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CN112211017A - A kind of alkaline pulping method using coconut husk as raw material - Google Patents

A kind of alkaline pulping method using coconut husk as raw material Download PDF

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Publication number
CN112211017A
CN112211017A CN202011164744.9A CN202011164744A CN112211017A CN 112211017 A CN112211017 A CN 112211017A CN 202011164744 A CN202011164744 A CN 202011164744A CN 112211017 A CN112211017 A CN 112211017A
Authority
CN
China
Prior art keywords
coconut
coconut husk
pulp
raw material
papermaking
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202011164744.9A
Other languages
Chinese (zh)
Inventor
管若伶
张立晨
贠子平
黄逊伟
雷方
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hainan Tropical Ocean University
Original Assignee
Hainan Tropical Ocean University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hainan Tropical Ocean University filed Critical Hainan Tropical Ocean University
Priority to CN202011164744.9A priority Critical patent/CN112211017A/en
Publication of CN112211017A publication Critical patent/CN112211017A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21BFIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00Fibrous raw materials or their mechanical treatment
    • D21B1/04Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • D21B1/06Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by dry methods
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C5/00Other processes for obtaining cellulose, e.g. cooking cotton linters ; Processes characterised by the choice of cellulose-containing starting materials
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21DTREATMENT OF THE MATERIALS BEFORE PASSING TO THE PAPER-MAKING MACHINE
    • D21D1/00Methods of beating or refining; Beaters of the Hollander type
    • D21D1/02Methods of beating; Beaters of the Hollander type
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21DTREATMENT OF THE MATERIALS BEFORE PASSING TO THE PAPER-MAKING MACHINE
    • D21D1/00Methods of beating or refining; Beaters of the Hollander type
    • D21D1/20Methods of refining
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21DTREATMENT OF THE MATERIALS BEFORE PASSING TO THE PAPER-MAKING MACHINE
    • D21D5/00Purification of the pulp suspension by mechanical means; Apparatus therefor
    • D21D5/02Straining or screening the pulp
    • D21D5/04Flat screens
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21FPAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
    • D21F11/00Processes for making continuous lengths of paper, or of cardboard, or of wet web for fibre board production, on paper-making machines

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Paper (AREA)

Abstract

本发明公开了一种以椰子皮为原料的碱法制纸浆方法,包括如下步骤:步骤一、备料:将椰子皮打散将椰子壳去除,得到打散椰子皮;步骤二、晾晒:将打散椰子皮自然晾晒一到两天得到晾晒后椰子皮;步骤三、浸泡;步骤四、蒸煮;步骤五、洗涤:使用筛网过筛,将滤渣洗净除去木素以及残余试剂;步骤六、磨浆:将滤渣加入磨浆机磨浆得到纸浆;步骤七、打浆:将磨好的纸浆加入造纸胶,纸浆的干料与造纸胶的质量比为1000:3‑8;然后通过拍打将纸浆与水混合;步骤八、抄纸:利用40目抄网进行抄纸,烘干即得到椰子皮纸。本发明提供了一种以椰子皮为原料制作纸张的方法,有效的利用了椰子皮资源,将椰子皮充分利用,变废为宝,提高经济效益的同时降低了环境污染。The invention discloses an alkaline pulping method using coconut husk as a raw material. The coconut husk is naturally aired for one to two days to obtain the sun-dried coconut husk; step 3, soaking; step 4, cooking; step 5, washing: sieve with a mesh, wash the filter residue to remove lignin and residual reagents; step 6, grind Pulp: add the filter residue to the refiner for refining to obtain pulp; Step 7, beating: add the ground pulp to the papermaking glue, and the mass ratio of the dry material of the pulp to the papermaking glue is 1000:3-8; Mixing with water; Step 8, papermaking: utilize 40 mesh making nets to make paper, and dry to obtain coconut husk paper. The invention provides a method for making paper with coconut peel as raw material, effectively utilizes coconut peel resources, fully utilizes coconut peel, turns waste into treasure, improves economic benefit and reduces environmental pollution.

Description

Alkaline method for making paper pulp by using coconut peel as raw material
Technical Field
The invention belongs to the field of papermaking environmental protection, and particularly relates to an alkaline method for making paper pulp by using coconut peel as a raw material.
Background
The coconut comprises coconut juice, coconut, meat, coconut shell and coconut peel from inside to outside in sequence. The coconut meat and the coconut juice can be used as food, the coconut shell can be used as a carved product, and the coconut skin is generally discarded as waste, so that resources are wasted, and the environment is polluted. At present, no method for making paper pulp by using coconut husk as raw material is available in China.
Disclosure of Invention
In order to solve the problems, the invention discloses an alkaline method for making paper pulp by taking coconut husk as a raw material. The invention provides a method for making paper by taking coconut peel as a raw material, which effectively utilizes coconut peel resources, fully utilizes the coconut peel, changes waste into valuable, improves economic benefits and reduces environmental pollution.
In order to achieve the purpose, the technical scheme of the invention is as follows:
an alkaline method for making paper pulp by using coconut peels as a raw material comprises the following steps:
step one, preparing materials: breaking up the coconut peel to remove the coconut shell, thereby obtaining broken up coconut peel;
step two, airing: naturally airing the scattered coconut peel for one to two days to obtain the aired coconut peel;
step three, soaking: fully soaking the coconut peel by using NaOH solution for 24 +/-5 hours until lignin is separated from fibers;
step four, cooking: steaming and boiling for 3-5 hours at 150-180 ℃;
step five, washing: sieving with a screen, and cleaning the filter residue to remove lignin and residual reagent;
step six, grinding the pulp: adding the filter residue into a pulping machine and pulping to obtain paper pulp;
step seven, pulping: adding the ground paper pulp into papermaking adhesive, wherein the mass ratio of dry materials of the paper pulp to the papermaking adhesive is 1000: 3-8; then mixing the pulp with water by beating;
step eight, papermaking: and (5) papermaking by using a 40-mesh papermaking net, and drying to obtain the coconut husk paper.
In a further improvement, the NaOH solution in the third step is a 1% NaOH solution.
In a further improvement, in the fifth step, the screen is a 40-mesh screen.
And in the sixth step, the filter residue is added into a pulping machine to be circularly ground for 5 times to obtain paper pulp.
The silver-containing composite adsorption film prepared by the alkaline pulping method taking coconut peel as the raw material is used for adsorbing bromide ions.
The invention has the advantages that:
the invention provides a method for making paper by taking coconut peel as a raw material, which effectively utilizes coconut peel resources, fully utilizes the coconut peel, changes waste into valuable, improves economic benefits and reduces environmental pollution.
Detailed Description
The present invention is further illustrated by the following examples.
Examples
An alkaline method for making paper pulp by using coconut peels as a raw material comprises the following steps:
step one, preparing materials: breaking up the coconut peel to remove the coconut shell, thereby obtaining broken up coconut peel;
step two, airing: naturally airing the scattered coconut peel for one to two days to obtain the aired coconut peel;
step three, soaking: fully soaking the coconut peel by using 1% NaOH solution for 24 +/-5 hours until lignin is separated from fibers;
step four, cooking: steaming and boiling the mixture in a 1% NaOH solution at 150-180 ℃ for 3-5 hours;
step five, washing: sieving with 40 mesh sieve, cleaning the residue to remove lignin and residual reagent;
step six, grinding the pulp: adding the filter residue into a pulping machine, and circularly pulping for 5 times to obtain paper pulp;
step seven, pulping: adding the ground paper pulp into papermaking adhesive, wherein the mass ratio of dry materials of the paper pulp to the papermaking adhesive is 1000: 3-8; then mixing the pulp with water by beating;
step eight, papermaking: and (5) papermaking by using a 40-mesh papermaking net, and drying to obtain the coconut husk paper.
While embodiments of the invention have been disclosed above, it is not limited to the applications set forth in the description and embodiments, which are fully applicable to various fields of endeavor for which the invention is intended, and further modifications may readily be effected therein by those skilled in the art, without departing from the general concept defined by the claims and their equivalents, which are to be limited not to the specific details shown and described herein.

Claims (4)

1.一种以椰子皮为原料的碱法制纸浆方法,其特征在于,包括如下步骤:1. a kind of alkali process pulping method taking coconut husk as raw material, is characterized in that, comprises the steps: 步骤一、备料:将椰子皮打散将椰子壳去除,得到打散椰子皮;Step 1. Preparation: Disperse the coconut husk and remove the coconut husk to obtain the smashed coconut husk; 步骤二、晾晒:将打散椰子皮自然晾晒一到两天得到晾晒后椰子皮;Step 2. Drying: Naturally dry the scattered coconut skin for one to two days to obtain the coconut skin after drying; 步骤三、浸泡:使用NaOH溶液充分浸泡椰子皮,浸泡时间为24±5h,至木素与纤维分离;Step 3, soaking: use NaOH solution to fully soak the coconut skin, the soaking time is 24±5h, until the lignin and fiber are separated; 步骤四、蒸煮:在150~180℃下蒸煮3~5小时;Step 4. Cooking: Cooking at 150~180℃ for 3~5 hours; 步骤五、洗涤:使用筛网过筛,将滤渣洗净除去木素以及残余试剂;Step 5. Washing: sieve with a mesh, and wash the filter residue to remove lignin and residual reagents; 步骤六、磨浆:将滤渣加入磨浆机磨浆得到纸浆;Step 6. Refining: adding the filter residue to the refiner for refining to obtain pulp; 步骤七、打浆:将磨好的纸浆加入造纸胶,纸浆的干料与造纸胶的质量比为1000:3-8;然后通过拍打将纸浆与水混合;Step 7. Beating: adding the ground pulp to the papermaking glue, the mass ratio of the dry material of the pulp to the papermaking glue is 1000:3-8; then mixing the pulp and water by beating; 步骤八、抄纸:利用40目抄网进行抄纸,烘干即得到椰子皮纸。Step 8, papermaking: utilize 40 mesh making net to carry out papermaking, and dry to obtain coconut husk paper. 2.如权利要求1所述的以椰子皮为原料的碱法制纸浆方法,其特征在于,所述步骤三中的NaOH溶液为1%NaOH溶液。2. the alkali process pulping method that takes coconut husk as raw material as claimed in claim 1, is characterized in that, the NaOH solution in described step 3 is 1%NaOH solution. 3.如权利要求1所述的以椰子皮为原料的碱法制纸浆方法,其特征在于,所述步骤五中,筛网为40目筛网。3. the alkali process pulping method that takes coconut husk as raw material as claimed in claim 1, is characterized in that, in described step 5, screen is 40 mesh screen. 4.如权利要求1所述的以椰子皮为原料的碱法制纸浆方法,其特征在于,所述步骤六中,将滤渣加入磨浆机循环磨浆5次得到纸浆。4. The alkali-processed pulping method using coconut husk as a raw material as claimed in claim 1, wherein in the step 6, the filter residue is added to the refiner for 5 times of circulating refining to obtain pulp.
CN202011164744.9A 2020-10-27 2020-10-27 A kind of alkaline pulping method using coconut husk as raw material Pending CN112211017A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113445345A (en) * 2021-07-06 2021-09-28 海南热带海洋学院 Mixer for manufacturing logistics packaging bags
CN115305738A (en) * 2022-08-22 2022-11-08 华南理工大学 A kind of LCP cleaning pulping method

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Publication number Priority date Publication date Assignee Title
CN1324967A (en) * 2000-05-18 2001-12-05 夏百平 Coconut husk fiber paper pulp making process
CN101899794A (en) * 2009-05-27 2010-12-01 北京英力和泓新材料技术有限公司 Green process for extracting fibers from plants
EP2333151A1 (en) * 2009-12-11 2011-06-15 Nederlandse Organisatie voor toegepast -natuurwetenschappelijk onderzoek TNO Novel method for processing lignocellulose containing material
CN106283935A (en) * 2016-08-16 2017-01-04 东华大学 Method and the purposes of pipe fiber is separated from coir fibre
CN108748592A (en) * 2018-06-22 2018-11-06 海南大学 The method that discarded coir fibre prepares egg tray padded coaming
CN109162132A (en) * 2018-09-19 2019-01-08 安徽九天印务有限公司 A kind of extracting method of coir fibre
TW201928149A (en) * 2017-12-15 2019-07-16 洪奕杉 Method for preparing paper or papermaking raw material to obtain papers with better tension and strength

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1324967A (en) * 2000-05-18 2001-12-05 夏百平 Coconut husk fiber paper pulp making process
CN101899794A (en) * 2009-05-27 2010-12-01 北京英力和泓新材料技术有限公司 Green process for extracting fibers from plants
EP2333151A1 (en) * 2009-12-11 2011-06-15 Nederlandse Organisatie voor toegepast -natuurwetenschappelijk onderzoek TNO Novel method for processing lignocellulose containing material
CN106283935A (en) * 2016-08-16 2017-01-04 东华大学 Method and the purposes of pipe fiber is separated from coir fibre
TW201928149A (en) * 2017-12-15 2019-07-16 洪奕杉 Method for preparing paper or papermaking raw material to obtain papers with better tension and strength
CN108748592A (en) * 2018-06-22 2018-11-06 海南大学 The method that discarded coir fibre prepares egg tray padded coaming
CN109162132A (en) * 2018-09-19 2019-01-08 安徽九天印务有限公司 A kind of extracting method of coir fibre

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张雪: "麦草的气穴辅助脱木素技术综述", 《国际造纸》, no. 06, 15 December 2014 (2014-12-15) *
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113445345A (en) * 2021-07-06 2021-09-28 海南热带海洋学院 Mixer for manufacturing logistics packaging bags
CN113445345B (en) * 2021-07-06 2022-07-12 海南热带海洋学院 Mixer for manufacturing logistics packaging bags
CN115305738A (en) * 2022-08-22 2022-11-08 华南理工大学 A kind of LCP cleaning pulping method

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Application publication date: 20210112

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