CN113855580A - Jelly-like mouth wash capable of melting in mouth and preparation method thereof - Google Patents
Jelly-like mouth wash capable of melting in mouth and preparation method thereof Download PDFInfo
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- CN113855580A CN113855580A CN202111384795.7A CN202111384795A CN113855580A CN 113855580 A CN113855580 A CN 113855580A CN 202111384795 A CN202111384795 A CN 202111384795A CN 113855580 A CN113855580 A CN 113855580A
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- 239000002324 mouth wash Substances 0.000 title claims abstract description 31
- 229940051866 mouthwash Drugs 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 26
- 238000002844 melting Methods 0.000 title description 5
- 230000008018 melting Effects 0.000 title description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 55
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 48
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 claims abstract description 38
- 239000000843 powder Substances 0.000 claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims abstract description 20
- 235000011187 glycerol Nutrition 0.000 claims abstract description 20
- 239000000049 pigment Substances 0.000 claims abstract description 20
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 20
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 20
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 20
- 239000000600 sorbitol Substances 0.000 claims abstract description 20
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims abstract description 19
- WSELJKAMVUHMJP-PUZYILPLSA-N (2s,3r,4s,5r)-2,3-dichloro-2,3,4,5,6-pentahydroxyhexanoyl chloride Chemical compound OC[C@@H](O)[C@H](O)[C@@](O)(Cl)[C@](O)(Cl)C(Cl)=O WSELJKAMVUHMJP-PUZYILPLSA-N 0.000 claims abstract description 19
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims abstract description 19
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000004359 castor oil Substances 0.000 claims abstract description 19
- 235000019438 castor oil Nutrition 0.000 claims abstract description 19
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims abstract description 19
- 229940041616 menthol Drugs 0.000 claims abstract description 19
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000011775 sodium fluoride Substances 0.000 claims abstract description 19
- 235000013024 sodium fluoride Nutrition 0.000 claims abstract description 19
- 239000000230 xanthan gum Substances 0.000 claims abstract description 19
- 229920001285 xanthan gum Polymers 0.000 claims abstract description 19
- 229940082509 xanthan gum Drugs 0.000 claims abstract description 19
- 235000010493 xanthan gum Nutrition 0.000 claims abstract description 19
- 239000000811 xylitol Substances 0.000 claims abstract description 19
- 235000010447 xylitol Nutrition 0.000 claims abstract description 19
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims abstract description 19
- 229960002675 xylitol Drugs 0.000 claims abstract description 19
- 239000001509 sodium citrate Substances 0.000 claims abstract description 16
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims abstract description 16
- 239000000155 melt Substances 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims description 24
- 239000000463 material Substances 0.000 claims description 19
- 230000001804 emulsifying effect Effects 0.000 claims description 18
- 238000010438 heat treatment Methods 0.000 claims description 18
- 239000007788 liquid Substances 0.000 claims description 12
- 239000003795 chemical substances by application Substances 0.000 claims description 9
- 239000013078 crystal Substances 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 9
- 238000004140 cleaning Methods 0.000 claims description 7
- 230000001954 sterilising effect Effects 0.000 claims description 7
- 235000015165 citric acid Nutrition 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- 230000000249 desinfective effect Effects 0.000 claims description 6
- 238000007599 discharging Methods 0.000 claims description 6
- 238000007689 inspection Methods 0.000 claims description 6
- 235000011083 sodium citrates Nutrition 0.000 claims description 6
- 239000002562 thickening agent Substances 0.000 claims description 6
- 125000003118 aryl group Chemical group 0.000 claims description 3
- 239000003755 preservative agent Substances 0.000 claims description 3
- 230000002335 preservative effect Effects 0.000 claims description 3
- 230000008569 process Effects 0.000 claims description 3
- 238000001223 reverse osmosis Methods 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- 239000000499 gel Substances 0.000 abstract description 16
- 235000015110 jellies Nutrition 0.000 abstract description 6
- 239000008274 jelly Substances 0.000 abstract description 6
- 238000005516 engineering process Methods 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 16
- 210000000214 mouth Anatomy 0.000 description 11
- 239000011780 sodium chloride Substances 0.000 description 8
- 241000894006 Bacteria Species 0.000 description 3
- 206010006326 Breath odour Diseases 0.000 description 3
- 235000003599 food sweetener Nutrition 0.000 description 3
- 239000003765 sweetening agent Substances 0.000 description 3
- 208000032139 Halitosis Diseases 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 239000003906 humectant Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 235000019605 sweet taste sensations Nutrition 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 208000002064 Dental Plaque Diseases 0.000 description 1
- 208000025157 Oral disease Diseases 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 208000014151 Stomatognathic disease Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 208000002925 dental caries Diseases 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000010794 food waste Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000000873 masking effect Effects 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 208000030194 mouth disease Diseases 0.000 description 1
- 235000021096 natural sweeteners Nutrition 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
- A61K8/21—Fluorides; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Emergency Medicine (AREA)
- Dispersion Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Inorganic Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a jelly-shaped mouthwash which melts immediately when entering the mouth and a preparation method thereof, and the mouthwash comprises the following components in percentage by weight: 0.8 to 1.5 percent of PEG-40 hydrogenated castor oil, 0.1 to 0.2 percent of menthol, 0.1 to 0.5 percent of edible essence, 88 to 90 percent of water, 3 to 7 percent of sorbitol, 1 to 3 percent of edible glycerin, 0.01 to 0.03 percent of trichlorogalactose, 0.3 to 0.8 percent of xylitol, 0.12 to 0.32 percent of gel powder, 0.0005 to 0.0015 percent of xanthan gum, 0.005 to 0.015 percent of citric acid, 0.1 to 0.4 percent of sodium citrate, 0.006 to 0.016 percent of sodium fluoride, 0.2 to 0.5 percent of sodium benzoate and 0.01 to 0.25 percent of edible pigment, compared with the traditional water-shaped mouthwash on the market, the jelly mouthwash is novel in a jelly gel state, is immediately converted into water after 3 seconds, the working efficiency is higher and the resource loss is lower by combining a freshener and an essence technology, the mouthfeel of the product can be kept unchanged at 50 ℃, meanwhile, the product has the advantages of small volume, convenient carrying, no pollution, no public nuisance, environmental protection, safety, edible and the like.
Description
Technical Field
The invention relates to the technical field of cavity care products, in particular to jelly-shaped mouthwash which melts immediately in the mouth and a preparation method thereof.
Background
Mouthwash (Mouthwash), also known as gargles (Oral rings), has been popular in developed countries in europe and america for many years and may have a great relationship with societal life eties, and has the main effects of cleaning the Oral cavity, masking bad breath caused by decomposition of food residues by bacteria or yeasts, and leaving a pleasant and refreshing feeling in the Oral cavity. In recent years, due to the strong market competition, products which emphasize the functions of preventing and treating dental and oral diseases and improving oral health, in addition to refreshing breath and claiming bacteria capable of eliminating halitosis, are increasing.
The existing gargle aquatic products are large in size, inconvenient to carry and not strong in environmental protection.
Disclosure of Invention
The invention aims to provide a jelly-shaped mouthwash which melts immediately when entering the mouth and a preparation method thereof, so as to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
a jelly-like mouth wash which melts immediately when entering the mouth and a preparation method thereof are disclosed, which comprises the following components in percentage by weight: 0.8-1.5% of PEG-40 hydrogenated castor oil, 0.1-0.2% of menthol, 0.1-0.5% of edible essence, 88-90% of water, 3-7% of sorbitol, 1-3% of edible glycerol, 0.01-0.03% of trichlorogalactose, 0.3-0.8% of xylitol, 0.12-0.32% of gel powder, 0.0005-0.0015% of xanthan gum, 0.005-0.015% of citric acid, 0.1-0.4% of sodium citrate, 0.006-0.016% of sodium fluoride, 0.2-0.5% of sodium benzoate and 0.01-0.25% of edible pigment, and the preparation method comprises the following steps:
the method comprises the following steps: cleaning and disinfecting the product according to the sanitary requirement;
step two: further placing a certain amount of PEG-40 hydrogenated castor oil, menthol and edible essence into a container in advance, heating to 50 ℃, and dissolving uniformly for later use;
step three: further putting a certain amount of water into an emulsifying pot, heating to 90 ℃, sterilizing, heating for 15min, cooling to 50 ℃, further adding a certain amount of sorbitol, edible glycerol, trichlorogalactose, xylitol, gel powder, xanthan gum, citric acid, sodium citrate and sodium fluoride into the emulsifying pot, starting stirring, uniformly dissolving, homogenizing for 30s, keeping stirring, keeping the temperature to 50 ℃, and keeping the temperature for 10 min;
step four: adding the material dissolved uniformly in the step two into the material in the step three at 50 ℃, stirring uniformly to be transparent, further adding sodium benzoate and edible pigment into an emulsifying pot, stirring uniformly, discharging at 38 ℃ after inspection is qualified, using a heat-insulating barrel for a standing workshop, and continuously operating when filling, wherein the temperature cannot be lower than 35 ℃.
As a further scheme of the invention: the PEG-40 hydrogenated castor oil, the menthol and the edible essence jointly form an agent A, the water, the sorbitol, the edible glycerol, the trichlorogalactose, the xylitol, the gel powder, the xanthan gum, the citric acid, the sodium citrate and the sodium fluoride jointly form an agent B, and the sodium benzoate and the edible pigment jointly form an agent C.
As a still further scheme of the invention: the PEG-40 hydrogenated castor oil is a solubilizer and is in a liquid state; the menthol is a freshener and is in a crystal shape.
As a still further scheme of the invention: the edible essence is an aromatic.
As a still further scheme of the invention: the water is colorless transparent liquid, and is prepared by adopting a secondary reverse osmosis process; the sorbitol is a colorless transparent liquid.
As a still further scheme of the invention: the edible glycerin is colorless transparent liquid.
As a still further scheme of the invention: the trichlorogalactose is powdery.
As a still further scheme of the invention: the xylitol is in a white crystal shape.
As a still further scheme of the invention: the gel powder is a food-grade thickener and is powdery.
As a still further scheme of the invention: the xanthan gum is a food-grade thickener and is in a powder shape; the sodium fluoride is white crystals; the sodium benzoate is powdery and is a food-grade preservative; the edible pigment is in powder form.
Compared with the prior art, the invention has the beneficial effects that:
1. compared with the traditional watery mouthwash on the market, the jelly mouthwash of the invention has novel appearance and is immediately turned into water after 3 seconds of entrance;
2. the combination of the freshener and the essence technology achieves higher efficiency and lower resource loss, and the taste and the aroma of the product can be maintained at 50 ℃;
3. the product has the advantages of small volume, convenient carrying, no pollution, no public nuisance, environmental protection, safety, edible and the like.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the embodiment of the invention, the jelly-shaped mouthwash which melts immediately when entering the mouth and the preparation method thereof comprise the following components in percentage by weight: 0.8-1.5% of PEG-40 hydrogenated castor oil, 0.1-0.2% of menthol, 0.1-0.5% of edible essence, 88-90% of water, 3-7% of sorbitol, 1-3% of edible glycerol, 0.01-0.03% of trichlorogalactose, 0.3-0.8% of xylitol, 0.12-0.32% of gel powder, 0.0005-0.0015% of xanthan gum, 0.005-0.015% of citric acid, 0.1-0.4% of sodium citrate, 0.006-0.016% of sodium fluoride, 0.2-0.5% of sodium benzoate and 0.01-0.25% of edible pigment, and the preparation method comprises the following steps:
the method comprises the following steps: cleaning and disinfecting the product according to the sanitary requirement;
step two: further placing a certain amount of PEG-40 hydrogenated castor oil, menthol and edible essence into a container in advance, heating to 50 ℃, and dissolving uniformly for later use;
step three: further putting a certain amount of water into an emulsifying pot, heating to 90 ℃, sterilizing, heating for 15min, cooling to 50 ℃, further adding a certain amount of sorbitol, edible glycerol, trichlorogalactose, xylitol, gel powder, xanthan gum, citric acid, sodium citrate and sodium fluoride into the emulsifying pot, starting stirring, uniformly dissolving, homogenizing for 30s, keeping stirring, keeping the temperature to 50 ℃, and keeping the temperature for 10 min;
step four: adding the material dissolved uniformly in the step two into the material in the step three at 50 ℃, stirring uniformly to be transparent, further adding sodium benzoate and edible pigment into an emulsifying pot, stirring uniformly, discharging at 38 ℃ after inspection is qualified, using a heat-insulating barrel for a standing workshop, and continuously operating when filling, wherein the temperature cannot be lower than 35 ℃.
The PEG-40 hydrogenated castor oil, the menthol and the edible essence jointly form an agent A, the water, the sorbitol, the edible glycerol, the trichlorogalactose, the xylitol, the gel powder, the xanthan gum, the citric acid, the sodium citrate and the sodium fluoride jointly form an agent B, and the sodium benzoate and the edible pigment jointly form an agent C;
the PEG-40 hydrogenated castor oil is a solubilizer, is liquid, can solubilize essence and a freshener, and enables the solution to be transparent;
the menthol is a freshener, is in a crystal shape, can refresh breath, refreshes the brain, and has strong refreshing feeling;
the edible essence is an aromatic, can cover halitosis, and has lasting fragrance in the oral cavity;
the water is colorless transparent liquid, and is prepared by adopting a two-stage reverse osmosis process, so that the quality is high;
the sorbitol is colorless transparent liquid, and the humectant has sweet taste and better mouthfeel due to the matching of the sorbitol and a sweetening agent;
the edible glycerin is colorless transparent liquid, and the humectant has sweet taste and better mouthfeel due to the matching of the edible glycerin and the sweetener;
the trichlorogalactose is powdery and is a sweetener, and can be used in mouthwash by adopting a 0 sugar concept;
the xylitol is white crystal, is a natural sweetener and prevents tooth decay;
the gel powder is a food-grade thickener, is powdery, and can form a jelly shape when being added into mouthwash;
the xanthan gum is a food-grade thickener and is in a powder shape;
the sodium fluoride is a white crystal, has the functions of sterilization and bacteriostasis, removes dental plaque bacteria and solves the problem of oral health;
the sodium benzoate is powder, food-grade preservative, and can control microorganisms by adding 0.3-0.5% of the sodium benzoate;
the edible pigment is powder and edible natural pigment.
Example one
A jelly-like mouth wash which melts immediately when entering the mouth and a preparation method thereof are disclosed, which comprises the following components in percentage by weight: 0.8% of PEG-40 hydrogenated castor oil, 0.1% of menthol, 0.1% of edible essence, 88% of water, 3% of sorbitol, 1% of edible glycerol, 0.01% of trichlorogalactose, 0.3% of xylitol, 0.12% of gel powder, 0.0005% of xanthan gum, 0.005% of citric acid, 0.1% of sodium citrate, 0.006% of sodium fluoride, 0.2% of sodium benzoate and 0.01% of edible pigment, and the preparation method comprises the following steps:
the method comprises the following steps: cleaning and disinfecting the product according to the sanitary requirement;
step two: further placing a certain amount of PEG-40 hydrogenated castor oil, menthol and edible essence into a container in advance, heating to 50 ℃, and dissolving uniformly for later use;
step three: further putting a certain amount of water into an emulsifying pot, heating to 90 ℃, sterilizing, heating for 15min, cooling to 50 ℃, further adding a certain amount of sorbitol, edible glycerol, trichlorogalactose, xylitol, gel powder, xanthan gum, citric acid, sodium citrate and sodium fluoride into the emulsifying pot, starting stirring, uniformly dissolving, homogenizing for 30s, keeping stirring, keeping the temperature to 50 ℃, and keeping the temperature for 10 min;
step four: adding the material dissolved uniformly in the step two into the material in the step three at 50 ℃, stirring uniformly to be transparent, further adding sodium benzoate and edible pigment into an emulsifying pot, stirring uniformly, discharging at 38 ℃ after inspection is qualified, using a heat-insulating barrel for a standing workshop, and continuously operating when filling, wherein the temperature cannot be lower than 35 ℃.
Example two
A jelly-like mouth wash which melts immediately when entering the mouth and a preparation method thereof are disclosed, which comprises the following components in percentage by weight: 1.2% of PEG-40 hydrogenated castor oil, 0.15% of menthol, 0.3% of edible essence, 89.804% of water, 5% of sorbitol, 2% of edible glycerol, 0.025% of trichlorogalactose, 0.5% of xylitol, 0.22% of gel powder, 0.001% of xanthan gum, 0.01% of citric acid, 0.2% of sodium citrate, 0.01% of sodium fluoride, 0.45% of sodium benzoate and 0.13% of edible pigment, and the preparation method comprises the following steps:
the method comprises the following steps: cleaning and disinfecting the product according to the sanitary requirement;
step two: further placing a certain amount of PEG-40 hydrogenated castor oil, menthol and edible essence into a container in advance, heating to 50 ℃, and dissolving uniformly for later use;
step three: further putting a certain amount of water into an emulsifying pot, heating to 90 ℃, sterilizing, heating for 15min, cooling to 50 ℃, further adding a certain amount of sorbitol, edible glycerol, trichlorogalactose, xylitol, gel powder, xanthan gum, citric acid, sodium citrate and sodium fluoride into the emulsifying pot, starting stirring, uniformly dissolving, homogenizing for 30s, keeping stirring, keeping the temperature to 50 ℃, and keeping the temperature for 10 min;
step four: adding the material dissolved uniformly in the step two into the material in the step three at 50 ℃, stirring uniformly to be transparent, further adding sodium benzoate and edible pigment into an emulsifying pot, stirring uniformly, discharging at 38 ℃ after inspection is qualified, using a heat-insulating barrel for a standing workshop, and continuously operating when filling, wherein the temperature cannot be lower than 35 ℃.
EXAMPLE III
A jelly-like mouth wash which melts immediately when entering the mouth and a preparation method thereof are disclosed, which comprises the following components in percentage by weight: 1.5% of PEG-40 hydrogenated castor oil, 0.2% of menthol, 0.5% of edible essence, 90% of water, 7% of sorbitol, 3% of edible glycerol, 0.03% of trichlorogalactose, 0.8% of xylitol, 0.32% of gel powder, 0.0015% of xanthan gum, 0.015% of citric acid, 0.4% of sodium citrate, 0.016% of sodium fluoride, 0.5% of sodium benzoate and 0.25% of edible pigment, and the preparation method comprises the following steps:
the method comprises the following steps: cleaning and disinfecting the product according to the sanitary requirement;
step two: further placing a certain amount of PEG-40 hydrogenated castor oil, menthol and edible essence into a container in advance, heating to 50 ℃, and dissolving uniformly for later use;
step three: further putting a certain amount of water into an emulsifying pot, heating to 90 ℃, sterilizing, heating for 15min, cooling to 50 ℃, further adding a certain amount of sorbitol, edible glycerol, trichlorogalactose, xylitol, gel powder, xanthan gum, citric acid, sodium citrate and sodium fluoride into the emulsifying pot, starting stirring, uniformly dissolving, homogenizing for 30s, keeping stirring, keeping the temperature to 50 ℃, and keeping the temperature for 10 min;
step four: adding the material dissolved uniformly in the step two into the material in the step three at 50 ℃, stirring uniformly to be transparent, further adding sodium benzoate and edible pigment into an emulsifying pot, stirring uniformly, discharging at 38 ℃ after inspection is qualified, using a heat-insulating barrel for a standing workshop, and continuously operating when filling, wherein the temperature cannot be lower than 35 ℃.
Experimental data
Experimental data sheet
The experimental steps are as follows:
dividing 600 g of jelly mouthwash into 6 beakers on average, weighing 100 g of material in each beaker, wherein the numbers are beaker 1, beaker 2, beaker 3, beaker 4, beaker 5 and beaker 6, weighing sodium chloride on a balance, simultaneously placing 0.02 g of sodium chloride in each beaker 1, placing 0.05 g of sodium chloride in each beaker 2, placing 0.1 g of sodium chloride in each beaker 3, placing 0.12 g of sodium chloride in each beaker 4, placing 0.15 g of sodium chloride in each beaker 5, placing 0.2 g of sodium chloride in each beaker 6, testing the time by using a stopwatch, wherein the materials in each beaker 5 and each beaker 6 are melted into water in 1 second, the materials in each beaker 2, each beaker 3, each beaker 4 and each 3 seconds are melted into water, and the materials in each beaker 1 and each 20 seconds are melted into water in 20 seconds
And (4) experimental conclusion:
the material melting time of the beaker 2, the beaker 3 and the beaker 4 is just right and is qualified; the material body melting time of the beaker 5 and the beaker 6 is too fast and unqualified; the melting time of the material body of the beaker 1 is too slow to be qualified, so that the sodium chloride of 0.05-0.12 percent has just influence on the state of the jelly mouthwash.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that various changes in the embodiments and/or modifications of the invention can be made, and equivalents and modifications of some features of the invention can be made without departing from the spirit and scope of the invention.
Claims (10)
1. A jelly-like mouth wash which melts immediately when entering the mouth and a preparation method thereof are characterized in that: the components and the weight percentage thereof are as follows: 0.8-1.5% of PEG-40 hydrogenated castor oil, 0.1-0.2% of menthol, 0.1-0.5% of edible essence, 88-90% of water, 3-7% of sorbitol, 1-3% of edible glycerol, 0.01-0.03% of trichlorogalactose, 0.3-0.8% of xylitol, 0.12-0.32% of gel powder, 0.0005-0.0015% of xanthan gum, 0.005-0.015% of citric acid, 0.1-0.4% of sodium citrate, 0.006-0.016% of sodium fluoride, 0.2-0.5% of sodium benzoate and 0.01-0.25% of edible pigment, and the preparation method comprises the following steps:
the method comprises the following steps: cleaning and disinfecting the product according to the sanitary requirement;
step two: further placing a certain amount of PEG-40 hydrogenated castor oil, menthol and edible essence into a container in advance, heating to 50 ℃, and dissolving uniformly for later use;
step three: further putting a certain amount of water into an emulsifying pot, heating to 90 ℃, sterilizing, heating for 15min, cooling to 50 ℃, further adding a certain amount of sorbitol, edible glycerol, trichlorogalactose, xylitol, gel powder, xanthan gum, citric acid, sodium citrate and sodium fluoride into the emulsifying pot, starting stirring, uniformly dissolving, homogenizing for 30s, keeping stirring, keeping the temperature to 50 ℃, and keeping the temperature for 10 min;
step four: adding the material dissolved uniformly in the step two into the material in the step three at 50 ℃, stirring uniformly to be transparent, further adding sodium benzoate and edible pigment into an emulsifying pot, stirring uniformly, discharging at 38 ℃ after inspection is qualified, using a heat-insulating barrel for a standing workshop, and continuously operating when filling, wherein the temperature cannot be lower than 35 ℃.
2. The jelly-like mouthwash for immediate intake and the preparation method thereof according to claim 1, wherein: the PEG-40 hydrogenated castor oil, the menthol and the edible essence jointly form an agent A, the water, the sorbitol, the edible glycerol, the trichlorogalactose, the xylitol, the gel powder, the xanthan gum, the citric acid, the sodium citrate and the sodium fluoride jointly form an agent B, and the sodium benzoate and the edible pigment jointly form an agent C.
3. The jelly-like mouthwash for immediate intake and the preparation method thereof according to claim 1, wherein: the PEG-40 hydrogenated castor oil is a solubilizer and is in a liquid state; the menthol is a freshener and is in a crystal shape.
4. The jelly-like mouthwash for immediate intake and the preparation method thereof according to claim 1, wherein: the edible essence is an aromatic.
5. The jelly-like mouthwash for immediate intake and the preparation method thereof according to claim 1, wherein: the water is colorless transparent liquid, and is prepared by adopting a secondary reverse osmosis process; the sorbitol is a colorless transparent liquid.
6. The jelly-like mouthwash for immediate intake and the preparation method thereof according to claim 1, wherein: the edible glycerin is colorless transparent liquid.
7. The jelly-like mouthwash for immediate intake and the preparation method thereof according to claim 1, wherein: the trichlorogalactose is powdery.
8. The jelly-like mouthwash for immediate intake and the preparation method thereof according to claim 1, wherein: the xylitol is in a white crystal shape.
9. The jelly-like mouthwash for immediate intake and the preparation method thereof according to claim 1, wherein: the gel powder is a food-grade thickener and is powdery.
10. The jelly-like mouthwash for immediate intake and the preparation method thereof according to claim 1, wherein: the xanthan gum is a food-grade thickener and is in a powder shape; the sodium fluoride is white crystals; the sodium benzoate is powdery and is a food-grade preservative; the edible pigment is in powder form.
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Application publication date: 20211231 |