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CN111141443A - A Capacitive Thin Film Vacuum Gauge Based on MEMS Technology - Google Patents

A Capacitive Thin Film Vacuum Gauge Based on MEMS Technology Download PDF

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Publication number
CN111141443A
CN111141443A CN201911362566.8A CN201911362566A CN111141443A CN 111141443 A CN111141443 A CN 111141443A CN 201911362566 A CN201911362566 A CN 201911362566A CN 111141443 A CN111141443 A CN 111141443A
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pressure
lower substrate
electrode
vacuum gauge
film
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李刚
成永军
何申伟
孙雯君
习振华
张瑞芳
杨利
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Lanzhou Institute of Physics of Chinese Academy of Space Technology
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Lanzhou Institute of Physics of Chinese Academy of Space Technology
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01LMEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
    • G01L9/00Measuring steady of quasi-steady pressure of fluid or fluent solid material by electric or magnetic pressure-sensitive elements; Transmitting or indicating the displacement of mechanical pressure-sensitive elements, used to measure the steady or quasi-steady pressure of a fluid or fluent solid material, by electric or magnetic means
    • G01L9/12Measuring steady of quasi-steady pressure of fluid or fluent solid material by electric or magnetic pressure-sensitive elements; Transmitting or indicating the displacement of mechanical pressure-sensitive elements, used to measure the steady or quasi-steady pressure of a fluid or fluent solid material, by electric or magnetic means by making use of variations in capacitance, i.e. electric circuits therefor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01LMEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
    • G01L13/00Devices or apparatus for measuring differences of two or more fluid pressure values
    • G01L13/06Devices or apparatus for measuring differences of two or more fluid pressure values using electric or magnetic pressure-sensitive elements
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01LMEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
    • G01L21/00Vacuum gauges

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  • General Physics & Mathematics (AREA)
  • Measuring Fluid Pressure (AREA)

Abstract

本发明公开了一种基于MEMS技术的电容薄膜真空计,基于MEMS技术,待测环境中气压的变化使感压薄膜产生位移,引起下基板电极与感压薄膜之间距离发生变化,从而改变了感压薄膜电极与下基板电极之间的电容值,通过测量电容值的大小即可得到待测环境的真空度,本发明能够显著降低真空计的尺寸和能耗,同时,通过根据测量需要使用不同参数的感压薄膜能够有效提高测量的灵敏度。

Figure 201911362566

The invention discloses a capacitance film vacuum gauge based on MEMS technology. Based on the MEMS technology, the change of air pressure in the environment to be measured causes the pressure-sensitive film to shift, causing the distance between the lower substrate electrode and the pressure-sensitive film to change, thereby changing the The capacitance value between the pressure-sensitive film electrode and the lower substrate electrode can be measured by measuring the capacitance value to obtain the vacuum degree of the environment to be measured. The present invention can significantly reduce the size and energy consumption of the vacuum gauge. Pressure-sensitive films with different parameters can effectively improve the sensitivity of the measurement.

Figure 201911362566

Description

Capacitance film vacuum gauge based on MEMS technology
Technical Field
The invention belongs to the technical field of vacuum measurement, and particularly relates to a capacitive film vacuum gauge based on an MEMS (micro-electromechanical system) technology.
Background
The miniaturization of vacuum gauges has led to a dramatic advance in order to meet field testing and space detection requirements. The MEMS sensor has the characteristics of miniaturization, low cost, high performance, easy compatibility with a CMOS integrated circuit and the like. Among the different types of MEMS sensors, the most common and widely used are piezoresistive and capacitive sensors, wherein capacitive sensors have the advantages of high sensitivity, low temperature coefficient, low power consumption, etc., compared to piezoresistive sensors. The MEMS capacitance film vacuum gauge is one of MEMS capacitance sensors, can meet the application requirements of the fields of deep space exploration, aerodynamic research, near space exploration and the like on high measurement accuracy, small volume, light weight and low power consumption of a vacuum measurement instrument, and has wide application prospect. However, the MEMS capacitive film vacuum gauge in the prior art mainly has the problems of high size and energy consumption, low sensitivity, and the like.
Disclosure of Invention
In view of this, the present invention provides a capacitance film vacuum gauge based on the MEMS technology, which can realize a vacuum gauge with a small size, low energy consumption, and high sensitivity.
The invention provides a capacitance film vacuum gauge based on an MEMS (micro-electromechanical system) technology, which comprises an upper substrate 7, a lower substrate 8, a silicon chip 1 and a glass sealing tube 4; the silicon chip 1 is provided with a pressure sensing film 10 and an electrode leading-out hole A5; the upper substrate 7 and the lower substrate 8 are made of glass, the upper surface of the lower substrate 8 is plated with a lower substrate electrode 2, the upper substrate 7 is provided with a vent hole 9 and an electrode leading-out hole B6, and the position of the vent hole 9 is aligned with the position of the pressure-sensitive film 10; the electrode of the lower substrate 8 is led out to the upper surface of the upper substrate 7 through an electrode lead-out hole A5 and an electrode lead-out hole B6; the electrode of the pressure-sensitive film 10 is led out to the upper surface of the upper substrate 7 through the electrode lead-out hole B6; the silicon chip 1 is respectively bonded with the lower surface of the upper substrate 7 and the upper surface of the lower substrate 8, the glass sealing tube 4 is hermetically buckled on the vent hole 9, and a sealed vacuum cavity is formed between the pressure sensing film 4 and the vent hole 9 of the upper substrate 7 and the upper surface of the lower substrate 9;
and placing the vacuum gauge in a vacuum environment to be measured, removing the glass sealing tube 4, and measuring the capacitance value between the electrode of the lower substrate 8 and the electrode of the pressure sensing film 1 to obtain the vacuum degree of the vacuum environment to be measured.
Further, the pressure-sensitive film 1 is obtained by etching the silicon wafer by adopting a concentrated boron doping method.
Further, the pressure-sensitive film 1 had a side length of 5mm and a thickness of 16 μm.
Has the advantages that:
based on the MEMS technology, the pressure sensing film is displaced due to the change of air pressure in the environment to be measured, so that the distance between the lower substrate electrode and the pressure sensing film is changed, the capacitance value between the pressure sensing film electrode and the lower substrate electrode is changed, the vacuum degree of the environment to be measured can be obtained by measuring the capacitance value, the size and the energy consumption of the vacuum gauge can be obviously reduced, and meanwhile, the pressure sensing film with different parameters can be used according to the measurement requirement, so that the measurement sensitivity can be effectively improved.
Drawings
Fig. 1 is a schematic structural diagram of a capacitance film vacuum gauge based on the MEMS technology provided in the present invention.
Fig. 2 is a schematic diagram of a silicon wafer structure of a capacitance thin film vacuum gauge based on the MEMS technology.
Fig. 3 is a schematic view of a lower substrate structure of a capacitance thin film vacuum gauge based on the MEMS technology.
Fig. 4 is a schematic structural diagram of an upper substrate of a capacitance thin film vacuum gauge based on the MEMS technology.
The structure comprises a silicon chip 1, a lower substrate electrode 2, an extraction electrode 3, a glass sealing tube 4, an electrode extraction hole 5, an electrode extraction hole B6, an upper substrate 7, a lower substrate 8, a vent hole 9, a pressure sensing film 10 and an electrode lead 11.
Detailed Description
The invention is described in detail below by way of example with reference to the accompanying drawings.
The invention provides a capacitance film vacuum gauge based on an MEMS (micro-electromechanical system) technology, as shown in figure 1, the capacitance film vacuum gauge is of a three-layer structure as a whole, the size of the capacitance film vacuum gauge is designed to be 10mm multiplied by 10mm, the capacitance film vacuum gauge comprises an upper substrate 7, a lower substrate 8 and a silicon chip 1, a pressure sensing film 10 is etched on the silicon chip 1 by adopting a concentrated boron doping technology, the upper substrate 7 and the lower substrate 8 are made of Pyrex glass, the silicon chip 1, the upper substrate and the lower substrate are subjected to monocrystalline silicon-glass bonding, a single-side capacitance structure is adopted, the concentrated boron doping pressure sensing film 10 and an electrode plated on the lower substrate form a flat capacitor. The extraction electrode 3 of the lower substrate electrode 2 and the electrode lead 11 of the pressure-sensitive film 10 are both extracted from the upper substrate, a vent 9 is provided in the middle of the upper substrate at a position aligned with the pressure-sensitive film, and the air inlet is sealed by a glass sealing tube 4 in order to protect the pressure-sensitive film from being damaged in the atmospheric environment.
During testing, the sensor is placed in a vacuum environment to be tested, the glass sealing tube 4 is broken, and the capacitance value between the lower substrate electrode 2 and the electrode of the pressure sensing film is measured to obtain the vacuum degree of the vacuum environment to be tested.
The silicon wafer 1 of the present invention, as shown in fig. 2, comprises a pressure-sensitive film structure and a support structure, and has a size of 10mm × 10mm × 56 μm, wherein the pressure-sensitive film is heavily boron-doped P + + Si, and has a size of 5mm × 5mm × 16 μm, and the depth of the upper and lower cavities is 20 μm. The pressure-sensing film electrode lead is realized on monocrystalline silicon by adopting a concentrated boron doping technology. Meanwhile, the silicon chip 1 is provided with an electrode lead-out hole A5 for leading out a lower substrate electrode 2.
The lower substrate of the present invention, as shown in fig. 3, includes two parts, i.e., a lower substrate and a lower substrate electrode 2, each having a size of 10mm × 10mm × 5mm, wherein the lower substrate is made of Pyrex glass, and the lower substrate electrode 2 is Ti + Au and has a thickness of 300 nm.
As shown in fig. 4, the upper substrate of the present invention is made of Pyrex glass and has dimensions of 10mm × 10mm × 5mm, and the upper substrate is provided with electrode lead-out holes B6 and vent holes 9.
In order to obtain optimized design parameters of the pressure-sensitive film, the side length and the thickness of the film are subjected to combined analysis by adopting an orthogonal optimization method, and key parameters concerned by the invention comprise: maximum deflection 1000Pa, base capacitance, sensitivity, and maximum stress.
In addition, the process difficulty and the product robustness are also key factors that must be considered in the design process. Simulation test results show that: for films with various side lengths, the maximum deflection, the sensitivity and the maximum stress of the film are all reduced along with the increase of the thickness, and the basic capacitance shows an opposite change rule because the basic capacitance is inversely proportional to the maximum deflection. Increasing the film thickness can reduce the process difficulty and improve the reliability of the sensor, but at the same time, the sensitivity is reduced; to improve sensitivity, the side length of the film can be increased, but this increases the process difficulty. Therefore, the size of the film must be reasonably optimized. When the side length is smaller, such as 2mm, the sensitivity is too low to be less than or equal to 0.2 fF/Pa; when the side length is increased to 6mm, a very high sensitivity of 2fF/Pa can be obtained even at a larger thickness of 20 μm. Therefore, the side length of the film should be as large as possible, as the process conditions allow. In view of the above, the film side length was designed to be 5mm and the thickness was designed to be 16 μm. Under the design parameters, the maximum deflection of the film under the pressure of 1000Pa is 14 μm, the maximum stress is 2.70E +07Pa, and the minimum sensitivity is 2.2 fF/Pa.
In summary, the above description is only a preferred embodiment of the present invention, and is not intended to limit the scope of the present invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (3)

1.一种基于MEMS技术的电容薄膜真空计,其特征在于,包括上基板(7)、下基板(8)、硅片(1)和玻璃密封管(4);所述硅片(1)上具有感压薄膜(10)及电极引出孔A(5);所述上基板(7)和下基板(8)的材料均为玻璃,所述下基板(8)的上表面镀有下基板电极(2),所述上基板(7)上开设通气孔(9)、电极引出孔B(6),所述通气孔(9)的位置与感压薄膜(10)的位置对准;所述下基板(8)电极通过电极引出孔A(5)和电极引出孔B(6)引出至上基板(7)的上表面;所述感压薄膜(10)的电极通过电极引出孔B(6)引出至上基板(7)的上表面;所述硅片(1)分别与上基板(7)的下表面和下基板(8)的上表面键合,所述玻璃密封管(4)密封扣合于所述通气孔(9)之上,使感压薄膜(4)与上基板(7)的通气孔(9)及下基板(9)的上表面之间形成密封的真空腔;1. A capacitive thin film vacuum gauge based on MEMS technology, characterized in that it comprises an upper substrate (7), a lower substrate (8), a silicon wafer (1) and a glass sealing tube (4); the silicon wafer (1) There is a pressure-sensitive film (10) and an electrode lead-out hole A (5) thereon; the upper substrate (7) and the lower substrate (8) are made of glass, and the upper surface of the lower substrate (8) is plated with a lower substrate The electrode (2), a vent hole (9) and an electrode lead-out hole B (6) are provided on the upper substrate (7), and the position of the vent hole (9) is aligned with the position of the pressure-sensitive film (10); The electrodes of the lower substrate (8) are led out to the upper surface of the upper substrate (7) through the electrode lead-out holes A (5) and the electrode lead-out holes B (6); the electrodes of the pressure-sensitive film (10) are led out through the electrode lead-out holes B (6). ) is led out to the upper surface of the upper substrate (7); the silicon wafer (1) is respectively bonded to the lower surface of the upper substrate (7) and the upper surface of the lower substrate (8), and the glass sealing tube (4) seals the buckle be fitted on the vent hole (9), so that a sealed vacuum cavity is formed between the pressure sensitive film (4), the vent hole (9) of the upper substrate (7) and the upper surface of the lower substrate (9); 将所述真空计置于待测真空环境中,去除所述玻璃密封管(4)后,测量所述下基板(8)电极与感压薄膜(1)的电极间的电容值即可得到待测真空环境的真空度。The vacuum gauge is placed in the vacuum environment to be measured, and after removing the glass sealing tube (4), the capacitance value between the electrode of the lower substrate (8) and the electrode of the pressure-sensitive film (1) can be obtained by measuring the capacitance value to be measured. Measure the vacuum degree of the vacuum environment. 2.根据权利要求1所述的真空计,其特征在于,所述感压薄膜(1)为在所述硅片上采用浓硼掺杂方法刻蚀得到。2 . The vacuum gauge according to claim 1 , wherein the pressure-sensitive film ( 1 ) is obtained by etching on the silicon wafer by using a boron-doped method. 3 . 3.根据权利要求1所述的真空计,其特征在于,所述感压薄膜(1)的边长为5mm、厚度为16μm。3 . The vacuum gauge according to claim 1 , wherein the pressure-sensitive film ( 1 ) has a side length of 5 mm and a thickness of 16 μm. 4 .
CN201911362566.8A 2019-12-26 2019-12-26 A Capacitive Thin Film Vacuum Gauge Based on MEMS Technology Pending CN111141443A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111982383A (en) * 2020-07-06 2020-11-24 厦门大学 Differential pressure contact type MEMS capacitance film vacuum gauge

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CN1379228A (en) * 2002-05-13 2002-11-13 厦门大学 Pressure sensor with electrostatic bonding and sealed capacitor cavity and its preparing process
CN2738224Y (en) * 2004-09-27 2005-11-02 厦门大学 Capacitance pressure sensor for vacuum measurement
CN102169038A (en) * 2011-01-10 2011-08-31 中国电子科技集团公司第五十五研究所 Side wall protection method for MEMS (Micro Electronic Mechanical System) silicon capacitive pressure transducer with sandwich structure
CN102445298A (en) * 2011-11-25 2012-05-09 沈阳仪表科学研究院 Method for improving overloading response speed of silicon capacitive pressure sensor
CN203365045U (en) * 2013-07-16 2013-12-25 东南大学 Capacitive air pressure sensor of microelectronic mechanical system
CN107356367A (en) * 2017-07-20 2017-11-17 中国电子科技集团公司第四十九研究所 One kind miniaturization differential type double-capacitance film vacuum sensor
CN108700479A (en) * 2016-02-25 2018-10-23 英福康股份公司 Capacitive vacuum measuring cell with multiple electrodes

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1379228A (en) * 2002-05-13 2002-11-13 厦门大学 Pressure sensor with electrostatic bonding and sealed capacitor cavity and its preparing process
CN2738224Y (en) * 2004-09-27 2005-11-02 厦门大学 Capacitance pressure sensor for vacuum measurement
CN102169038A (en) * 2011-01-10 2011-08-31 中国电子科技集团公司第五十五研究所 Side wall protection method for MEMS (Micro Electronic Mechanical System) silicon capacitive pressure transducer with sandwich structure
CN102445298A (en) * 2011-11-25 2012-05-09 沈阳仪表科学研究院 Method for improving overloading response speed of silicon capacitive pressure sensor
CN203365045U (en) * 2013-07-16 2013-12-25 东南大学 Capacitive air pressure sensor of microelectronic mechanical system
CN108700479A (en) * 2016-02-25 2018-10-23 英福康股份公司 Capacitive vacuum measuring cell with multiple electrodes
CN107356367A (en) * 2017-07-20 2017-11-17 中国电子科技集团公司第四十九研究所 One kind miniaturization differential type double-capacitance film vacuum sensor

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111982383A (en) * 2020-07-06 2020-11-24 厦门大学 Differential pressure contact type MEMS capacitance film vacuum gauge

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