JP2004226205A - Test method for evaluating coat film adhesion performance of spectacle lenses - Google Patents
Test method for evaluating coat film adhesion performance of spectacle lenses Download PDFInfo
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- JP2004226205A JP2004226205A JP2003013612A JP2003013612A JP2004226205A JP 2004226205 A JP2004226205 A JP 2004226205A JP 2003013612 A JP2003013612 A JP 2003013612A JP 2003013612 A JP2003013612 A JP 2003013612A JP 2004226205 A JP2004226205 A JP 2004226205A
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- Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)
Abstract
Description
【0001】
【発明の属する技術分野】
本発明は、眼鏡レンズの評価試験方法及びその条件に関し、特にコート膜密着性能(ハガレ難さ)を評価する評価試験方法及びその条件に関する。
【0002】
【従来の技術】
近年主流となっている合成樹脂製眼鏡レンズは、ガラスレンズに比べて一般的に表面硬度が劣る為、生地よりも硬度の高い合成樹脂材料で表面にコート膜を施している。眼鏡レンズに求められる性能としては、使用者の視力を矯正できる光学的性能は勿論であるが、使用中または保管時の環境に左右されず、長期に渡って当初のコート膜密着性能を保持する耐久品質等が挙げられる。しかしながら合成樹脂製眼鏡レンズの場合、表面(コート膜)に付いた傷からアルカリ性物質,酸性物質,薬品等が浸透し、更に使用中の紫外線,熱等による影響も受け、コート膜ハガレを誘発することがあった。この為、コート膜密着性能は重要な評価項目となっている。
【0003】
眼鏡レンズのコート膜密着性能の評価方法として、JIS規格K5400(塗料一般試験方法)8.5.2「碁盤目テープ法」が一般的に用いられている。碁盤目テープ法は、表面のコート膜にカッター等で碁盤の目状の鋭い傷(コート膜を通過し生地まで達する深い傷)を入れ粘着テープを貼り、剥がした後のコート膜の付着状態を目視によって評価する方法である。
【0004】
また、眼鏡レンズのコート膜の耐候性を評価する方法としては、前記碁盤目テープ法を応用し、傷を入れた眼鏡レンズを耐候性等の加速試験機へ投入し、一定時間毎に取り出して、該碁盤の目状の鋭い傷に粘着テープを貼り付け一気に剥がした後、該碁盤の目状の鋭い傷のハガレ部分の面積大小,形状,ハガレ界面等からコート膜密着性能を評価する方法が用いられている。
【0005】
【発明が解決しようとする課題】
しかしながら、前記方法によって評価を行う場合、コート膜ハガレの状態が、ユーザーの実際の使用に伴うハガレ状態と異なり、再現が出来ないという問題点を有していた。更に、長時間加速試験機へ投入してもなかなかコート膜ハガレに至らず、加速性能が遅いという問題点を有していた。
【0006】
本発明は、上記事情に鑑みなされたもので、眼鏡レンズのコート膜密着性能を評価するに当たって、ユーザーの実際の使用に伴うコート膜ハガレ状態及び繰り返し試験の再現性が高く、且つ加速性能も早く、相対比較を行う場合でも信頼性の高い評価試験方法を提供することを目的とする。
【0007】
【課題を解決するための手段】
本発明者は、上記目的を達成するため鋭意検討を重ねた結果、眼鏡レンズのコート膜密着性能を精度良く評価する方法として、該眼鏡レンズのコート膜上に擦傷物を押し付けながら傷を施す方が、カッターで碁盤の目状の鋭い傷を入れ粘着テープ等の粘着物を貼付け一気に剥がす場合より、評価試験の信頼性に有効であると知見した。
【0008】
すなわち、眼鏡レンズを保持し、該眼鏡レンズのコート膜に対して、表面に粗さを持った擦傷物を接触させた状態で、該擦傷物に荷重をかけて該コート膜上に押し付けながら水平方向の運動をさせて傷(コート膜を通過しない浅い傷、及び通過し生地まで達する深い傷)を入れ耐候性等の加速試験機へ投入し、一定時間毎に取り出して、該傷付け部分のハガレ部分の面積大小,形状,ハガレ界面等を観察することによって、該レンズのコート膜密着性能を評価する。
【0009】
この場合、評価の結果を左右する傷条件として、擦傷物の材質や形状,荷重の量,水平方向の運動ストロークや速度,運動回数,運動時間があるが、これらの傷条件は全て試験装置を用いることにより数値データあるいは明確な値として規定出来る。従って、次回の実験時にはこの傷条件を再現することによって完全に同一条件下で傷入れが可能であり、信頼性や再現性が高い評価が出来る。又、これらの傷条件は任意に変更できる為、想定される使用環境によってその傷条件の組み合わせを変更すれば、使用者の必要とする様々な試験を行う事が出来る。又、試験装置に同一の機構を複数組み込み、同一の運動を行う事で、複数のレンズを同一条件下で一度に傷を入れる、或いは複数の傷条件を同時に入れることも可能である。
【0010】
従って、請求項1記載の発明は、表面にコート膜を有する眼鏡レンズのコート膜密着性能評価試験方法であって、眼鏡レンズを保持し、該眼鏡レンズのコート膜に対して、表面に粗さを持った擦傷物を押し付けながら水平方向の運動をさせて傷を施し、耐候性等の加速試験機へ任意の期間投入した後、該眼鏡レンズのコート膜密着性能を評価することを特徴とする、眼鏡レンズのコート膜密着性能評価試験方法である。
【0011】
請求項2記載の発明は、請求項1に記載の眼鏡レンズのコート膜密着性能評価試験方法において、前記擦傷物の種類を任意に変更して傷を施し、耐候性等の加速試験機へ任意の期間投入した後、該眼鏡レンズのコート膜密着性能を評価することを特徴とする、眼鏡レンズのコート膜密着性能評価試験方法を提供する。
【0012】
請求項3記載の発明は、請求項1または2に記載の眼鏡レンズのコート膜密着性能評価試験方法において、前記擦傷物の水平方向の運動ストローク,回数,押し付ける荷重の量を任意に変更して傷を施し、耐候性等の加速試験機へ任意の期間投入した後、該眼鏡レンズのコート膜密着性能を評価することを特徴とする、眼鏡レンズのコート膜密着性能評価試験方法を提供する。
【0013】
請求項4記載の発明は、請求項1〜3のいずれかに記載の眼鏡レンズのコート膜密着性能評価試験方法において、該加速試験機の種類及び試験条件を任意に変更して投入した後の該眼鏡レンズのコート膜密着性能を評価することを特徴とする、眼鏡レンズのコート膜密着性能評価試験方法を提供する。
【0014】
【発明の実施の形態】
以下、本発明の実施の形態について説明するが、本発明は下記の実施の形態に限定されるものではない。
【0015】
図1に示すように、レンズ1をチャック2で挟み込んで保持する。レンズ1を保持する方法としては他に接着,吸着等が考えられる。レンズ1上には擦傷治具3を垂直方向に設置する。擦傷治具3は、支持部材4によって支持される。支持方法等は任意であるが、水平方向の運動を行った際にレンズ形状に追従できるように可動する構造とする。さらに擦傷治具3の上端には重り5を載せる。この重り5は任意の重さに変更できる物とする。又は、バネ等、他の手段によって荷重を付加しても良い。チャック2は評価試験装置6の往復運動テーブル7上に取り付けられており、さらに往復運動テーブル7はカムなどの手段によって水平方向に往復運動が可能な構造になっている。
【0016】
図1の評価試験装置ではレンズを水平方向に運動させているが、レンズを固定し擦傷治具が運動する構造にしても良い。或いは、レンズと擦傷治具が別の方向に運動することによってさらに複雑な水平方向の運動を得ても良い。
【0017】
往復運動テーブル7は電源スイッチ10の操作によって可動を開始し、その運動スピードは速度調整ボリューム8によって任意に可変できる。又、運動回数をカウンター9によってあらかじめ設定し、その回数に達したところで往復運動を停止するように設定しておけば正確に任意の回数往復運動を行うことも可能である。
【0018】
又、評価試験装置6は往復運動テーブル7上に複数のチャック2、擦傷治具3、支持部材4、重り5を設置し、複数のレンズを同一条件下で一度に傷を施すことも可能である。
【0019】
この状態で擦傷治具3の先端に擦傷物11を固定し、レンズ1に擦傷物11を重り5の荷重によって押し付けつつ往復運動テーブル7を任意の回数往復運動させ、終了後レンズ1の表面に傷を施すことが出来る。擦傷物11の種類は、サンドペーパー、スチールウール、ワイヤーブラシ、プラスチック、布、石、砂、木材等任意であり、それらのメッシュ等の種類も任意である。
【0020】
この評価試験装置を用いると、往復運動の速度,回数を任意に設定出来る。また、往復運動テーブル7を稼動させるカムなどの変更によって、往復運動のストロークの設定も任意に行える。
【0021】
これらの条件で付けられた傷(コート膜を通過しない浅い傷、及び通過し生地まで達する深い傷)のレンズを、耐候性,耐熱性,耐湿性,耐高温多湿性,耐温水性等の加速試験機へ投入し、一定時間毎に取り出して、該傷付け部分のハガレ部分の面積大小,形状,ハガレ界面等を観察することによって、該レンズのコート膜密着性能を評価することが出来る。尚、該耐候性の試験機の種類は、サンシャインウェザメーター、キセノンウェザメーター、フェードメーター、屋外暴露等任意であり、それぞれの試験条件も任意である。
【0022】
又、従来の様に、該傷付け部分に粘着テープを貼り付け一気に剥がした後、ハガレ部分の面積大小,形状,ハガレ界面等からコート膜密着性能を評価する方法を、本発明の該傷付け部分に実施することによって、更に過酷に該レンズのコート膜密着性能を評価することが出来る。
【0023】
【実施例】
図1に示した評価試験装置の擦傷物11としてサンドペーパー(♯1000番)のサンド面側がレンズ1上を擦れる様に擦傷治具3に取り付け、重りとして1kgの分銅を擦傷治具3上に取り付けた。チャック2にレンズ1を固定し、レンズ1上に擦傷物11を置き、その状態で1秒間に1ストローク30mmの速度で往復運動テーブルを水平方向に1回だけ運動させ停止した。その後レンズ1を外し、レンズ表面の傷の状態を観察した。該レンズ表面には1回だけ運動した方向に、コート膜を通過しない浅い傷、及び通過し生地まで達する深い傷が複数付いた。同一素材,同一製造履歴のレンズを複数枚同一条件で試験を行ったところ、試験後のレンズ表面状態はほぼ同じであり、再現性の高い傷付けが行われていた。
【0024】
尚、上記と同等の傷付けを簡易的に行う方法として、台ハカリ等の加重計の上にレンズを置き固定治具又は片手で固定し、両面粘着テープ等でサンドペーパーのサンド面側がレンズ上を擦れる様に固定治具又は指先に固定して、加重計に約1kgの加重を掛けながら、サンドペーパーを約1秒間に1ストローク約30mmの速度で水平方向に1回だけ擦り、傷付けをする。その後レンズを外し、レンズ表面の傷の状態を観察した所、上記とほぼ同等のコート膜を通過しない浅い傷、及び通過し生地まで達する深い傷が複数付いた。
【0025】
該傷付けレンズを、加速試験機のサンシャインウェザメーターへ投入し、一定の20時間毎に取り出して、該傷付け部分のハガレ部分の面積大小,形状,ハガレ界面等を観察した所、ユーザーの実際の使用に伴うハガレに近い状態を、従来方法(約200時間)より約半分短い時間(約100時間)で再現することが出来た。
【0026】
又、繰り返し同一試験を行った所、再現性が極めて高く、且つ加速性能も早く(加速試験機への投入時間が、従来方法より短時間で済み)、更には相対比較を行う場合でも信頼性の高い評価試験を行うことが出来た。
【0027】
【発明の効果】
以上述べた様に、本発明の評価試験方法およびその装置によれば、眼鏡レンズのコート膜密着性能を、実際の使用状況に近い環境下で高い精度で評価可能である。又、付加する荷重の大きさや、擦傷物の形状や材質、レンズと擦傷物の水生方向の運動速度や方向,回数,ストロークといったパラメータを任意で設定出来る為、より傷付け方法の自由度が大きく、且つ信頼性の高いコート膜密着性能評価を得ることが可能である。更に、傷付け方法として、複数の機構を1台に設置することによって、同一条件下で複数のレンズを同時に傷付けする、或いは複数の傷付け条件を同時に実施することが可能である為、コート膜密着性能評価試験の時間を大幅に短縮出来る。
【図面の簡単な説明】
【図1】本発明の第1実施形態における、往復運動テーブルに保持した眼鏡レンズ上に垂直方向に擦傷治具を設置し、その上端に重りを載せ、さらに往復運動テーブルが水平方向に稼動するようにした装置構成を説明する概念図である。
【符号の説明】
1 眼鏡レンズ
2 チャック
3 擦傷治具
4 支持部材
5 重り
6 評価試験装置
7 往復運動テーブル
8 速度調整ボリューム
9 カウンター
10 電源スイッチ
11 擦傷物[0001]
TECHNICAL FIELD OF THE INVENTION
The present invention relates to an eyeglass lens evaluation test method and its conditions, and more particularly to an evaluation test method for evaluating coat film adhesion performance (hard peeling) and its conditions.
[0002]
[Prior art]
Synthetic resin spectacle lenses, which have become mainstream in recent years, are generally inferior in surface hardness as compared with glass lenses, and thus are coated on the surface with a synthetic resin material having a higher hardness than fabric. The performance required for the spectacle lens is, of course, the optical performance that can correct the user's visual acuity, but is not affected by the environment during use or storage, and maintains the original coat film adhesion performance for a long time. Durability quality and the like. However, in the case of synthetic resin spectacle lenses, alkaline substances, acidic substances, chemicals, and the like penetrate from scratches on the surface (coat film), and are further affected by ultraviolet rays, heat, and the like during use, causing coat film peeling. There was something. For this reason, the coat film adhesion performance is an important evaluation item.
[0003]
As a method for evaluating the coat film adhesion performance of spectacle lenses, JIS K5400 (paint general test method) 8.5.2 “cross-cut tape method” is generally used. The crosscut tape method uses a cutter or the like to make sharp cuts in a grid pattern (deep scratches that pass through the coat film and reach the fabric) on the surface coat film, apply an adhesive tape, and check the adhesion state of the coat film after peeling. This is a method of visually evaluating.
[0004]
In addition, as a method of evaluating the weather resistance of the coat film of the spectacle lens, the cross-cut tape method is applied, and the spectacle lens with the scratch is put into an acceleration tester such as a weather resistance, and taken out at regular intervals. A method of applying an adhesive tape to the sharp scratches on the grid and peeling it off at a stretch, and then evaluating the coat film adhesion performance from the size, shape, interface, etc. of the stripped portion of the sharp scratches on the grid. Used.
[0005]
[Problems to be solved by the invention]
However, when the evaluation is performed by the above method, there is a problem that the state of the coating film peeling cannot be reproduced unlike the peeling state accompanying the actual use of the user. Furthermore, even if the film was put into an acceleration test machine for a long time, the coating film was not easily peeled, and the acceleration performance was slow.
[0006]
The present invention has been made in view of the above circumstances, and in evaluating the coat film adhesion performance of spectacle lenses, the coat film peeling state associated with the actual use of the user and the reproducibility of the repeated test are high, and the acceleration performance is also fast. Another object of the present invention is to provide a highly reliable evaluation test method even when performing a relative comparison.
[0007]
[Means for Solving the Problems]
The present inventors have conducted intensive studies to achieve the above object, and as a method of accurately evaluating the coat film adhesion performance of the spectacle lens, a method of applying a scratch while pressing an abrasion object on the coat film of the spectacle lens However, it was found that it was more effective for the reliability of the evaluation test than a case where sharp cuts like a grid were cut with a cutter and an adhesive such as an adhesive tape was attached and peeled off at a stretch.
[0008]
That is, while holding the spectacle lens, and in a state where an abraded object having a rough surface is brought into contact with the coat film of the spectacle lens, a load is applied to the abraded object and pressed horizontally onto the coat film while pressing the abraded object. Move it in the direction to make scratches (shallow scratches that do not pass through the coat film and deep scratches that pass and reach the fabric), put them into an accelerated testing machine for weather resistance, etc., and take them out at regular intervals, and remove By observing the area size, shape, peeling interface, etc. of the portion, the coating film adhesion performance of the lens is evaluated.
[0009]
In this case, the scratch conditions that affect the evaluation result include the material and shape of the abrasion object, the amount of load, the horizontal stroke and speed of movement, the number of times of movement, and the duration of the movement. By using it, it can be defined as numerical data or a clear value. Therefore, in the next experiment, it is possible to make a flaw under completely the same conditions by reproducing these flaw conditions, and high reliability and reproducibility can be evaluated. Further, since these flaw conditions can be arbitrarily changed, various tests required by the user can be performed by changing the combination of the flaw conditions according to the assumed use environment. In addition, by incorporating a plurality of the same mechanisms into the test apparatus and performing the same movement, it is possible to simultaneously scratch a plurality of lenses under the same conditions, or to simultaneously apply a plurality of scratch conditions.
[0010]
Therefore, the invention according to claim 1 is a method for evaluating the coat film adhesion performance of a spectacle lens having a coat film on the surface, wherein the spectacle lens is held, and the surface of the spectacle lens has a roughness on the coat film. It is characterized by performing a horizontal motion while pressing an abrasion object having a scratch to apply a scratch to the tester for an arbitrary period of time such as weather resistance, and then evaluating the coat film adhesion performance of the spectacle lens. This is a test method for evaluating coat film adhesion performance of spectacle lenses.
[0011]
According to a second aspect of the present invention, in the method for evaluating a coat film adhesion performance of a spectacle lens according to the first aspect, the kind of the abrasion object is arbitrarily changed to apply a flaw, and an arbitrary tester is applied to an accelerated testing machine for weather resistance and the like. The present invention provides an eyeglass lens coat film adhesion performance evaluation test method, which comprises evaluating the coat film adhesion performance of the spectacle lens after charging for a period of time.
[0012]
According to a third aspect of the present invention, in the method for evaluating the coat film adhesion performance of an eyeglass lens according to the first or second aspect, the horizontal movement stroke of the abrasion object, the number of times, and the amount of pressing load are arbitrarily changed. The present invention provides a method for evaluating the coat film adhesion performance of spectacle lenses, which is characterized by evaluating the coat film adhesion performance of the spectacle lens after being scratched and charged into an accelerated testing machine for weather resistance or the like for an arbitrary period.
[0013]
According to a fourth aspect of the present invention, in the test method for evaluating the coat film adhesion performance of an eyeglass lens according to any one of the first to third aspects, the type and the test conditions of the acceleration tester are arbitrarily changed and then input. Provided is a method for evaluating the coat film adhesion performance of a spectacle lens, which comprises evaluating the coat film adhesion performance of the spectacle lens.
[0014]
BEST MODE FOR CARRYING OUT THE INVENTION
Hereinafter, embodiments of the present invention will be described, but the present invention is not limited to the following embodiments.
[0015]
As shown in FIG. 1, a lens 1 is sandwiched and held by a
[0016]
In the evaluation test apparatus of FIG. 1, the lens is moved in the horizontal direction. However, a structure in which the lens is fixed and the abrasion jig moves may be used. Alternatively, a more complicated horizontal movement may be obtained by moving the lens and the abrasion jig in different directions.
[0017]
The reciprocating motion table 7 starts moving by operating the power switch 10, and the speed of the motion can be arbitrarily changed by the speed adjusting volume 8. Also, if the number of exercises is set in advance by the counter 9 and the reciprocation is stopped when the number of exercises is reached, it is possible to perform the reciprocation exactly an arbitrary number of times.
[0018]
In addition, the
[0019]
In this state, the
[0020]
Using this evaluation test device, the speed and number of reciprocating movements can be set arbitrarily. Further, the stroke of the reciprocating motion can be arbitrarily set by changing a cam or the like for operating the reciprocating motion table 7.
[0021]
Acceleration of lenses with scratches (shallow scratches that do not pass through the coating film and deep scratches that reach the fabric through the coating film) under these conditions, such as weather resistance, heat resistance, moisture resistance, high temperature and humidity resistance, hot water resistance, etc. The lens is taken out at regular intervals and taken out at regular intervals, and by observing the size, shape, interface, etc. of the frayed portion of the flaw, the coating film adhesion performance of the lens can be evaluated. The type of the weather resistance tester is arbitrary such as a sunshine weather meter, a xenon weather meter, a fade meter, and outdoor exposure, and each test condition is also arbitrary.
[0022]
Further, as in the prior art, after affixing the adhesive tape to the damaged portion and peeling it off at a stretch, a method of evaluating the coat film adhesion performance from the area size, shape, peeling interface, etc. of the peeled portion is applied to the wounded portion of the present invention. By carrying out, it is possible to more severely evaluate the coating film adhesion performance of the lens.
[0023]
【Example】
As an
[0024]
In addition, as a simple method of performing the same scratching as above, place the lens on a weight meter such as a base weighing fixture and fix it with a fixing jig or one hand, and the sand side of the sandpaper with double-sided adhesive tape etc. The sandpaper is rubbed only once in a horizontal direction at a speed of about 30 mm per stroke for about one second while a weight of about 1 kg is applied to the weight meter while being fixed to a fixing jig or a fingertip so as to be rubbed. Thereafter, the lens was removed, and the state of the scratch on the lens surface was observed. As a result, there were a plurality of shallow scratches that did not pass through the coat film, and a plurality of deep scratches that did pass through to the fabric.
[0025]
The scratched lens was put into a sunshine weather meter of an acceleration tester, taken out every 20 hours, and observed for the size, shape, interface, etc. of the peeled part of the damaged part. A state close to peeling accompanying the above was able to be reproduced in about half shorter time (about 100 hours) than the conventional method (about 200 hours).
[0026]
In addition, when the same test is repeatedly performed, the reproducibility is extremely high and the acceleration performance is fast (the time for inputting to the acceleration test machine is shorter than the conventional method), and even when performing a relative comparison, the reliability is improved. A high evaluation test was performed.
[0027]
【The invention's effect】
As described above, according to the evaluation test method and the apparatus of the present invention, the coat film adhesion performance of the spectacle lens can be evaluated with high accuracy under an environment close to the actual use situation. In addition, since parameters such as the magnitude of the load to be applied, the shape and material of the abrasion object, the speed and direction of the aquatic movement of the lens and the abrasion object, the number of times, and the stroke can be arbitrarily set, the degree of freedom in the method of scratching is greater. In addition, it is possible to obtain a highly reliable coating film adhesion performance evaluation. Further, as a method of scratching, by installing a plurality of mechanisms on one unit, a plurality of lenses can be scratched simultaneously under the same condition, or a plurality of scratching conditions can be simultaneously performed. Evaluation test time can be significantly reduced.
[Brief description of the drawings]
FIG. 1 shows a first embodiment of the present invention, in which a scuffing jig is set vertically on a spectacle lens held on a reciprocating table, a weight is placed on the upper end thereof, and the reciprocating table is operated in a horizontal direction. FIG. 2 is a conceptual diagram illustrating the configuration of the apparatus as described above.
[Explanation of symbols]
DESCRIPTION OF SYMBOLS 1
Claims (4)
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| Application Number | Priority Date | Filing Date | Title |
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| JP2003013612A JP4013769B2 (en) | 2003-01-22 | 2003-01-22 | Test method for coating film adhesion performance evaluation of spectacle lenses |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2003013612A JP4013769B2 (en) | 2003-01-22 | 2003-01-22 | Test method for coating film adhesion performance evaluation of spectacle lenses |
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| JP2004226205A true JP2004226205A (en) | 2004-08-12 |
| JP4013769B2 JP4013769B2 (en) | 2007-11-28 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008096300A (en) * | 2006-10-12 | 2008-04-24 | Hoya Corp | Test condition determination method of adhesive capacity to titanium type hard coat lens base material, and testing method |
| JP2012032241A (en) * | 2010-07-29 | 2012-02-16 | Hoya Corp | Method for evaluating film adhesion |
| CN104807750A (en) * | 2015-04-23 | 2015-07-29 | 中国石油大学(华东) | Testing method of microscale tension of two self-polymeric proppant particles |
| CN106404663A (en) * | 2016-06-06 | 2017-02-15 | 苏州华源包装股份有限公司 | Coating and scrubbing tester |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103900956A (en) * | 2014-04-22 | 2014-07-02 | 成都彩星科技实业有限公司 | Paint film adhesion test device |
-
2003
- 2003-01-22 JP JP2003013612A patent/JP4013769B2/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008096300A (en) * | 2006-10-12 | 2008-04-24 | Hoya Corp | Test condition determination method of adhesive capacity to titanium type hard coat lens base material, and testing method |
| JP2012032241A (en) * | 2010-07-29 | 2012-02-16 | Hoya Corp | Method for evaluating film adhesion |
| CN104807750A (en) * | 2015-04-23 | 2015-07-29 | 中国石油大学(华东) | Testing method of microscale tension of two self-polymeric proppant particles |
| CN104807750B (en) * | 2015-04-23 | 2017-08-11 | 中国石油大学(华东) | The method of testing of micro pulling force between a kind of two autohemagglutination proppant particulates |
| CN106404663A (en) * | 2016-06-06 | 2017-02-15 | 苏州华源包装股份有限公司 | Coating and scrubbing tester |
Also Published As
| Publication number | Publication date |
|---|---|
| JP4013769B2 (en) | 2007-11-28 |
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