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PE20081305A1 - Bromuro de tiotropio cristalino anhidrido como agente anticolinergico y procedimiento para la preparacion de un medicamento - Google Patents

Bromuro de tiotropio cristalino anhidrido como agente anticolinergico y procedimiento para la preparacion de un medicamento

Info

Publication number
PE20081305A1
PE20081305A1 PE2007000660A PE2007000660A PE20081305A1 PE 20081305 A1 PE20081305 A1 PE 20081305A1 PE 2007000660 A PE2007000660 A PE 2007000660A PE 2007000660 A PE2007000660 A PE 2007000660A PE 20081305 A1 PE20081305 A1 PE 20081305A1
Authority
PE
Peru
Prior art keywords
tiotropium bromide
procedure
preparation
crystalline
anticholinergic agent
Prior art date
Application number
PE2007000660A
Other languages
English (en)
Inventor
Peter Sieger
Ulrike Werthmann
Original Assignee
Boehringer Ingelheim Pharma
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Boehringer Ingelheim Pharma filed Critical Boehringer Ingelheim Pharma
Publication of PE20081305A1 publication Critical patent/PE20081305A1/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D451/00Heterocyclic compounds containing 8-azabicyclo [3.2.1] octane, 9-azabicyclo [3.3.1] nonane, or 3-oxa-9-azatricyclo [3.3.1.0<2,4>] nonane ring systems, e.g. tropane or granatane alkaloids, scopolamine; Cyclic acetals thereof
    • C07D451/02Heterocyclic compounds containing 8-azabicyclo [3.2.1] octane, 9-azabicyclo [3.3.1] nonane, or 3-oxa-9-azatricyclo [3.3.1.0<2,4>] nonane ring systems, e.g. tropane or granatane alkaloids, scopolamine; Cyclic acetals thereof containing not further condensed 8-azabicyclo [3.2.1] octane or 3-oxa-9-azatricyclo [3.3.1.0<2,4>] nonane ring systems, e.g. tropane; Cyclic acetals thereof
    • C07D451/04Heterocyclic compounds containing 8-azabicyclo [3.2.1] octane, 9-azabicyclo [3.3.1] nonane, or 3-oxa-9-azatricyclo [3.3.1.0<2,4>] nonane ring systems, e.g. tropane or granatane alkaloids, scopolamine; Cyclic acetals thereof containing not further condensed 8-azabicyclo [3.2.1] octane or 3-oxa-9-azatricyclo [3.3.1.0<2,4>] nonane ring systems, e.g. tropane; Cyclic acetals thereof with hetero atoms directly attached in position 3 of the 8-azabicyclo [3.2.1] octane or in position 7 of the 3-oxa-9-azatricyclo [3.3.1.0<2,4>] nonane ring system
    • C07D451/06Oxygen atoms
    • C07D451/10Oxygen atoms acylated by aliphatic or araliphatic carboxylic acids, e.g. atropine, scopolamine
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/33Heterocyclic compounds
    • A61K31/395Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
    • A61K31/435Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with one nitrogen as the only ring hetero atom
    • A61K31/468-Azabicyclo [3.2.1] octane; Derivatives thereof, e.g. atropine, cocaine
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P11/00Drugs for disorders of the respiratory system
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P11/00Drugs for disorders of the respiratory system
    • A61P11/06Antiasthmatics

Landscapes

  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Veterinary Medicine (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Pulmonology (AREA)
  • Animal Behavior & Ethology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Emergency Medicine (AREA)
  • Epidemiology (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Medicinal Preparation (AREA)
  • Steroid Compounds (AREA)

Abstract

SE REFIERE AL BROMURO DE TIOTROPIO CRISTALINO ANHIDRO CARACTERIZADO POR UNA CELDA ELEMENTAL MONOCLINICA DETERMINADA MEDIANTE ANALISIS ESTRUCTURAL DE RAYOS X CON LOS PARAMETROS a=10,4336(2)A, b= 11,3297(3)A, c=17,6332(4)A Y O=90°, ß=105,158(2)° Y y=90° (VOLUMEN DE CELDA=2011,89(8)A. SE REFIERE TAMBIEN A UN PROCEDIMIENTO PARA LA PREPARACION DE BROMURO DE TIOTROPIO ANHIDRO MEDIANTE UNA DESECACION A MAS DE 50°C PREFERIBLEMENTE ENTRE 60ºC Y 100ºC, BAJO PRESION REDUCIDA DURANTE UN PERIODO DE TIEMPO DE 15 MINUTOS A 24 HORAS. SE PREPARA POR ALMACENAMIENTO DE MONOHIDRATO DE BROMURO DE TIOTROPIO CRISTALINO SOBRE UN AGENTE DE DESECACION APROPIADO DURANTE UN PERIODO DE 12 A 96 HORAS. EL BROMURO DE TIOTROPIO ES UN AGENTE ANTICOLINERGICO Y ES UTIL PARA EL TRATAMIENTO DE ASMA Y EPOC
PE2007000660A 2001-06-22 2002-06-21 Bromuro de tiotropio cristalino anhidrido como agente anticolinergico y procedimiento para la preparacion de un medicamento PE20081305A1 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10129710 2001-06-22
DE10215436 2002-04-08

Publications (1)

Publication Number Publication Date
PE20081305A1 true PE20081305A1 (es) 2008-10-01

Family

ID=26009556

Family Applications (2)

Application Number Title Priority Date Filing Date
PE2002000538A PE20030130A1 (es) 2001-06-22 2002-06-21 Procedimientos para la preparacion de bromuro de tiotropio cristalino anhidro
PE2007000660A PE20081305A1 (es) 2001-06-22 2002-06-21 Bromuro de tiotropio cristalino anhidrido como agente anticolinergico y procedimiento para la preparacion de un medicamento

Family Applications Before (1)

Application Number Title Priority Date Filing Date
PE2002000538A PE20030130A1 (es) 2001-06-22 2002-06-21 Procedimientos para la preparacion de bromuro de tiotropio cristalino anhidro

Country Status (37)

Country Link
EP (1) EP1401445B1 (es)
JP (1) JP2005504015A (es)
KR (2) KR101011353B1 (es)
CN (1) CN100586948C (es)
AR (1) AR037491A1 (es)
AT (1) ATE337006T1 (es)
AU (1) AU2002345016B2 (es)
BG (1) BG66303B1 (es)
BR (1) BR0210537A (es)
CA (1) CA2450961C (es)
CO (1) CO5550423A2 (es)
CY (1) CY1105223T1 (es)
CZ (1) CZ302786B6 (es)
DE (1) DE50207943D1 (es)
DK (1) DK1401445T3 (es)
EA (1) EA005813B1 (es)
EE (1) EE05316B1 (es)
EG (1) EG24851A (es)
ES (1) ES2271280T3 (es)
HR (1) HRP20031066B1 (es)
HU (1) HUP0400333A3 (es)
IL (2) IL159238A0 (es)
ME (1) ME00412B (es)
MX (1) MXPA03011718A (es)
MY (1) MY122779A (es)
NO (1) NO334301B1 (es)
NZ (1) NZ530690A (es)
PE (2) PE20030130A1 (es)
PL (1) PL208137B1 (es)
PT (1) PT1401445E (es)
RS (1) RS50441B (es)
SA (1) SA02230255B1 (es)
SI (1) SI1401445T1 (es)
SK (1) SK287262B6 (es)
TW (2) TWI261589B (es)
UY (1) UY27342A1 (es)
WO (1) WO2003000265A1 (es)

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BRPI0510080B8 (pt) 2004-04-22 2021-05-25 Boehringer Ingelheim Int combinação farmacêutica e seu uso
US7220742B2 (en) 2004-05-14 2007-05-22 Boehringer Ingelheim International Gmbh Enantiomerically pure beta agonists, process for the manufacture thereof and use thereof as medicaments
DE102004024454A1 (de) 2004-05-14 2005-12-08 Boehringer Ingelheim Pharma Gmbh & Co. Kg Neue Enantiomerenreine Betaagonisten, Verfahren zu deren Herstellung und deren Verwendung als Arzneimittel
ATE427108T1 (de) 2004-08-11 2009-04-15 Boehringer Ingelheim Pharma Anticholinergika enthaltende arzneimittel zur behandlung von krankheiten der ableitenden harnwege
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DE102004048389A1 (de) 2004-10-01 2006-04-06 Boehringer Ingelheim Pharma Gmbh & Co. Kg Modifizierung von Oberflächen von Laktose als Hilfsstoff zur Verwendung für Pulverinhalativa
MX2007012907A (es) 2005-04-28 2008-03-14 Boehringer Ingelheim Int Nuevos compuestos para el tratamiento de enfermedades inflamatorias.
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DK1874781T3 (da) 2006-04-19 2009-11-02 Boehringer Ingelheim Int Dihydrothienopyrimidiner til behandling af inflammatoriske sygdomme
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PE20080610A1 (es) 2006-08-22 2008-07-15 Boehringer Ingelheim Int Nuevos beta-agonistas enantiomericamente puros, procedimientos para su preparacion y uso como medicamentos
GB0716026D0 (en) 2007-08-16 2007-09-26 Norton Healthcare Ltd An inhalable medicament
DK2215092T3 (da) 2007-10-19 2012-05-07 Boehringer Ingelheim Int Substitueret piperidino-dihydrothienopyrimidin
EP2093219A1 (de) 2008-02-22 2009-08-26 Boehringer Ingelheim International Gmbh Kristalline, enantiomerenreine Salzform eines Betamimetikums und dessen Verwendung als Arzneimittel
NZ592723A (en) 2008-12-19 2013-06-28 Boehringer Ingelheim Int Cyclic pyrimidin-4-carboxamides as ccr2 receptor antagonists for treatment of inflammation, asthma and copd
WO2010101538A2 (en) 2009-03-06 2010-09-10 Bilgic Mahmut New crystal forms
AP3170A (en) 2009-12-17 2015-03-31 Boehringer Ingelheim Int New CCR2 receptor antagonists and uses thereof
EP2513086B1 (en) 2009-12-17 2015-04-29 Boehringer Ingelheim International GmbH Novel antagonists for ccr2 and uses thereof
EP2528915B1 (en) 2010-01-29 2015-10-28 Boehringer Ingelheim International GmbH Substituted naphthyridines and their use as syk kinase inhibitors
EP2569295B1 (en) 2010-05-12 2014-11-19 Boehringer Ingelheim International GmbH New ccr2 receptor antagonists, method for producing the same, and use thereof as medicaments
EP2569298B1 (en) 2010-05-12 2015-11-25 Boehringer Ingelheim International GmbH Novel ccr2 receptor antagonists, method for producing the same, and use thereof as medicaments
EP2571870B1 (en) 2010-05-17 2015-01-21 Boehringer Ingelheim International GmbH Ccr2 antagonists and uses thereof
US9018212B2 (en) 2010-05-25 2015-04-28 Boehringer Ingelheim International Gmbh Pyridazine carboxamides as CCR2 receptor antagonists
WO2011151251A1 (en) 2010-06-01 2011-12-08 Boehringer Ingelheim International Gmbh New ccr2 antagonists
TR201007108A2 (tr) * 2010-08-25 2012-03-21 B�Lg�� Mahmut Yeni tiotropyum bromür kristali ve üretim yöntemi.@
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TR201101897A2 (tr) 2011-02-28 2012-09-21 Bi̇lgi̇ç Mahmut Tiotropyum bromür içeren kristal madde
TR201102068A2 (tr) 2011-03-03 2012-09-21 Bi̇lgi̇ç Mahmut Tiotropyum bromür içeren kristal maddeler
TR201111589A2 (tr) * 2011-03-03 2012-09-21 Bi̇lgi̇ç Mahmut Tiotropyum bromür susuz kristal formu.
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WO2013010839A1 (en) 2011-07-15 2013-01-24 Boehringer Ingelheim International Gmbh Novel and selective ccr2 antagonists
AU2012288969B2 (en) 2011-07-26 2017-02-23 Boehringer Ingelheim International Gmbh Substituted quinolines and their use as medicaments
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Also Published As

Publication number Publication date
PL364489A1 (en) 2004-12-13
AU2002345016B2 (en) 2008-04-17
SK287262B6 (sk) 2010-04-07
EP1401445A1 (de) 2004-03-31
HRP20031066A2 (en) 2004-04-30
HUP0400333A3 (en) 2012-10-29
NZ530690A (en) 2005-05-27
DE50207943D1 (de) 2006-10-05
SK522004A3 (en) 2004-06-08
TWI261589B (en) 2006-09-11
MY122779A (en) 2006-05-31
PE20030130A1 (es) 2003-04-02
CZ302786B6 (cs) 2011-11-09
EP1401445B1 (de) 2006-08-23
AR037491A1 (es) 2004-11-17
KR101011353B1 (ko) 2011-01-28
CA2450961A1 (en) 2003-01-03
NO20035696D0 (no) 2003-12-19
EA200301293A1 (ru) 2004-08-26
EE05316B1 (et) 2010-08-16
NO334301B1 (no) 2014-02-03
HRP20031066B1 (en) 2011-10-31
SA02230255B1 (ar) 2006-10-31
UY27342A1 (es) 2003-02-28
RS50441B (sr) 2010-03-02
EG24851A (en) 2010-10-27
IL159238A0 (en) 2004-06-01
KR100971616B1 (ko) 2010-07-22
PT1401445E (pt) 2006-10-31
BR0210537A (pt) 2004-06-22
CA2450961C (en) 2010-03-30
CN1520294A (zh) 2004-08-11
HK1068540A1 (zh) 2005-04-29
PL208137B1 (pl) 2011-03-31
ES2271280T3 (es) 2007-04-16
KR20040018285A (ko) 2004-03-02
CN100586948C (zh) 2010-02-03
ATE337006T1 (de) 2006-09-15
ME00412B (me) 2011-10-10
TW200617007A (en) 2006-06-01
YU99703A (sh) 2006-05-25
SI1401445T1 (sl) 2007-02-28
DK1401445T3 (da) 2006-11-27
CY1105223T1 (el) 2010-03-03
MEP62008A (en) 2011-05-10
EA005813B1 (ru) 2005-06-30
CZ2004120A3 (cs) 2004-05-12
WO2003000265A1 (de) 2003-01-03
MXPA03011718A (es) 2004-12-06
CO5550423A2 (es) 2005-08-31
IL159238A (en) 2010-04-15
KR20090031638A (ko) 2009-03-26
BG108440A (bg) 2004-08-31
EE200400029A (et) 2004-04-15
BG66303B1 (bg) 2013-03-29
JP2005504015A (ja) 2005-02-10
HUP0400333A2 (hu) 2004-12-28

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