
2. Heavy metals: detecting the contents of chromium, arsenic, cadmium, antimony and lead in the sample according to a method specified in GB/T35828-2018 inductively coupled plasma mass spectrometry for determining chromium, arsenic, cadmium, antimony and lead in cosmetics, wherein the detection standard refers to GB7916-87 cosmetic hygienic standard, and the detection results are shown in the following table:
table 2 determination results of heavy metal content of lip color cosmetic products prepared in examples 1 to 10 and comparative examples 1 to 6
Note: in the above table, a indicates no detection.
As can be seen from the data in Table 2, no heavy metal such as chromium, arsenic, cadmium, antimony, lead and the like is detected in the lip color cosmetic products of examples 1 to 10 and comparative examples 1 to 6, and the lip color cosmetic products meet the requirements of GB7916-87 cosmetic hygienic Standard.
3. Sensory evaluation: selecting 100 female volunteers, wherein the female volunteers are 25-40 years old, scoring the texture, color, hardness, moistening degree, smell and the like of the lip color cosmetic products of examples 1-10 and comparative examples 1-6 according to sensory evaluation indexes, wherein the scoring standard is 0-10 points, the closer the lip color cosmetic products to the scoring standard, the higher the score, and on the contrary, the lower the score, the sensory evaluation indexes are shown in table 3, and the scoring results are shown in table 4:
TABLE 3 sensory evaluation index
| Item | Evaluation index |
| Texture of | Smooth surface, pearly luster, smooth and uniform paste texture, no air holes and no granular sensation |
| Color | Bright color, soft and beautiful color, uniform and natural color |
| Hardness of | Is not easy to bend and break, but is not too soft and too hard |
| Degree of wetness | After being coated, the coating is not dry, greasy, caking and good in moistening degree |
| Smell(s) | Has light sweet taste, no pungent flavor and petroleum smell, and thick cured meat flavor |
TABLE 4 Scoring situation
The data in table 4 show that the scores of the texture, color, hardness, moisture and smell of the lip color cosmetic products of examples 1-10 of the present invention are all over 9 points, which are higher than the scores of the lip color cosmetic products of comparative examples 1-6, and thus, the lip color cosmetic products prepared in examples 1-10 of the present invention have the advantages of smooth and uniform texture, smooth surface, proper color, moderate hardness, and less possibility of bending and breaking, the skin is not greasy and has good moisture after the use of the lip color cosmetic products of the present invention, and meanwhile, the lip color cosmetic products prepared in the examples of the present invention have good smell, have light sweet taste after the use, and are suitable for wide consumers.
Compared with the lip color cosmetic products of examples 1-10, the lip color cosmetic product of comparative example 1 has relatively poor wettability and texture because mica is not modified in the lip color cosmetic product of comparative example 1, which indicates that after the mica is modified by yttrium oxide and bait oxide, the lip color cosmetic product can be added to the lip color cosmetic product to obviously improve the hardness, color and texture of the lip color cosmetic product. The yttrium oxide and the oxidized bait are adopted to modify mica, the obtained modified mica has good colorability and crystal transparency, and when the modified mica is added into a lip color cosmetic product, the modified mica has good hyperchromic and color-retaining effects on natural pigments, so that the prepared lip color cosmetic product is strict, uniform and full in color. The addition of the modified mica also promotes the dispersion of pigments in the lip color cosmetic product, so that the components in the lip color cosmetic product are dispersed more uniformly, and the lip color cosmetic product has smooth texture and moderate hardness and is not easy to break off in the using process.
Compared with examples 1-10, the lip color cosmetic product of comparative example 2 has relatively poor color and luster and wettability, because poloxamer is not added to the lip color cosmetic product of comparative example 2, which indicates that the color and luster and wettability of the lip color cosmetic product can be remarkably improved by adding poloxamer to the lip color cosmetic product. The water solubility of the natural pigment is poor, and the poloxamer is added, so that the dispersion of the natural pigment in water is promoted in the process of preparing the natural pigment solution, and when the oil phase is slowly added into the natural pigment solution, the hydrophilic group and the hydrophobic group in the poloxamer molecule respectively interact with the natural pigment solution and the oil phase, so that the compatibility of the natural pigment solution and the oil phase interface is changed, the dispersion of the natural pigment in the lip color cosmetic product is further promoted, the color of the lip color cosmetic product is more uniform and full, the poloxamer has good hydrophilicity, and the lip color cosmetic product has a better moisturizing effect.
Compared with examples 1-10, the lip color cosmetic products of comparative example 3 and comparative example 4 have slightly poorer odor, because the mahonia dubia extract is not added in the lip color cosmetic product of comparative example 3, and the hesperetin is not added in the lip color cosmetic product of comparative example 4, which indicates that the odor of the lip color cosmetic product can be obviously improved by adding the mahonia dubia extract and the hesperetin to the lip color cosmetic product. The mahonia stem extract is also compatible with hesperetin, so that the prepared lip color cosmetic product has light sweet taste and is popular with consumers. The mahonia stem extract also has a good antioxidation effect, and is added into a lip color cosmetic product to endow the lip color cosmetic product with an antioxidation function, so that the lip skin is better protected, and the practicability is stronger.
Compared with examples 1-10, the lip color cosmetic product of comparative example 5 has a slightly poorer texture and wettability, because the lip color cosmetic product of comparative example 5 is not added with the polypentaerythritol tri-polyhydroxystearate and the cholesteryl hydroxystearate, which shows that the addition of the polypentaerythritol tri-polyhydroxystearate and the cholesteryl hydroxystearate to the lip color cosmetic product can obviously improve the texture and the wettability of the lip color cosmetic product. The mutual compatibility of the polypentaerythritol tri-polyhydroxy stearate and the cholesterol hydroxy stearate can obviously improve the surface tension among various constituent phases in the lip color cosmetic product to form a uniform and stable dispersion system, so that the lip color cosmetic product has smooth and uniform texture; the mutual compatibility of the poly pentaerythritol tri-polyhydroxy stearate and the cholesterol hydroxy stearate can efficiently keep moisture, and has good skin moistening effect, thereby improving the moistening degree of the lip color cosmetic product.
Compared with examples 1-10, the lip color cosmetic product of comparative example 6 has poorer wettability and hardness, because potassium abietyl hydrolyzed soy protein, dioctadecyl dimethyl ammonium chloride and coconut monoethanolamide are not added in the lip color cosmetic product of comparative example 6, which indicates that the wettability and hardness of the lip color cosmetic product can be obviously improved by adding the potassium abietyl hydrolyzed soy protein, the dioctadecyl dimethyl ammonium chloride and the coconut monoethanolamide into the lip color cosmetic product. The potassium abietyl hydrolyzed soybean protein, the dioctadecyl dimethyl ammonium chloride and the coconut monoethanolamide have synergistic effect and strong permeability, and can effectively promote the absorption of active ingredients, thereby improving the wettability of the lip color cosmetic product, and the lip color cosmetic product is compatible with other components in the formula, thereby obviously improving the hardness of the lip color cosmetic product.
The present invention is not limited to the above preferred embodiments, and any modifications, equivalent substitutions, improvements, etc. within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (7)
1. The lip color cosmetic product is characterized by comprising the following components in parts by weight:
1-10 parts of natural pigment, 2-15 parts of bitter orange peel oil, 5-10 parts of modified mica, 3-8 parts of poloxamer, 1-5 parts of polyethylene glycol, 0.5-2 parts of palm oil, 0.5-2 parts of cane sugar, 0.5-2 parts of tartaric acid, 2-5 parts of dipentaerythritol tri-hydroxystearate, 2-5 parts of cholesterol hydroxystearate, 0.1-0.5 part of hesperetin, 0.8-2.5 parts of mahonia stem extract, 0.5-1.5 parts of abietyl hydrolyzed soybean protein potassium, 0.5-1.5 parts of dioctadecyl dimethyl ammonium chloride, 0.5-1.5 parts of coconut monoethanolamide,
the modified mica comprises the following components in parts by weight: 2.5-10 parts of mica, 0.2-0.5 part of yttrium oxide, 0.2-0.5 part of erbium oxide and 3-8 parts of water;
the preparation method of the modified mica comprises the following steps: adding mica, yttrium oxide and erbium oxide into water, uniformly mixing, wet-grinding, drying, and roasting at 800 ℃ for 10-15 min to obtain modified mica;
the preparation method of the mahonia stem extract comprises the following steps: decocting caulis Mahoniae powder with water, filtering, heating the filtrate, concentrating, eluting with ethanol, concentrating, and drying to obtain caulis Mahoniae extract.
2. The lip color cosmetic product according to claim 1, comprising the following components in parts by weight:
5 parts of natural pigment, 8 parts of bitter orange peel oil, 7 parts of modified mica, 5 parts of poloxamer, 3 parts of polyethylene glycol, 1.3 parts of palm oil, 1.3 parts of cane sugar, 1.3 parts of tartaric acid, 3 parts of dipentaerythritol tri-polyhydroxy stearate, 3 parts of cholesteryl hydroxy stearate, 0.3 part of hesperetin, 1.6 parts of mahonia stem extract, 1 part of potassium abietyl hydrolyzed soybean protein, 1 part of dioctadecyl dimethyl ammonium chloride, 1 part of coconut monoethanolamide,
the modified mica comprises the following components in parts by weight: 6 parts of mica, 0.35 part of yttrium oxide, 0.35 part of erbium oxide and 5 parts of water.
3. The lip color cosmetic product of claim 1, wherein the natural pigments comprise one or more of grape skin red, hibiscus sabdariffa red, mulberry red, and blackcurrant red.
4. A preparation method of a lip color cosmetic product is characterized by comprising the following steps:
s1, weighing the components according to the formula of the lip color cosmetic product as claimed in any one of claims 1 to 3 for later use;
s2, adding poloxamer into water 2 times of the weight of the poloxamer, heating to 65-80 ℃, adding natural pigment, and dissolving to obtain a natural pigment solution;
s3, heating bitter orange peel oil, palm oil, poly pentaerythritol tri-polyhydroxy stearate and cholesterol hydroxy stearate to 80-85 ℃, stirring until the materials are completely dissolved to obtain an oil phase,
s4, slowly adding the oil phase obtained in the step S3 into the natural pigment solution obtained in the step S2, adding polyethylene glycol, potassium abietyl hydrolyzed soybean protein, dioctadecyl dimethyl ammonium chloride and coconut monoethanolamide, and uniformly stirring and dispersing to obtain a primary mixed material;
s5, adding the modified mica, tartaric acid, hesperetin and the mahonia stem extract into the primary mixed material obtained in the step S4, and uniformly stirring and dispersing to obtain the lip color cosmetic product.
5. The method for preparing a lip color cosmetic product according to claim 4, wherein the stirring speed in step S3 is 200 r/min.
6. The method for preparing a lip color cosmetic product according to claim 4, wherein the stirring speed in step S4 is 800 r/min.
7. The method for preparing a lip color cosmetic according to claim 4, wherein the stirring speed in step S5 is 500 r/min.
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| FR3011178A1 (en) * | 2013-10-01 | 2015-04-03 | Oreal | LIQUID COMPOSITION COMPRISING A NON-VOLATILE OIL, 12-HYDROXYSTEARIC ACID, AN ADDITIONAL WAX, A VINYLPYRROLIDONE COPOLYMER AND A SILICA AEROGEL |
| CN105168031A (en) * | 2015-10-14 | 2015-12-23 | 广州市花安堂生物科技有限公司 | Lip gloss containing multi-colored particles and preparation method thereof |
| CN107648108A (en) * | 2017-10-18 | 2018-02-02 | 佛山娇芙生物科技有限公司 | A kind of non-sticky cup liquid lipstick and preparation method thereof |
| CN109806197A (en) * | 2019-02-27 | 2019-05-28 | 广州尚姿化妆品有限公司 | A kind of multiple plant cyanines extraction lip gloss and preparation method thereof |
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|---|---|---|---|---|
| FR3011178A1 (en) * | 2013-10-01 | 2015-04-03 | Oreal | LIQUID COMPOSITION COMPRISING A NON-VOLATILE OIL, 12-HYDROXYSTEARIC ACID, AN ADDITIONAL WAX, A VINYLPYRROLIDONE COPOLYMER AND A SILICA AEROGEL |
| CN105168031A (en) * | 2015-10-14 | 2015-12-23 | 广州市花安堂生物科技有限公司 | Lip gloss containing multi-colored particles and preparation method thereof |
| CN107648108A (en) * | 2017-10-18 | 2018-02-02 | 佛山娇芙生物科技有限公司 | A kind of non-sticky cup liquid lipstick and preparation method thereof |
| CN109806197A (en) * | 2019-02-27 | 2019-05-28 | 广州尚姿化妆品有限公司 | A kind of multiple plant cyanines extraction lip gloss and preparation method thereof |
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