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EP2242821A1 - Additif conditionneur d'essence synthétique universel, procédé et produit en résultant - Google Patents

Additif conditionneur d'essence synthétique universel, procédé et produit en résultant

Info

Publication number
EP2242821A1
EP2242821A1 EP08867084A EP08867084A EP2242821A1 EP 2242821 A1 EP2242821 A1 EP 2242821A1 EP 08867084 A EP08867084 A EP 08867084A EP 08867084 A EP08867084 A EP 08867084A EP 2242821 A1 EP2242821 A1 EP 2242821A1
Authority
EP
European Patent Office
Prior art keywords
blend
weight
percent
primary
producing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
EP08867084A
Other languages
German (de)
English (en)
Inventor
Ronald J. Sloan
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BestLine International Research Inc
Original Assignee
BestLine International Research Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from PCT/US2007/088252 external-priority patent/WO2009078882A1/fr
Priority claimed from PCT/US2008/005095 external-priority patent/WO2008130676A1/fr
Application filed by BestLine International Research Inc filed Critical BestLine International Research Inc
Publication of EP2242821A1 publication Critical patent/EP2242821A1/fr
Ceased legal-status Critical Current

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    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M111/00—Lubrication compositions characterised by the base-material being a mixture of two or more compounds covered by more than one of the main groups C10M101/00 - C10M109/00, each of these compounds being essential
    • C10M111/04—Lubrication compositions characterised by the base-material being a mixture of two or more compounds covered by more than one of the main groups C10M101/00 - C10M109/00, each of these compounds being essential at least one of them being a macromolecular organic compound
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/143—Organic compounds mixtures of organic macromolecular compounds with organic non-macromolecular compounds
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    • C10L10/00—Use of additives to fuels or fires for particular purposes
    • C10L10/08—Use of additives to fuels or fires for particular purposes for improving lubricity; for reducing wear
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    • C10M141/00—Lubricating compositions characterised by the additive being a mixture of two or more compounds covered by more than one of the main groups C10M125/00 - C10M139/00, each of these compounds being essential
    • C10M141/08—Lubricating compositions characterised by the additive being a mixture of two or more compounds covered by more than one of the main groups C10M125/00 - C10M139/00, each of these compounds being essential at least one of them being an organic sulfur-, selenium- or tellurium-containing compound
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    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
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    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/042—Mixtures of base-materials and additives the additives being compounds of unknown or incompletely defined constitution only
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    • C10M169/04—Mixtures of base-materials and additives
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    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/14—Organic compounds
    • C10L1/20—Organic compounds containing halogen
    • C10L1/206—Organic compounds containing halogen macromolecular compounds
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    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/14—Organic compounds
    • C10L1/22—Organic compounds containing nitrogen
    • C10L1/23—Organic compounds containing nitrogen containing at least one nitrogen-to-oxygen bond, e.g. nitro-compounds, nitrates, nitrites
    • C10L1/231—Organic compounds containing nitrogen containing at least one nitrogen-to-oxygen bond, e.g. nitro-compounds, nitrates, nitrites nitro compounds; nitrates; nitrites
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    • C10L1/00—Liquid carbonaceous fuels
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    • C10L1/14—Organic compounds
    • C10L1/24—Organic compounds containing sulfur, selenium and/or tellurium
    • C10L1/2431—Organic compounds containing sulfur, selenium and/or tellurium sulfur bond to oxygen, e.g. sulfones, sulfoxides
    • C10L1/2437—Sulfonic acids; Derivatives thereof, e.g. sulfonamides, sulfosuccinic acid esters
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    • C10L2300/00—Mixture of two or more additives covered by the same group of C10L1/00 - C10L1/308
    • C10L2300/20—Mixture of two components
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    • C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
    • C10M2203/02—Well-defined aliphatic compounds
    • C10M2203/022—Well-defined aliphatic compounds saturated
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    • C10M2203/1045—Aromatic fractions used as base material
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    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
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    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
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    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/34—Fragrance or deodorizing properties
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/60—Electro rheological properties
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/14—Electric or magnetic purposes
    • C10N2040/16—Dielectric; Insulating oil or insulators
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/14—Electric or magnetic purposes
    • C10N2040/17—Electric or magnetic purposes for electric contacts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/25—Internal-combustion engines
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2070/00—Specific manufacturing methods for lubricant compositions

Definitions

  • the field of invention relates to the latest technology in the development of a synthetic gasoline conditioner to clean and lubricate the fuel pump, injectors and valves.
  • the oxygenates dries the fuel creating premature wear between the moving components and in such component as injectors where premature wear can allow excess fuel to discharge causing unburned fuel to be exhausted into the atmosphere.
  • the results are twofold: (1) the environmental effect and (2) the cost to the operators for fuel loss or poor fuel mileage.
  • the invention disclosed herein has been extensively tested experimentally. These test show that it meets is its primary purpose which is to lubricate the fuel system to reduce wear of the mechanical components, which over time will restore injectors' impulse movement required to maintain the greatest fuel efficiencies. The invention will not, however, restore broken components or components that have suffered severe wear.
  • the invention incorporates a strong element of extreme pressure lubrication, octane booster, detergent, dicing agent and cleaner that cleans and restores the valve surface. In-house testing on stationary engines under load have demonstrated increased run time as high as 12% on fuel treated with the invention.
  • a synthetic gasoline conditioner additive with strong lubrication characteristics to reduce premature mechanical wear and failure, increased octane, while cleaning and restoring the valves face to a more efficient operation.
  • This lubricant comprises alpha-olefins; low odor aromatic solvents; and at least one a base oil selected from the base oil group consisting of hydrolsomerized high base oils and HT Severe Hydro-cracked Base Oils; as well as other ingredients.
  • a method for producing this fuel conditioner and lubricant additive is also disclosed.
  • this universal synthetic gasoline conditioner additive for improving lubrication comprises: alpha-olefins comprising from 5 to 30 percent thereof, by weight; low odor aromatic solvents comprising from 3 to 27 percent thereof, by weight; 2-Propanol comprising of 3 to 30 percent thereof, by weight; and at least one a base oil comprising from .50 to 15 percent thereof, by weight; wherein: the percentages by weight are specified in relative proportion to one another.
  • the invention relates to the use of a synthetic gasoline conditioner additive containing a lubricant which that can be added to gasoline fuels stocks to replace the dramatic loss of lubrication generally associated with oxygenated enhanced fuels.
  • the product will have utility in all forms and grades of gasoline, gasoline engines, naturally aspirated or turbo-charged where oxygenated fuels will result in premature wear to the integral components of internal combustion engine.
  • the invention has been submitted by confidential disclosure to the EPA and has received registration under 40CFR 79.23 in October 2007.
  • the finished product (preferred embodiment of the invention) is a combination of:
  • PAO Alpha-Olefins
  • PAO is a primary ingredient also known as Alkenes, Polymerized, Chlorowax Liquids, and Chlorinated Paraffins whose carbon chain length are 12 to 24 with chloric weight percentage from 21.4 to 70%, an HCI of 4 to 10 ppm and molecular weight of 273.5 to 650 and Wt.
  • Cl (2) from 20 to 70% with specific gravity at 25 degrees centigrade of 1.050 to 1.50 and a JQD weight percentage of HCL being 0.20 to 0.60 maximum.
  • the primary use is for the above ingredient is for lubricant formulations, lubricant additive compounds, extreme-pressure additive formulations and for metal working compounds.
  • alpha-olefins or associated products reduce the growth of algae in fuel as aging or excessive moisture accumulates and stabilize the fuel over time while providing extreme lubrication to the fuel system and the firing chamber of the engine. This provides the lubrication lacking in ultra low sulfur diesel.
  • Aromatic Solvents This is a primary ingredient which is a highly-refined, low toxic, low- odor solvent ideal for paints, varnishes, food grade coatings, adhesives, diluents, thinners, agrochemicals, household pesticides, spray oils and specialty chemicals.
  • Aromatic percentage is 5 to 40% (EC-A-G04), a flash point of 20 to 80 degrees centigrade (ASTM D-93) and a density at 30 degrees centigrade (plus/minus) 0.600 to 0.900 (ASTM D- 4052).
  • Hydrolsomerized High-Base Oils or HT Severe Hydro-cracked Base Oils This primary ingredient is a severe hydro-cracked or hydroisomerized base oil with low or no aromatics and impurities achieved by chemically reacting the feed stock with hydrogen to reduce or remove polar compounds containing sulphur, nitrogen and oxygen and to convert aromatic hydrocarbons to saturated cyclic hydrocarbons breaking up the heavy polycyclo-paraffin molecules to light saturated hydrocarbons.
  • This may include fractionated oils that have been hydro-finished or hydro-polished.
  • the base oils can be used in a host of lubricating oils, motor oils, cutting oils, food processing, pharmaceutical, industry, agriculture lubricants and extreme pressure additives. These add to the lubrication of ultra synthetic gasoline conditioner.
  • 2-F 1 TOPaHoI This known as Isopropanol Alcohol (IPA) or industrial alcohol 2-Propanol and is a colorless, flammable chemical compound with a chemical formula of C3 H8 O.
  • the compound has a Molar Mass of 60.10g/mol; density of 0.785 g/cm3, liquid; dipole moment of 1.66D(gas); viscosity of
  • Octane Booster and Detergent Blend In accordance with this invention, this is a blend comprising: hydrocarbon solvents, CAS 64741-86-2; petroleum naphtha, CAS 64742-94-5; polyester amine; and said naphthalene, CAS 91-20-3.
  • 2-Ethylhexyl Nitrate with suggested percentage of 10 to 30% by weight, particularly where calcium sulfonates are restricted, see below. This group of compounds when blended together will clean and maintain the firing chamber of the engine, increase the octane while neutralizing any acids within the fuel system and firing chamber.
  • Synthetic Calcium Sulfonates An over-based synthetic calcium sulfonate with a TBN of 100 to 600 whose primary purpose is for extreme pressure additive formulations offering corrosion protection, dispersants and detergency in oil soluble additives for ferrous and non-ferrous metals with a minimum calcium weight of 10.00 to 20.00%, a total base number, mg KOH/g (ASTM D-2896) of 200 to 600 and an average molecular weight (ASTM d-3712) of 800 to 1200.
  • TBN 100 to 600
  • ASTM D-2896 mg KOH/g
  • ASTM d-3712 average molecular weight
  • Solvent activated dyes These are commonly used to identify grades or designated uses of fuels and lubricants. They are produced in both powder and liquid form and when introduced to the product are stable and leave an identifiable color to the product.
  • Pour Point Depressants or Cloud Point Depressants are used to reduce agglomeration or massing together of wax crystals in paraffin compounds such as lubricants and diesel fuel.
  • Isomer Reformate also referred to as a Solvent, Toluene, Toluol, Methylbenzene and Phenylmethane with a chemical formula of C7H8 (C6H5CH3) and a CAS No. 108-88-3, a molecular weight of 90.00 to 95.00 g/mole and a specific gravity of 0.800 to 0.900 (water being 1).
  • the chemical is an aromatic hydrocarbon that is widely used as an industrial feedstock and as a solvent for cleaning the fuel systems, holding tanks and the combustion chamber of the engine.
  • Dimethyl Ketones Also referred to as Acetone or 2-propanone with molecular structure of CH3COCH3. It is colorless, has low boiling point, and is miscible in proportions with water, alcohols, most hydrocarbons and other organic liquids including diesel fuel stocks to help clean and reduce carbon build up on valves and piston tops.
  • Preferred Blending Ratios Preferred Blending Ratios
  • the preferred blending Ratios for each component are shown as below. It is important to maintain a blend of component that fall within the following percentages. These percentages by weight are specified in relative proportion to one another. Therefore, in the event one or more of the ingredients shown below is omitted from the synthetic gasoline conditioner additive, the percentages by weight of the remaining ingredients are proportionately increased:
  • Alpha-Olefins 5 to 30% by weight and preferably 7.0 to 25% by weight and more preferably 9.0 to 18% by weight. Most preferable is 10.45% by weight.
  • Low Odor Aromatic Solvents 3.0 to 27% by weight and preferably 5.0 to 22% by weight and more preferably is 7.0 to 18% by weight. Most preferable is 7.50 % by weight.
  • Hydrolsomerized High-Base Oils or HT Severe Hydro-cracked Base Oils .50 to 15 percent by weight and preferably 0.75 to 8 % by weight and more preferably 1.0 to 4.0% by weight. Most preferable is 1.52 % by weight.
  • 2-Proponal 5-40% by weight and preferably 7-30% by weight and more preferably 12 to 24% by weight. Most preferable is 18.5%
  • Octane Booster, Detergent and Acid Neutralizer Blend 0.30 to 7.5 % by weight and preferably 0.50 to 5.0 % by weight and more preferably 0.75 to 2.5 % by weight. Most preferable is 1.0 % by weight.
  • Synthetic Calcium Sulfonates 0.05 to 0.25% by weight, preferably 0.07 to 0.20% by weight and more preferably 0.10 to 0.18% by weight. Most preferable is 0.125 % by weight.
  • Low Flash Mineral Spirits 15 to 50% by weight and preferably 20 to 45% by weight and more preferably 25 - 39% by weight. Most preferable is 33.5% by weight.
  • Solvent Activated Dyes 0.002 to 0.005 percent by weight and preferably 0.0025 to 0.004% by weight and more preferably 0.027 to 0.035% by weight. Most preferable is 0.003 percent by weight.
  • Isomer Reformate 0.50 to 15.0% by weight and preferably 1.50 to 10 % by weight and more preferably 2.5 to 7.0 % by weight. Most preferable is 4.0% by weight.
  • Dimethyl Ketones 10 to 50% by weight and preferably 17 to 40% by weight and more preferably 24 to 28% by weight. Most preferable is 23.4%.
  • Preferred Sequence of Blending Components 10 to 50% by weight and preferably 17 to 40% by weight and more preferably 24 to 28% by weight. Most preferable is 23.4%.
  • the initial blend (primary blend) will require the Poly Alpha Olefins, the Low Aromatic Solvent and the Base Oil being blended until the liquid is a consistent amalgamation without any appearance of separation. Blending is based on speed of the agitator and temperature will dictate the amount of time for the blend to complete. The blending time range may vary from 2 to 4 hours. The ideal temperature for each component is between 22 to 30 degrees centigrade for ideal blending. While this is blending, a secondary blend for the Octane Booster, Detergent and Acid Neutralizer, 2-Propanol and said Dimethyl Ketones at 25/75 ratio can be prepared in a smaller high speed enclosed blender, and then added to the main blend.
  • Blend Equipment The Process sequence involves a series of blending and holding tanks where the product can be weighed and then pumped through control valves to maintain consistent flow and pressure.
  • Blending should be performed in a enclosed tank to reduce product evaporation (loss) and prevent exposure to open spark.
  • Blending equipment can be by a combination of high or low speed blending apparatus. Size or volume of tank is not critical to the blend. Universal Use of Invention
  • the engines were run measuring fuel which was both treated and untreated, and the results analyzed.
  • the engines were engines without an OB computer system so accurate reading of fuel consumption was measured.
  • the resulted demonstrated that the treated fuel ran for an average consistently of 12 % longer over the untreated fuel.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Lubricants (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

L'invention concerne un procédé de fabrication d'un additif d'essence synthétique universel qui nettoie le circuit d'alimentation, y compris la surface des soupapes, qui lubrifie la pompe à carburant, les injecteurs et les soupapes, tout en permettant une combustion propre et plus efficace. Une grande partie sera constituée (a) d'alpha-oléfines, (b) de 2-propanol (c) d'huiles de base HT VI hautement hydrolsomérisées, (d) de diméthylcétones, (e) de spiritueux minéraux à détente brusque faible, (f) de solvant aromatique faible, (g) de reformat d'isomère, (h) de colorant activé par solvant. Dans un mode préféré de réalisation, cet additif conditionneur d'essence synthétique universel destiné à améliorer la lubrification comporte : de 5 à 30 pour cent en poids d'alpha-oléfines; de 3 à 27 pour cent en poids de solvants aromatiques à faible odeur; de 3 à 30 pour cent en poids de 2-propanol; et au moins de 0,50 à 15 pour cent en poids d'une huile de base; les pourcentages en poids étant précisés en proportion relative les uns par rapport aux autres.
EP08867084A 2007-12-19 2008-12-18 Additif conditionneur d'essence synthétique universel, procédé et produit en résultant Ceased EP2242821A1 (fr)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
PCT/US2007/088252 WO2009078882A1 (fr) 2007-12-19 2007-12-19 Lubrifiant synthétique universel, procédé et produit obtenu à partir de ce procédé pour remplacer la lubrification au soufre perdu lors de l'utilisation de carburants diesels à faible teneur en soufre
US12/060,637 US8022020B2 (en) 2005-01-18 2008-04-01 Universal synthetic penetrating lubricant, method and product-by-process
PCT/US2008/005095 WO2008130676A1 (fr) 2007-04-20 2008-04-18 Panneaux de construction ayant des revêtements améliorés
PCT/US2008/087433 WO2009085957A1 (fr) 2007-12-19 2008-12-18 Additif conditionneur d'essence synthétique universel, procédé et produit en résultant

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EP2242821A1 true EP2242821A1 (fr) 2010-10-27

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EP08867084A Ceased EP2242821A1 (fr) 2007-12-19 2008-12-18 Additif conditionneur d'essence synthétique universel, procédé et produit en résultant
EP08867519A Ceased EP2245122A1 (fr) 2007-12-19 2008-12-18 Lubrifiant synthétique universel pénétrant, procédé et produit en résultant

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US (2) US8022020B2 (fr)
EP (2) EP2242821A1 (fr)
JP (1) JP2011508022A (fr)
CN (2) CN101952399B (fr)
CA (2) CA2710530C (fr)
WO (2) WO2009085957A1 (fr)

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Publication number Publication date
WO2009085967A1 (fr) 2009-07-09
HK1192900A1 (zh) 2014-09-05
EP2245122A1 (fr) 2010-11-03
US20080182769A1 (en) 2008-07-31
CA2710530C (fr) 2016-07-05
CN103865609A (zh) 2014-06-18
CN101952399A (zh) 2011-01-19
US8071513B2 (en) 2011-12-06
US20100273688A1 (en) 2010-10-28
CN101952399B (zh) 2014-01-01
CN103865609B (zh) 2015-12-30
CA2710403C (fr) 2016-02-02
CA2710403A1 (fr) 2009-07-09
JP2011508022A (ja) 2011-03-10
CA2710530A1 (fr) 2009-07-09
US8022020B2 (en) 2011-09-20
WO2009085957A1 (fr) 2009-07-09
HK1153498A1 (en) 2012-03-30

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