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RU2001165C1 - Method for producing fibers from pitch - Google Patents

Method for producing fibers from pitch

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Publication number
RU2001165C1
RU2001165C1 SU5030395A RU2001165C1 RU 2001165 C1 RU2001165 C1 RU 2001165C1 SU 5030395 A SU5030395 A SU 5030395A RU 2001165 C1 RU2001165 C1 RU 2001165C1
Authority
RU
Russia
Prior art keywords
pitch
producing fibers
fiber
carried out
diameter
Prior art date
Application number
Other languages
Russian (ru)
Inventor
Валерий Яковлевич Варшавский
Александр Львович Журавлев
Михаил Львович Учитель
ков Олег Леонидович Мещер
Сергей Алексеевич Корепанов
Ирина Михайловна Стырикович
Original Assignee
Валерий Яковлевич Варшавский
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Валерий Яковлевич Варшавский filed Critical Валерий Яковлевич Варшавский
Priority to SU5030395 priority Critical patent/RU2001165C1/en
Application granted granted Critical
Publication of RU2001165C1 publication Critical patent/RU2001165C1/en

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Description

Сформированную нить выт гивают с помощью эжектора и укладывают в приемное устройство Лучший режим формовани  (пример 3) позвол ет в этих услови х получить волокно диаметром 32 мкм. Из этого волокна путем термообработки не удаетс  получить углеродное волокно с высокими показател ми, его прочность составл ет 31 кг/мм , что объ сн етс  большим диаметром свежесформированного и, соответственно , углеродного волокнаThe formed thread is drawn using an ejector and placed in a receiving device. The best spinning mode (Example 3) allows one to obtain a fiber with a diameter of 32 microns under these conditions. It is not possible to obtain high-performance carbon fiber from this fiber by heat treatment, its strength is 31 kg / mm, which is explained by the large diameter of the freshly formed and, accordingly, carbon fiber

Стабильность процесса формовани  также невысока: через 30 минут наблюдает- ст засор отверстий фипьерыThe stability of the molding process is also low: after 30 minutes, there is a clogging of the openings of the fixture

Увеличение диаметра отверсти  фильеры дл  снижени  опасности засора невозможно , так как при этом дополнительно возрастает диаметр сформованного волок0It is not possible to increase the diameter of the die hole to reduce the risk of clogging, since this also increases the diameter of the formed fiber

Увеличение подачи во эдуха в )рктор с целью повышени  ступени вытчгипани  и снижени  Диаметра волокна приводит к рез кому возрастанию его обрывности При повышении температуры формование с 260 до 280°С (пример 4) плов пека тер ет спо собность к волокнообразооанию, что обьчс н етс  (как это отмечено в описании зачвки) сильным снижением в зкости расплава п каIncreasing the supply to edu c) the reactor in order to increase the degree of extrusion and reduce the Diameter of the fiber leads to a sharp increase in its breakage. At an increase in temperature, molding from 260 to 280 ° C (Example 4), the baked cake loses its ability to fiber formation, which is usually the case. (as noted in the description of the dressing) a strong decrease in the viscosity of the melt

(56) Патент США N 4230650, кл В 06 В 1 /02, опублик 1980(56) U.S. Patent No. 4,230,650, class B 06 B 1/02, published 1980

Edle D D., Dunham M G Cation 151989 г , т 27, гФ 5, р 647-655Edle D D., Dunham M G Cation 151,989 g, t 27, gF 5, p 647-655

Плтент США Мг 4762652 кл П01Р9/14 опублик 1988Plent USA Mg 4762652 class P01R9 / 14 published 1988

Вли ние г л о п и и поThe impact of gl

Claims (1)

Формула изобретени The claims СПОСОБ ПОЛУЧЕНИЯ ВОЛОК1IA ИЗ ПЕКА ЭКСТруна 110 - 200 С превышающейMETHOD FOR PRODUCING WOLF1IA FROM EXTUNE PECK 110 - 200 С exceeding температуруtemperature дированием расплава пека через фильеру 40 Разм гчени  пека d проводит в и выт жкой, отличающийс  тем, что экстру- дирование осуществл ют при температуреby pressing the molten pitch through a die 40, Softening the pitch d is carried out in and by extraction, characterized in that the extrusion is carried out at a temperature электростатическом поле со средней напр женностью 3 - 20 кЗ/смelectrostatic field with an average strength of 3 - 20 kg / cm углРроД Ь.1 ЙОПС 1CARBON L.1 JOPS 1 П здт 2 шеP 2 2 на 110 - 200 С превышающей110 - 200 C higher Разм гчени  пека d проводит в  Grind the pitch of the pitch d holds in электростатическом поле со средней напр женностью 3 - 20 кЗ/смelectrostatic field with an average strength of 3 - 20 kg / cm
SU5030395 1992-03-03 1992-03-03 Method for producing fibers from pitch RU2001165C1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU5030395 RU2001165C1 (en) 1992-03-03 1992-03-03 Method for producing fibers from pitch

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU5030395 RU2001165C1 (en) 1992-03-03 1992-03-03 Method for producing fibers from pitch

Publications (1)

Publication Number Publication Date
RU2001165C1 true RU2001165C1 (en) 1993-10-15

Family

ID=21598413

Family Applications (1)

Application Number Title Priority Date Filing Date
SU5030395 RU2001165C1 (en) 1992-03-03 1992-03-03 Method for producing fibers from pitch

Country Status (1)

Country Link
RU (1) RU2001165C1 (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2160225C2 (en) * 1995-06-07 2000-12-10 Коноко Инк. Method and device for drawing carbon fibers from solvated resin
RU2318932C2 (en) * 2002-08-07 2008-03-10 Олбани Интернэшнл Текнивив, Инк. Tar-based graphite fabrics and needle stitched felts for gas diffusion layer substrates of fuel cell, and reinforced high thermal conductivity composites
RU2538687C2 (en) * 2013-01-17 2015-01-10 Открытое акционерное общество "Авиационная корпорация "Рубин" (ОАО "АК "Рубин") Method of determining degree of impregnation of carbon fibre braids with pitches and device for its realisation

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2160225C2 (en) * 1995-06-07 2000-12-10 Коноко Инк. Method and device for drawing carbon fibers from solvated resin
RU2318932C2 (en) * 2002-08-07 2008-03-10 Олбани Интернэшнл Текнивив, Инк. Tar-based graphite fabrics and needle stitched felts for gas diffusion layer substrates of fuel cell, and reinforced high thermal conductivity composites
RU2538687C2 (en) * 2013-01-17 2015-01-10 Открытое акционерное общество "Авиационная корпорация "Рубин" (ОАО "АК "Рубин") Method of determining degree of impregnation of carbon fibre braids with pitches and device for its realisation

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