KR950003258A - Method for Purifying 2-hydroxyethyl Methacrylate - Google Patents
Method for Purifying 2-hydroxyethyl Methacrylate Download PDFInfo
- Publication number
- KR950003258A KR950003258A KR1019930014433A KR930014433A KR950003258A KR 950003258 A KR950003258 A KR 950003258A KR 1019930014433 A KR1019930014433 A KR 1019930014433A KR 930014433 A KR930014433 A KR 930014433A KR 950003258 A KR950003258 A KR 950003258A
- Authority
- KR
- South Korea
- Prior art keywords
- organic solvent
- purifying
- halohydrocarbon
- ethyl methacrylate
- hydroxy ethyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title claims abstract 10
- WOBHKFSMXKNTIM-UHFFFAOYSA-N Hydroxyethyl methacrylate Chemical compound CC(=C)C(=O)OCCO WOBHKFSMXKNTIM-UHFFFAOYSA-N 0.000 title claims abstract 5
- 239000003960 organic solvent Substances 0.000 claims abstract 6
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims abstract 5
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims abstract 4
- 150000005826 halohydrocarbons Chemical group 0.000 claims abstract 4
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims abstract 3
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 claims abstract 2
- 238000000746 purification Methods 0.000 claims abstract 2
- 238000000638 solvent extraction Methods 0.000 claims abstract 2
- 239000002904 solvent Substances 0.000 claims 1
- 125000003944 tolyl group Chemical group 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 abstract 2
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 238000007259 addition reaction Methods 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 238000006116 polymerization reaction Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
본 발명은 산, 염기 촉매 존재하에서 메타크릴산과 산화에틸렌을 부가반응시켜 얻어진 2-하이드록시 에틸 메타아크레이트를 정제하는 방법에 관한 것으로서, 유기용제로 에틸렌 디클로라이드, 메틸렌 디클로라이드와 같은 할로탄화수소 또는 톨루엔과 같은 방향족 탄화수소를 사용하는 용매추출법으로 정제함을 특징으로 한다.The present invention relates to a method for purifying 2-hydroxy ethyl methacrylate obtained by addition reaction of methacrylic acid and ethylene oxide in the presence of an acid or a base catalyst, wherein the organic solvent is a halohydrocarbon such as ethylene dichloride, methylene dichloride or It is characterized in that the purification by the solvent extraction method using an aromatic hydrocarbon such as toluene.
본 발명에 따르면 증류도중에 중합이 일어날 가능성이 없고, 잔유물이 생성되지 않아 제거 공정이 필요없고, 미반응 메타아크릴산과 부산물이 수용액층으로 충분히 제거되어 고순도의 제품을 고수율로 얻을 수 있다.According to the present invention, there is no possibility of polymerization during distillation, no residues are generated, and no removal process is required, and unreacted methacrylic acid and by-products are sufficiently removed in the aqueous solution layer to obtain a high-purity product in high yield.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음Since this is an open matter, no full text was included.
Claims (6)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019930014433A KR950003258A (en) | 1993-07-28 | 1993-07-28 | Method for Purifying 2-hydroxyethyl Methacrylate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019930014433A KR950003258A (en) | 1993-07-28 | 1993-07-28 | Method for Purifying 2-hydroxyethyl Methacrylate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR950003258A true KR950003258A (en) | 1995-02-16 |
Family
ID=67142715
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019930014433A Withdrawn KR950003258A (en) | 1993-07-28 | 1993-07-28 | Method for Purifying 2-hydroxyethyl Methacrylate |
Country Status (1)
| Country | Link |
|---|---|
| KR (1) | KR950003258A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10987762B2 (en) | 2014-09-30 | 2021-04-27 | Illinois Tool Works Inc. | Armband based systems and methods for controlling welding equipment using gestures and like motions |
| US11179796B2 (en) | 2010-07-14 | 2021-11-23 | Illinois Tool Works Inc. | Welding parameter control |
| US11654501B2 (en) | 2014-09-30 | 2023-05-23 | Illinois Tool Works Inc. | Systems and methods for gesture control of a welding system |
| US12279993B2 (en) | 2020-07-31 | 2025-04-22 | Illinois Tool Works Inc. | Smart welding helmet modules with adaptable helmet devices |
-
1993
- 1993-07-28 KR KR1019930014433A patent/KR950003258A/en not_active Withdrawn
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11179796B2 (en) | 2010-07-14 | 2021-11-23 | Illinois Tool Works Inc. | Welding parameter control |
| US10987762B2 (en) | 2014-09-30 | 2021-04-27 | Illinois Tool Works Inc. | Armband based systems and methods for controlling welding equipment using gestures and like motions |
| US11654501B2 (en) | 2014-09-30 | 2023-05-23 | Illinois Tool Works Inc. | Systems and methods for gesture control of a welding system |
| US12279993B2 (en) | 2020-07-31 | 2025-04-22 | Illinois Tool Works Inc. | Smart welding helmet modules with adaptable helmet devices |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 19930728 |
|
| PG1501 | Laying open of application | ||
| PC1203 | Withdrawal of no request for examination | ||
| WITN | Application deemed withdrawn, e.g. because no request for examination was filed or no examination fee was paid |