JPS5450088A - Purification of liquid polybutadiene - Google Patents
Purification of liquid polybutadieneInfo
- Publication number
- JPS5450088A JPS5450088A JP11609477A JP11609477A JPS5450088A JP S5450088 A JPS5450088 A JP S5450088A JP 11609477 A JP11609477 A JP 11609477A JP 11609477 A JP11609477 A JP 11609477A JP S5450088 A JPS5450088 A JP S5450088A
- Authority
- JP
- Japan
- Prior art keywords
- liquid polybutadiene
- polybutadiene
- hypochlorite
- methanol
- compound
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
Abstract
PURPOSE: To prepare colorless liquid polybutadiene by treating a polymerization reaction mixture containing liquid polybutadiene successively with NaOH, a hypochlorite, and methanol.
CONSTITUTION: A polymerization reaction mixture containing a liquid polybutadiene having a viscosity of 100W10,000 cp (at 30°C) obtained by the polymerization of 1,3-butadiene in a thdrocarbon solvent in the presence of a catalyst prepared from a halogen-containing organic aluminum compound, a soluble Co compound, and an organo-phosphorus compound, is mixed with an aqueous solution of sodium hydroxide or potassium hydroxide, and the water layer is separated and removed. The oil layer containing the polymer is made to contact with an aqueous solution of a hypochlorite or hydrogen peroxide, and the water layer is removed. The oil layer containing the polymer is distilled to remove the dydrocarbon solvent, and the remaining liquid polybutadiene is washed with methanol to obtain purified polybutadiene
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11609477A JPS5450088A (en) | 1977-09-29 | 1977-09-29 | Purification of liquid polybutadiene |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11609477A JPS5450088A (en) | 1977-09-29 | 1977-09-29 | Purification of liquid polybutadiene |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5450088A true JPS5450088A (en) | 1979-04-19 |
| JPS6138203B2 JPS6138203B2 (en) | 1986-08-28 |
Family
ID=14678548
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP11609477A Granted JPS5450088A (en) | 1977-09-29 | 1977-09-29 | Purification of liquid polybutadiene |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5450088A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2007135946A1 (en) * | 2006-05-22 | 2007-11-29 | Ube Industries, Ltd. | Method for producing polybutadiene |
| WO2019159752A1 (en) * | 2018-02-14 | 2019-08-22 | 日本ゼオン株式会社 | Waste water reutilization method |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6422503U (en) * | 1987-07-31 | 1989-02-06 |
-
1977
- 1977-09-29 JP JP11609477A patent/JPS5450088A/en active Granted
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2007135946A1 (en) * | 2006-05-22 | 2007-11-29 | Ube Industries, Ltd. | Method for producing polybutadiene |
| US7868103B2 (en) | 2006-05-22 | 2011-01-11 | Ube Industries, Ltd. | Method for producing polybutadiene |
| WO2019159752A1 (en) * | 2018-02-14 | 2019-08-22 | 日本ゼオン株式会社 | Waste water reutilization method |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6138203B2 (en) | 1986-08-28 |
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