KR830002005B1 - Yulmu beverage manufacturing method - Google Patents
Yulmu beverage manufacturing method Download PDFInfo
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- KR830002005B1 KR830002005B1 KR1019820003687A KR820003687A KR830002005B1 KR 830002005 B1 KR830002005 B1 KR 830002005B1 KR 1019820003687 A KR1019820003687 A KR 1019820003687A KR 820003687 A KR820003687 A KR 820003687A KR 830002005 B1 KR830002005 B1 KR 830002005B1
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- 238000000034 method Methods 0.000 claims description 7
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Abstract
내용 없음.No content.
Description
율무(仁 : Coixma-yuen Roman)는 벼과의 1년생 초본과 식물로서 우리나라 전국 각지에서 재배가 가능하며 특히 천수답, 간척지, 유휴지에서 재배하면 종가에서 상당한 수익을 올릴 수 있는 것이다.Yulmu ( 仁: Coixma-yuen Roman) is a year-old herbaceous herbaceous plant that can be cultivated in all parts of Korea.
율무 쌀의 성분은 대략 단백질 21%, 지질 7%, 탄수화물 50% 이상을 함유하는 영양 곡물이며 그 함유성분 약효로서는 고래로부터 치질, 백태하, 발진, 관절통 등에 쓰이고 왔으며, 또한 항암성분인 코이크세노리드(Coixennolide)가 함유되어 방암, 치암효과도 지니고 있는 생약 식물로도 취급되어 왔다.Yulmu Rice is a nutritious grain containing approximately 21% protein, 7% lipid, and 50% carbohydrate. Its ingredients have been used by whales for hemorrhoids, white fetuses, rashes, joint pain, etc. It has been treated as a herbaceous plant that contains lead (Coixennolide) and also has cancer and haemorrhage effects.
이러한 율무는 현재 율무쌀로서 밥을 지어 먹든가, 가루를 가공하여 분말음료 형태로 식용되고 있으나 기호상, 식용상 여러가지 불편한 점이 많기 때문에 널리 사용되지 못하고 있는 실정이다.Such yulmu is currently used as a yulmu rice to make rice or processed powder to be edible in the form of powdered beverage, but it is not widely used because of many inconveniences in terms of taste and food.
본 발명은 이러한 식용상 좋지 않은 상태의 율무를 기호상 좋고 대중적으로 상용할 수 있는 상태의 음료로 만들 필요성이 절실함에 있어서 율무의 약용성분의 열수 추출과 아울러 그 본래의 청량한 향미를 향상시킬 수 있는 율무 음료 원액의 제조방법에 관한 것이다.According to the present invention, the necessity of making such a badly edible juice in a taste good and popularly available is urgently needed, as well as the hot water extraction of the medicinal ingredients of the yulmu can improve its original refreshing flavor. The present invention relates to a method for preparing a raw beverage beverage.
이를 구체적으로 상술하면 다음과 같다.This will be described in detail below.
먼저 율무 종실의 외피를 탈피하고 이것을 일반 곡물의 도정공정에 따라 내피를 벗겨서 율무쌀을 만든다.First, peel the outer shell of Yulmu seeds and peel the inner skin according to the general grain milling process to make Yulmu rice.
이 율무쌀을 수회 수세한 후 20∼30분간 탕자(湯煮)하여 연화시키거나 또는 율무쌀을 그대로 2∼3시간 동안 수침하여 충분히 팽윤시킨 것을 일정량의 물을 가하면서 100∼150멧슈(mesh)의 콜로이드 밀(colloid mill)로 마쇄하여 율무쌀의 마쇄슬러리(slurry)를 얻는다. 이 마쇄 슬러리의 분산 고형물은 전분 입자와 마쇄된 단백질, 지방, 섬유질 등의 복함체의 불용성 고형물들이고 그 고형물 함량이 5∼10중량 %정도가 되도록 가수 마쇄하여 농도를 조절한다. 이 율무의 슬러리는 효소반응 탱크(압력관)에 주입하여 액화 효소로서 전분질의 액화, 즉 호정화(Dextrine化) 반응을 시킨다. 이때 사용되는 액화 효소로서는 일반사상균(系狀菌)배양에서 추출 분리한 α-아미라아제는 보통 50℃전후에서 활성이 가장 크며 70℃에 이르면 활성이 급격히 감소되는 등액화에 장시간 소요하게 된다. 반응을 단시간에 끝나도록 하되, 제품의 신선미를 유지하기 위하여는 고온반응이 필요하며 따라서 효소의 내열성을 증가시키기 위하여 pH조정 CaCl2NaCl 등과 같은 염류를 첨가할 필요가 있된다. 그러나 현재 구미의 식품공업계에 많이 사용되는 세균성 α-아미라아제로서 터아밀(Termamyl 상품명), 옵티텀(optitherm-L 상품명) 등은 강력한 효소활성을 나타낼 분만이 아니라 내열성이 강하여 특히 본 발명에 있어서 율무의 향미와 청량미 등의 신선미를 보존하면서 전분질의 액화에 매우 효과적인 것이라 할 수 있다. 즉 효소의 활성 내열성이 약하면 저온에서 장시간의 반응이 필요하게 됨으로 그간 율무 고유의 향미와 청량미가 저하 소실되어 제품의 청량음료 원액으로서 상품적 가치를 매우 저하시키는 원인이 될 수 있는 것이다.After washing this Yulmu rice several times, it is bathed in water for 20 to 30 minutes and softened, or it is soaked for 2 to 3 hours as it is, and swelled sufficiently to add 100 ~ 150 mesh colloid while adding a certain amount of water. Grinding with a colloid mill to obtain a grinding slurry of yulmu rice. The dispersed solids of the ground slurry are insoluble solids of complexes such as starch particles and ground proteins, fats and fibers, and are hydrolyzed to adjust the concentration so that the solids content is about 5 to 10% by weight. The slurry of this yulmu is injected into an enzyme reaction tank (pressure tube) to liquefy the starch as a liquefied enzyme, that is, a dextrinization reaction. At this time, as the liquefied enzyme used, α-amylase extracted and separated from general filamentous fungi cultures usually has the greatest activity around 50 ° C, and it takes a long time to equalize liquefaction when the activity rapidly decreases to 70 ° C. The reaction is to be completed in a short time, but in order to maintain the freshness of the product, a high temperature reaction is required, and therefore, salts such as pH-adjusted CaCl 2 NaCl, etc. need to be added to increase the heat resistance of the enzyme. However, as a bacterial α-amylase that is widely used in the food industry of Gumi, Teramyl (Optamyl trade name), Optitum (L-Optitherm-L trade name), etc. exhibit not only strong enzyme activity but also heat resistance, especially in the present invention. It can be said that it is very effective for liquefaction of starch while preserving fresh flavors such as flavor and refreshing taste. That is, if the active heat resistance of the enzyme is low, it requires a long time reaction at a low temperature, and thus the flavor and intrinsic taste of Yulmu may be lowered and lost, which may cause a very low commercial value as a soft drink stock of the product.
본 발명의 음료 원액의 제조 조건으로서는 터마밀의 세균성 α-아미나아제로서 율무의 전분질량에 대하여 0.05∼0.1 중량 %, 반응온도 95℃ 전후, 반응시간 10∼30분간일 때 가장 좋은 제품을 얻을 수 있다고 할 수 있다.As a preparation condition of the beverage stock solution of the present invention, the best product can be obtained when the bacterial α-aminase of teramyl is 0.05 to 0.1% by weight based on the starch mass of yulmu, the reaction temperature is about 95 ° C, and the reaction time is 10 to 30 minutes. can do.
즉, 율무 스러리 또는 호화액과 세균성 α-아미라아제의 혼액을 효소반응의 균일성을 도모하기 위하여 효소반응 탱크에 주입시킬 때 분무식으로 탱크의 수개소에서 펌프로서 분산 주입시키며 또 교반효과를 높이기 위하여 탱크의 중심회전축에 2개의 날개로서 100RPM전후로 교반하면서 95℃의 온도에서 만탱크가 될 때까지 약 20분 정도 소요되는 속도로서 주입을 완료하게 되는 것이다.In other words, when a mixture of Yulmu slurry or gelatinous liquid and bacterial α-amylase is injected into the enzyme reaction tank in order to achieve uniformity of the enzyme reaction, it is sprayed and injected as a pump at several places of the tank by spraying, and the stirring effect is improved. In order to increase the speed, it takes about 20 minutes to reach the tank at the temperature of 95 ° C while stirring around 100RPM with two blades on the center axis of rotation of the tank.
95℃의 액온을 탱크를 밀폐하여 105℃로 가압 승온하여 5∼7분간 전분의 미셀의 개열을 도모하고 배기냉각시켜 다시 95℃로 환원하여 10∼30분 반응을 지속시킨다. 효소의 첨가는 일차로 율무 스러리에 전 소요량의 0.7 중량 %를 혼합하여 반응시키고 이차로 95℃로 환원하였을 때 나머지 0.3 중량 %를 첨가 반응시킨다. 반응의 정도는 옥소 반응시험으로 적갈색 또는 담적색을 나타낼 때까지이며 D.E. 환원당의 양/고형물포중 전분질의 양)로서 15∼20 정도에서 끝이게 된다.The liquid temperature of 95 degreeC is sealed, pressurized and heated up at 105 degreeC, the cleavage of the starch micelle is aimed for 5 to 7 minutes, exhaust-cooled, it is reduced to 95 degreeC, and reaction is continued for 10 to 30 minutes. The enzyme is first reacted by mixing 0.7 wt% of the total amount required in Yulmu slurry and secondly by adding the remaining 0.3 wt% when reducing to 95 ° C. The extent of the reaction was determined by the oxo test until it was reddish brown or light red. Amount of reducing sugar / amount of starch in solid blister).
이 단계의 반응 기구로서 α-아미라아제 효소는 전분질의 아미로우스에 작용하여 α-1,4 결합을 가수 분해함으로서 포도당 6∼8개로 구성된 말토 덱스트린(malto Dextrine)이 70∼80%이 되며 율무스러리는 맑은 용액으로 변하고 용액의 점도는 매우 저하되어 불용성 단백질, 지질, 섬유질의 복합체의 고형물과의 분리현상이 뚜렷하게 나타나게 된다.As a reaction mechanism at this stage, the α-amylase enzyme acts on the starch amylose to hydrolyze α-1,4 bonds, resulting in 70 to 80% malto dextrin composed of 6-8 glucose. The slurry changes to a clear solution and the viscosity of the solution is very low, resulting in a clear separation of solids from insoluble protein, lipid, and fiber complexes.
효소 반응이 끝나면 효소의 실활조작과 율무 성분의 열수추출물을 더욱 촉진키위하여 가압 승온하여 120∼140℃에서 10∼15분간 유지시킨 다음 배기 냉각하여 60∼70℃의 액온으로 만든다.After the enzymatic reaction, the enzyme was inactivated and the hot-water extract of Yulmu was further heated to pressurized temperature and maintained at 120-140 ° C for 10-15 minutes, and then cooled by exhaust to 60-70 ° C.
이때 율무 효소 반응원액의 한약초의 향기와 청량미를 향상시키기 위하여서는 효소의 실활 조작에 들어가기 전에 정선된 한약초 향신로 분말을 일정량 첨가하여 반응시켜 율무 원액에 추출되도록 한다. 향신료 분말로서는 일반적인 계피분말, 생강분말, 또는, 감초, 당귀분말 등으로 다이어트 음료, 영양음료 제조 원액으로 할 것이며, 스포츠 드링크로서는 미네랄로 인한 염미(味)의 마스킹 및 청량감을 부여하는 진피, 레몬 등을 사용할 것이다.At this time, in order to improve the fragrance and refreshing taste of herbal medicine of Yulmu enzyme reaction stock solution, a certain amount of powder was added to the selected herbal medicine fragrance before entering the deactivation operation of the enzyme to react and extract to Yulmu stock solution. As a spice powder, general cinnamon powder, ginger powder, licorice, and Angelica powder, etc., will be used as dietary drinks and nutritional beverages. I) Skin and lemon will be used to give masking and refreshing feeling.
즉, 율무 효소 반응 원액을 여과하였을 때 여액 속에는 향신료 향미액기스분이 추출되어 나오고 분말케이크 속에 혼재되어 있는 향신료 분말은 그 분말 음료의 향미를 더욱 높이게 된다.In other words, when the Yulmu enzyme-reaction stock solution is filtered, the spice flavor extract powder is extracted from the filtrate, and the spice powder mixed in the powder cake further enhances the flavor of the powder beverage.
이와 같이 본 발명에서 세균성 α-아미라아제로서 율무의 전분질을 호정화시켜 음료원액의 점성을 저지시킴과 동시에 고온 가압 반응으로 율무 성분 중의 단백질의 연화 및 일부 가용화와 무기질 및 특수성분의 열수 추출을 도모하게 되어 음료의 의약적, 영양적 성분 가치를 높이게 되고 율무 고유의 한약제적인 향기와 청량미를 더욱 향상시킬 수 있으며 불용성 성분과 쉽게 분리할 수 있는 율무음료 원액을 얻게 되는 것이다.As described above, in the present invention, as a bacterial α-amylase, the starch of yulmu is stabilized to prevent the viscosity of the beverage stock solution, and at the same time, the softening and partial solubilization of proteins in the yulmu component and hot water extraction of minerals and special components are carried out by high temperature pressurization. This will increase the value of the medicinal and nutritional ingredients of the beverage, and further improve the unique herbal medicinal aroma and refreshing taste of Yulmu and obtain the Yulmu Beverage, which can be easily separated from insoluble ingredients.
효소 반응이 끝나고 실활 조작을 마친 율무원액은 여과하여 투명한 율무 추출 액체원액과 불용성 고형물 케이크로 분리하게 된다.After completion of the enzyme reaction and deactivation, the Yulmu solution was filtered and separated into a transparent Yulmu extract liquid solution and an insoluble solid cake.
여기서 얻어지는 액체 원액은 청정 후 스포츠 드링크, 다이어트 음료, 영양 음료 또는 탄산청량음료 등으로 조제하여 여러가지 건강음료의 원액으로 사용된다.The liquid stock solution obtained here is prepared as a sports drink, a diet drink, a nutritional drink or a carbonated soft drink after cleansing, and is used as a stock solution of various healthy drinks.
탄산음료에 있어서는 탄산가스 주입시는 4∼5℃에서 병내 압력 0.4∼1.5kg/cm2가량의 탄산가스 주입량으로 하여 밀봉하고 음료는 영양 성분이 많음으로 밀봉 후 70∼75℃에서 20∼30분간 살균이 필요하다.In carbonated beverages, carbonic acid gas is sealed at 4 to 5 ° C with a bottled pressure of 0.4 to 1.5 kg / cm 2, and the beverage is rich in nutrients. The beverage is sealed for 20 to 30 minutes at 70 to 75 ° C. Sterilization is required.
별도로 분리된 율무 고형물 케이크는 배소 건조하거나, 통풍 건조하여 다른 곡물류 분말과 혼합하여 분말음료의 기제로 사용할 수 있다.The separately separated yulmu solid cake can be roasted or air dried to be mixed with other grain powders and used as a base for powdered beverages.
효소 반응 원액을 투명 액체 추출 원액과 고형물 게이크로 분리하지 않고 전체를 두유와 혼합하여 영양음료를 만들 수도 있다.Instead of separating the enzyme reaction stock into a clear liquid extraction stock and a solids gasket, the whole can be mixed with soy milk to make a nutritious drink.
이때는 효소 반응 원액을 충분히 균질, 유화시킬 필요가 있으며, 균질 유화에는 호모게나이저나 고속코로이드 밀을 사용하게 되며, 호모게나이저(Homogenizer)로서는 60∼70℃의 원액을 100∼150kg/cm2의 압력으로 미리 원액균질을 하거나 3,000∼5,000RPM의 고속 코로이드 밀로공기 혼입을 억제하면서 마쇄한 것에 대두 단백질 2%, 지방질 1%를 더 첨가하여 또 유화제 0.3% 향료 감미료 등도 가하여 재차균질 마쇄하여 대두와 율무의 혼합 영양음료를 만든다.At this time, it is necessary to sufficiently homogenize and emulsify the enzyme reaction stock solution, and homogenizer or high speed colloid mill is used for homogeneous emulsification, and 100 to 150 kg / cm 2 of the stock solution at 60 to 70 ° C is used as a homogenizer. Pre-homogeneous solution homogenous at a pressure of 3,000 to 5,000 RPM, while suppressing the incorporation of 3,000 to 5,000 RPM high-speed colloidal mill air, 2% of soy protein and 1% of fat were added, and 0.3% of fragrance sweetener was added to the mixture so that it was ground again. Make a mixed nutritional drink with Yulmu.
이때 대두 단백질은 본인 특허 제4998호(공고번호 76-91호)에서 얻은 정선된 무취인 농축 두유를 가하여 율무원액의 불용성 고형물을 안전한 상태의 균일한 음료로 할 수 있다.In this case, soy protein can be added to the selected odorless concentrated soy milk obtained in the patent No. 4998 (Notice No. 76-91) to make the insoluble solids of the yulmu juice as a safe drink uniform.
[실시예]EXAMPLE
탈피 도정한 율무쌀 10kg를 세척기에 넣어 흰혼탁물이 나오지 않을 때까지 충분히 수세하여 일정량의 물과 같이 탕자(湯煮)한 것을 물을 가하면서 100∼150멧슈(mesh) 고속 코로이드 밀로서 마쇄하여 스러리를 얻는다. 가수량은 전체 율무 스러리이 100∼120kg이 되게 하고 액성을 Ca++이온 50PPM, pH6.5이 되게끔 조절한다.10 kg of peeled rice was put in a washing machine and washed with water until no white turbidity appeared, and it was ground as 100 ~ 150 mesh high speed colloid mill while adding water to a hot water like a certain amount of water. Get the slurry The amount of hydrolysis is adjusted to 100-120 kg of total moisture slurry, and the liquidity is set to 50 PPM, pH 6.5 of Ca ++ ion.
먼저 터마밀(Termamyl) 또 옵티럼-L(optitherm-L) 1g를 물 20kg에 녹인 수용액을 탱크에 넣어 95℃로 가열하여 두고 여기서 율무스러리에 러마밀 2.5g을 혼합한 것을 2개의 분무기로서 분사 주입시키는데 밀크 륌프로서 전체 주입시간이 약 20분 정도로서 만탱크가 되도록 주입액량을 조절한다. 이때 반응 탱크의 교반은 80∼100RPM 정도로 유지하며 생증기를 탱크내에 주입하여 95℃로 유지되도록 한다. 주입이 끝나면 반응탱크를 밀폐하여 105℃로 승온 가압하여 5분 정도 지속시킨 다음 증기를 배출시켜 강압하여 액온을 95℃로 냉각시킨다. 다음 2차로 나머지 1.5g의 타마밀을 주입 혼합하여 10∼15분 정도 교반하면서 반응시키고 옥소반응이 적갈색 또는 담적색이 되게끔 진행시킨다.First, an aqueous solution of 1 g of Teramyl or Optitim-L dissolved in 20 kg of water was added to a tank and heated to 95 ° C., where 2.5 g of Rummy Mill was mixed with Yulyul as two sprayers. Inject the milk pump and adjust the amount of injection so that the total injection time is about 20 minutes. At this time, the stirring of the reaction tank is maintained at about 80 ~ 100RPM to inject live steam into the tank to maintain at 95 ℃. After the injection, the reaction tank is sealed and pressurized to 105 ° C. to continue for about 5 minutes, and then the steam is forced down to cool the liquid temperature to 95 ° C. Next, the remaining 1.5 g of tamamyl is injected and mixed, reacted with stirring for about 10 to 15 minutes, and the oxo reaction proceeds to become reddish brown or light red.
반응이 끝나면 반응액에 게피가루 100g와 생강가루 200g를 넣어 혼합한 다음, 효소의 실활과 향신료 성분의 추출을 도모하기 위하여 120℃에서 10∼15분간 지속시킨 다음 배기 냉각시킨다.After the reaction, 100 g of geoff powder and 200 g of ginger powder are mixed in the reaction solution, and then, the mixture is maintained at 120 ° C. for 10 to 15 minutes in order to facilitate deactivation of enzymes and extraction of spices.
이 반응 원액을 40∼50℃ 정도 냉각되었을 때 훨터프레스(Filter press)에 걸러 2.5kg의 건조 게이크와 80∼90kg의 여액을 얻게 된다.When the reaction stock is cooled to about 40 to 50 ° C., a filter press is filtered to obtain 2.5 kg of dry gage and 80 to 90 kg of filtrate.
여액은 황색 투명한 액체로서 2∼3시간 원통에 넣어 청정한 다음, 스포츠 드링크, 다이어트 음료 또는 영양 음료 혹은 탄산 청량음료의 원액으로 사용된다.The filtrate is a yellow clear liquid which is placed in a cylinder for 2 to 3 hours to be cleaned and used as a stock for sports drinks, diet drinks or nutritional drinks or carbonated soft drinks.
탄산음료의 제조시 카보네이숀에 있어서는 시럽의 조합시산미료, 감미료, 착향료 등을 엄선할 것이며, 병조림에는 일반적인 프레믹스법을 사용하여 검사 후 살균공정에 들어간다. 영양 음료이기 때문에 살균과정은 매우 중요하며 탄산가스 주입으로 살균시 가스 팽창으로 병마개 파손에 주의하여야 한다.In the production of carbonated beverages, carbonaceous acid, sweeteners, flavorings, etc. will be carefully selected for carbonated beverages. In case of bottled foods, normal premix method is used for the sterilization process after inspection. As it is a nutritious drink, the sterilization process is very important and care must be taken to avoid bottle cap damage due to gas expansion during sterilization with carbon dioxide injection.
4∼5℃에서 병내 압력 0.4∼1.5kg/cm2정도의 가스 주입량으로 할 것이며, 살균도 70∼75℃에서 30∼40분간 하게 된다. 가스압을 높여서 탄산가스 주입량을 많이할 것 같으면 율무 음료의 진미를 상실할 염려가 있다.The gas injection amount is about 0.4 to 1.5 kg / cm 2 at 4 to 5 ° C and the sterilization degree is 30 to 40 minutes at 70 to 75 ° C. If you increase the gas pressure to increase the amount of carbon dioxide injection, you may lose the delicacy of Yulmu drink.
불용성 고형물 케이크는 회전 배소기에 넣어 180∼200℃에서 1∼2시간 정도 배소 건조하거나 통풍건조하여 150∼200멧슈 정도의 미립자 분말로 하여 분말 음료 기제로 사용된다.The insoluble solid cake is placed in a rotary roaster and roasted for 1 to 2 hours at 180 to 200 ° C., or dried in a ventilated form to form a fine powder of about 150 to 200 mesh and used as a powder beverage base.
또 율무 효소 반응 원액을 여과 분리하지 않고 전체를 60∼70℃에서 100∼150kg/cm2균질기로서 1차 균질한 것을 농축 두유(측허 4998호 공고번호 76-91호) 수분 80∼85%이고 단백농도 15∼18%인 것을 10∼20kg와 혼합하고 여기에 식물유 1kg와 유화제 0.3kg, 설탕 3∼4kg, 향로 약간을 가하여 전체 액량 100kg이 되게 하고 교반 혼합한 것을 2차로 60∼70℃에서 150∼200kg/cm2압으로 균질하여 포장용기에 주입 밀봉한 후 고압 살균하여 대두 율무 영양음료로 만들 수 있다.In addition, the first homogeneous whole was subjected to 100% -150kg / cm 2 homogenizer at 60-70 ° C without filtration separation of Yulmu enzyme-reaction stock solution, and 80-85% of soymilk concentrate (No. 4998 Publication No. 76-91). 15 to 18% of protein concentration is mixed with 10 to 20 kg, and 1 kg of vegetable oil, 0.3 kg of emulsifier, 3 to 4 kg of sugar, and a small amount of incense are added to make a total amount of 100 kg and stirred and mixed at 150 to 60 to 70 ° C. Homogeneous with ~ 200kg / cm 2 pressure can be injected and sealed in a packaging container, and then autoclaved to make soybean yulmu nutrition beverage.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019820003687A KR830002005B1 (en) | 1982-08-17 | 1982-08-17 | Yulmu beverage manufacturing method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019820003687A KR830002005B1 (en) | 1982-08-17 | 1982-08-17 | Yulmu beverage manufacturing method |
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