JPS57166311A - Production of x-type zeolite - Google Patents
Production of x-type zeoliteInfo
- Publication number
- JPS57166311A JPS57166311A JP4839581A JP4839581A JPS57166311A JP S57166311 A JPS57166311 A JP S57166311A JP 4839581 A JP4839581 A JP 4839581A JP 4839581 A JP4839581 A JP 4839581A JP S57166311 A JPS57166311 A JP S57166311A
- Authority
- JP
- Japan
- Prior art keywords
- aqueous sodium
- type zeolite
- sodium silicate
- sodium aluminate
- equation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 title abstract 5
- 229910021536 Zeolite Inorganic materials 0.000 title abstract 3
- 239000010457 zeolite Substances 0.000 title abstract 3
- 239000004115 Sodium Silicate Substances 0.000 abstract 3
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 abstract 3
- 229910001388 sodium aluminate Inorganic materials 0.000 abstract 3
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 abstract 3
- 229910052911 sodium silicate Inorganic materials 0.000 abstract 3
- 229910000323 aluminium silicate Inorganic materials 0.000 abstract 2
- 238000002425 crystallisation Methods 0.000 abstract 2
- 230000008025 crystallization Effects 0.000 abstract 2
- 230000000694 effects Effects 0.000 abstract 2
- 230000032683 aging Effects 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 238000001879 gelation Methods 0.000 abstract 1
- 230000003068 static effect Effects 0.000 abstract 1
Landscapes
- Silicates, Zeolites, And Molecular Sieves (AREA)
Abstract
PURPOSE: The reaction between aqueous sodium silicate and aqueous sodium aluminate is continuously carried out without back-mixing to form aluminosilicate gel and the compound is crystallized, thus producing pure X-type zeolite.
CONSTITUTION: Aqueous sodium silicate and aqueous sodium aluminate are simultaneously fed into a tubular static mixer to effect their continuous reaction without back mixing. The residence time in second, given by the equation, is set at less than 10 seconds. In the equation, a and b are the feed rates of aqueous sodium silicate and sodium aluminate in l/sec respectively and V is the capacity of the mixer in liter. The resulant aluminosilicate gel is aged to effect crystallization, thus producing X-type zeolite. Seeds are added at one of three stage: gelation, gel aging or crystallization.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP4839581A JPS57166311A (en) | 1981-04-02 | 1981-04-02 | Production of x-type zeolite |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP4839581A JPS57166311A (en) | 1981-04-02 | 1981-04-02 | Production of x-type zeolite |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS57166311A true JPS57166311A (en) | 1982-10-13 |
| JPS6245168B2 JPS6245168B2 (en) | 1987-09-25 |
Family
ID=12802103
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP4839581A Granted JPS57166311A (en) | 1981-04-02 | 1981-04-02 | Production of x-type zeolite |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS57166311A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4661334A (en) * | 1983-09-21 | 1987-04-28 | Rhone-Poulenc Chimie De Base | Preparation of zeolites 4A and/or 13X |
| US7528201B2 (en) | 2004-12-22 | 2009-05-05 | Exxonmobil Chemical Patents Inc. | Synthesis of silicoaluminophosphate molecular sieves |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62114771U (en) * | 1986-01-10 | 1987-07-21 |
-
1981
- 1981-04-02 JP JP4839581A patent/JPS57166311A/en active Granted
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4661334A (en) * | 1983-09-21 | 1987-04-28 | Rhone-Poulenc Chimie De Base | Preparation of zeolites 4A and/or 13X |
| US7528201B2 (en) | 2004-12-22 | 2009-05-05 | Exxonmobil Chemical Patents Inc. | Synthesis of silicoaluminophosphate molecular sieves |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6245168B2 (en) | 1987-09-25 |
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