WO1992011347A3 - Enzyme preparation for washing and cleansing agents - Google Patents
Enzyme preparation for washing and cleansing agents Download PDFInfo
- Publication number
- WO1992011347A3 WO1992011347A3 PCT/EP1991/002340 EP9102340W WO9211347A3 WO 1992011347 A3 WO1992011347 A3 WO 1992011347A3 EP 9102340 W EP9102340 W EP 9102340W WO 9211347 A3 WO9211347 A3 WO 9211347A3
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- washing
- fermentation
- additives
- mixing
- water
- Prior art date
Links
- 102000004190 Enzymes Human genes 0.000 title abstract 4
- 108090000790 Enzymes Proteins 0.000 title abstract 4
- 238000005406 washing Methods 0.000 title abstract 3
- 239000003599 detergent Substances 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title 1
- 238000000855 fermentation Methods 0.000 abstract 4
- 230000004151 fermentation Effects 0.000 abstract 4
- 229940088598 enzyme Drugs 0.000 abstract 3
- 239000008187 granular material Substances 0.000 abstract 3
- 239000000654 additive Substances 0.000 abstract 2
- 235000013339 cereals Nutrition 0.000 abstract 2
- 102000013142 Amylases Human genes 0.000 abstract 1
- 108010065511 Amylases Proteins 0.000 abstract 1
- 102000005575 Cellulases Human genes 0.000 abstract 1
- 108010084185 Cellulases Proteins 0.000 abstract 1
- 102000004882 Lipase Human genes 0.000 abstract 1
- 108090001060 Lipase Proteins 0.000 abstract 1
- 239000004367 Lipase Substances 0.000 abstract 1
- 102000035195 Peptidases Human genes 0.000 abstract 1
- 108091005804 Peptidases Proteins 0.000 abstract 1
- 239000004365 Protease Substances 0.000 abstract 1
- 229920002472 Starch Polymers 0.000 abstract 1
- 235000019418 amylase Nutrition 0.000 abstract 1
- 229940025131 amylases Drugs 0.000 abstract 1
- 235000013312 flour Nutrition 0.000 abstract 1
- 239000003979 granulating agent Substances 0.000 abstract 1
- 235000019421 lipase Nutrition 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000001471 micro-filtration Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 235000019698 starch Nutrition 0.000 abstract 1
- 239000008107 starch Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38672—Granulated or coated enzymes
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
In the production of enzyme granulates with grain sizes from 0.1 to 2 mm, containing 2 to 20 % wt. proteases, lipases, amylases and/or cellulases, 10 to 50 % wt. swellable starch, 5 to 50 % wt. granulating agent, 3 to 12 % wt. water and not more than 10 % wt. water-soluble salt, by extruding an enzyme pre-mixture obtained by mixing a fermentation liquor cleared of insoluble components and concentrated with additives and spheroidizing the extrudate in a rounder, the use of relatively highly concentrated fermentation liquours has previously been necessary. By removing the insoluble components from the fermentation liquor by micro-filtration and mixing with additives which, in relation to the finished granulate, contains 10 to 35 % wt. cereal flour, it is possible, by the use of low-concentration fermentation liquors, to obtain highly active enzyme granulates with a long shelf life which are suitable for inclusion in washing and cleansing agents and are distinguished by uniform solubility properties in aqueous washing and cleansing baths.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP92900162A EP0564476B1 (en) | 1990-12-24 | 1991-12-06 | Enzyme preparation for washing and cleansing agents |
| DE59105338T DE59105338D1 (en) | 1990-12-24 | 1991-12-06 | ENZYME PREPARATION FOR DETERGENT AND CLEANING AGENT. |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEP4041752.2 | 1990-12-24 | ||
| DE4041752A DE4041752A1 (en) | 1990-12-24 | 1990-12-24 | ENZYME PREPARATION FOR WASHING AND CLEANING AGENTS |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| WO1992011347A2 WO1992011347A2 (en) | 1992-07-09 |
| WO1992011347A3 true WO1992011347A3 (en) | 1992-08-06 |
Family
ID=6421424
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/EP1991/002340 WO1992011347A2 (en) | 1990-12-24 | 1991-12-06 | Enzyme preparation for washing and cleansing agents |
Country Status (6)
| Country | Link |
|---|---|
| EP (1) | EP0564476B1 (en) |
| AT (1) | ATE121770T1 (en) |
| DE (2) | DE4041752A1 (en) |
| DK (1) | DK0564476T3 (en) |
| ES (1) | ES2071478T3 (en) |
| WO (1) | WO1992011347A2 (en) |
Families Citing this family (75)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08500375A (en) * | 1992-08-14 | 1996-01-16 | ゾルファイ エンツィーメス ゲゼルシャフト ミツト ベシユレンクテル ハフツング ウント コンパニー コマンディートゲゼルシャフト | New enzyme granules |
| DE4310506A1 (en) * | 1993-03-31 | 1994-10-06 | Cognis Bio Umwelt | Enzyme preparation for detergents and cleaning agents |
| DE4322229A1 (en) * | 1993-07-05 | 1995-01-12 | Cognis Bio Umwelt | Enveloped enzyme preparation for detergents and cleaners |
| DE4329463A1 (en) * | 1993-09-01 | 1995-03-02 | Cognis Bio Umwelt | More enzyme granules |
| DE4344215A1 (en) * | 1993-12-23 | 1995-06-29 | Cognis Bio Umwelt | Silver corrosion inhibitor-containing enzyme preparation |
| DE4420730A1 (en) * | 1994-06-15 | 1995-12-21 | Henkel Kgaa | Process for the deodorization and stabilization of biotechnologically obtained valuable substances and their aqueous preparations |
| DE4422609A1 (en) * | 1994-06-28 | 1996-01-04 | Cognis Bio Umwelt | Multi-enzyme granules |
| DE4422433A1 (en) * | 1994-06-28 | 1996-01-04 | Cognis Bio Umwelt | Multi-enzyme granules |
| JPH10508755A (en) * | 1994-11-18 | 1998-09-02 | ジェネンコア インターナショナル インコーポレーテッド | Coated enzyme granules |
| DE19521371A1 (en) * | 1995-06-12 | 1996-12-19 | Henkel Kgaa | Enzyme granules containing silver corrosion inhibitor |
| US5571446A (en) * | 1995-07-27 | 1996-11-05 | Diversey Corporation | Anionic stabilized enzyme based clean-in-place system |
| PT758018E (en) * | 1995-07-28 | 2004-08-31 | Basf Ag | PREPARATIONS OF ENZYMES STABILIZED WITH A SALT |
| DE19543197A1 (en) * | 1995-11-20 | 1997-05-22 | Henkel Kgaa | Cobuilderhaltige enzyme preparation |
| DE19545729A1 (en) | 1995-12-08 | 1997-06-12 | Henkel Kgaa | Bleach and detergent with an enzymatic bleaching system |
| DE19600018A1 (en) | 1996-01-03 | 1997-07-10 | Henkel Kgaa | Detergent with certain oxidized oligosaccharides |
| DE19605688A1 (en) * | 1996-02-16 | 1997-08-21 | Henkel Kgaa | Transition metal complexes as activators for peroxygen compounds |
| EP0891415A1 (en) * | 1996-04-01 | 1999-01-20 | Henkel Kommanditgesellschaft auf Aktien | Cleaning agent with oligoammine activator complexes for peroxide compounds |
| DE19620411A1 (en) | 1996-04-01 | 1997-10-02 | Henkel Kgaa | Transition metal amine complexes as activators for peroxygen compounds |
| DE19615776A1 (en) * | 1996-04-20 | 1997-10-23 | Henkel Kgaa | Solubility-enhanced enzyme granules |
| DE19616693A1 (en) * | 1996-04-26 | 1997-11-06 | Henkel Kgaa | Enol esters as bleach activators for detergents and cleaning agents |
| DE19619219A1 (en) | 1996-05-13 | 1997-12-04 | Hoechst Ag | Enzyme pre-granules for animal feed granules |
| US8828432B2 (en) | 1996-10-28 | 2014-09-09 | General Mills, Inc. | Embedding and encapsulation of sensitive components into a matrix to obtain discrete controlled release particles |
| DE19649375A1 (en) | 1996-11-29 | 1998-06-04 | Henkel Kgaa | Acetonitrile derivatives as bleach activators in detergents |
| DE19651446A1 (en) | 1996-12-11 | 1998-06-18 | Henkel Kgaa | Enveloped enzyme preparation with improved solubility |
| DE19700327A1 (en) * | 1997-01-08 | 1998-07-09 | Henkel Kgaa | Protease and amylase detergent |
| DE19713852A1 (en) | 1997-04-04 | 1998-10-08 | Henkel Kgaa | Activators for peroxygen compounds in detergents and cleaning agents |
| DE19718978A1 (en) * | 1997-05-05 | 1998-11-12 | Henkel Kgaa | Process for inhibiting color transfer in textiles during washing |
| TW409035B (en) | 1997-06-04 | 2000-10-21 | Gist Brocades Bv | Starch-based enzyme granulates |
| DE19732751A1 (en) | 1997-07-30 | 1999-02-04 | Henkel Kgaa | New Bacillus beta glucanase |
| DE19732750A1 (en) | 1997-07-30 | 1999-02-04 | Henkel Kgaa | Cleaning agent containing glucanase for hard surfaces |
| DE19732749A1 (en) | 1997-07-30 | 1999-02-04 | Henkel Kgaa | Detergent containing glucanase |
| BR9813768A (en) | 1997-12-20 | 2000-10-10 | Genencor Int | Granule, and, process of producing a granule. |
| US7201923B1 (en) | 1998-03-23 | 2007-04-10 | General Mills, Inc. | Encapsulation of sensitive liquid components into a matrix to obtain discrete shelf-stable particles |
| PE20000601A1 (en) | 1998-03-23 | 2000-07-25 | Gen Mills Inc | ENCAPSULATION OF COMPONENTS IN EDIBLE PRODUCTS |
| DE19819187A1 (en) | 1998-04-30 | 1999-11-11 | Henkel Kgaa | Solid dishwasher detergent with phosphate and crystalline layered silicates |
| DE19824705A1 (en) | 1998-06-03 | 1999-12-09 | Henkel Kgaa | Detergents and cleaning agents containing amylase and protease |
| CA2345815C (en) | 1998-10-09 | 2011-02-08 | General Mills, Inc. | Encapsulation of sensitive liquid components into a matrix to obtain discrete shelf-stable particles |
| DE19850100A1 (en) | 1998-10-29 | 2000-05-04 | Henkel Kgaa | Polymer granules through fluidized bed granulation |
| DE19857204A1 (en) | 1998-12-11 | 2000-06-15 | Henkel Kgaa | Aqueous foam regulator emulsion |
| DE19859385A1 (en) | 1998-12-22 | 2000-06-29 | Basf Ag | Process for the preparation of enzyme-containing granules |
| DE19908051A1 (en) | 1999-02-25 | 2000-08-31 | Henkel Kgaa | Process for the preparation of compounded acetonitrile derivatives |
| DE19956239A1 (en) * | 1999-11-23 | 2001-05-31 | Henkel Kgaa | Recovery of biotechnological products comprises an additional wash step which is carried out with a previously obtained filtration liquid |
| DE19956382A1 (en) * | 1999-11-24 | 2001-05-31 | Henkel Kgaa | Microencapsulated enzymes retaining their activity in detergents are obtained by dispersing an aqueous enzyme solution in a starch solution and/or emulsion |
| AU2001287643A1 (en) | 2000-07-28 | 2002-02-13 | Henkel Kommanditgesellschaft Auf Aktien | Novel amylolytic enzyme extracted from bacillus SP. A 7-7 (DSM 12368) and washing and cleaning agents containing this novel amylolytic enzyme |
| DE10058645A1 (en) | 2000-11-25 | 2002-05-29 | Clariant Gmbh | Use of cyclic sugar ketones as catalysts for peroxygen compounds |
| DE50113038D1 (en) | 2000-11-28 | 2007-10-31 | Henkel Kgaa | CYCLODEXTRINE -GLUCANOTRANSFERASE (CG TASE) FROM BACILLUS AGARADHERENS (DSM 9948) AND WASHING AND CLEANING AGENT WITH THIS NEW CYCLODEXTRIN GLUCANOTRANSFERASE |
| DE10061280A1 (en) * | 2000-12-08 | 2002-06-13 | Novaprot Gmbh | Cleaning-effective, surface-active combination of renewable raw materials with high fat-dissolving power |
| DE10102248A1 (en) | 2001-01-19 | 2002-07-25 | Clariant Gmbh | Use of transition metal complexes with oxime ligands as bleach catalysts |
| DE10108459A1 (en) | 2001-02-22 | 2002-09-12 | Henkel Kgaa | Stability of foam-regulator granulates for use in detergents is improved by using a carrier containing alkali carbonate and a Bronsted acid |
| DE10142124A1 (en) | 2001-08-30 | 2003-03-27 | Henkel Kgaa | Coated active ingredient preparation for use in particulate detergents and cleaning agents |
| DE10163748A1 (en) | 2001-12-21 | 2003-07-17 | Henkel Kgaa | New glycosyl hydrolases |
| DE10211389A1 (en) | 2002-03-15 | 2003-09-25 | Clariant Gmbh | Ammonium nitrile compounds, used as activator for peroxide bleach in laundry, dishwasher and other detergents and disinfectants and in bleaching textile, paper and wood are new |
| US7431986B2 (en) | 2002-07-24 | 2008-10-07 | General Mills, Inc. | Encapsulation of sensitive components using pre-emulsification |
| DE10304131A1 (en) | 2003-02-03 | 2004-08-05 | Clariant Gmbh | Transition metal complexes with nitrogen-containing ligands are used as catalysts for peroxy compounds, especially in detergent, bleaching and cleansing agents |
| JP2007514025A (en) | 2003-12-13 | 2007-05-31 | ヘンケル・コマンディットゲゼルシャフト・アウフ・アクチエン | Multi-component thin-to-sic system |
| US8361946B2 (en) | 2004-04-08 | 2013-01-29 | Akzo Nobel N.V. | Detergent composition |
| EP1754781B1 (en) | 2005-08-19 | 2013-04-03 | The Procter and Gamble Company | A solid laundry detergent composition comprising anionic detersive surfactant and a calcium-augmented technology |
| DE102005039580A1 (en) | 2005-08-19 | 2007-02-22 | Henkel Kgaa | Color protecting detergent |
| US7803413B2 (en) | 2005-10-31 | 2010-09-28 | General Mills Ip Holdings Ii, Llc. | Encapsulation of readily oxidizable components |
| DE102006038448A1 (en) | 2005-12-28 | 2008-02-21 | Henkel Kgaa | Enzyme-containing cleaning agent |
| DE102007029643A1 (en) | 2006-09-08 | 2009-01-15 | Henkel Ag & Co. Kgaa | cleaning supplies |
| DE102007016391A1 (en) | 2007-04-03 | 2008-10-09 | Henkel Ag & Co. Kgaa | Detergent or cleaning agent for preventing transfer of textile color of colored textiles from uncolored or different colored textiles in laundry, particularly in tenside containing aqueous solution, has color transfer inhibitor |
| DE102007028310A1 (en) | 2007-06-20 | 2008-12-24 | Clariant International Ltd. | Surfactant mixtures with synergistic properties |
| DE102008013606A1 (en) | 2008-03-11 | 2009-09-17 | Clariant International Ltd. | Process for the preparation of solid alkaline earth metal salts of secondary paraffin sulphonic acids |
| US8492324B2 (en) | 2008-04-09 | 2013-07-23 | Basf Se | Use of metal hydrazide complex compounds as oxidation catalysts |
| EP2585431B1 (en) | 2010-06-28 | 2017-09-06 | Basf Se | Metal free bleaching composition |
| BR112013014591B1 (en) | 2010-12-13 | 2019-04-16 | Basf Se | COMPOSITION, DETERGENT, CLEANING, DISINFECTANT OR BLASTING COMPOSITION, GRANULA, PROCESS FOR STAINING DIRT OR DIRT IN MATERIALS, AND USE OF COMPOUND |
| DE102011010818A1 (en) | 2011-02-10 | 2012-08-16 | Clariant International Ltd. | Use of transition metal complexes as bleaching catalysts in detergents and cleaners |
| DE102014009836B4 (en) | 2014-07-03 | 2017-04-06 | Weylchem Wiesbaden Gmbh | Sodium salts of secondary alkanesulfonates containing compounds, their preparation and use and washing, disinfecting and cleaning agents containing these |
| DE102015217816A1 (en) | 2015-09-17 | 2017-03-23 | Henkel Ag & Co. Kgaa | Use of highly concentrated enzyme granules to increase the storage stability of enzymes |
| WO2017076771A1 (en) | 2015-11-03 | 2017-05-11 | Basf Se | Bleach catalysts |
| EP3176157A1 (en) | 2015-12-01 | 2017-06-07 | Basf Se | Bleach catalysts |
| WO2017186480A1 (en) | 2016-04-26 | 2017-11-02 | Basf Se | Metal free bleaching composition |
| EP3372663A1 (en) | 2017-03-10 | 2018-09-12 | Basf Se | Bleach catalysts |
| NL2021893B1 (en) | 2018-10-26 | 2020-05-13 | Citeq B V | Biological pest control agent |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1067711B (en) * | 1957-06-11 | 1959-10-22 | Bancroft Brillotex Internat S | Method of cleaning wool |
| US4176079A (en) * | 1977-04-20 | 1979-11-27 | The Procter & Gamble Company | Water-soluble enzyme-containing article |
| EP0168526A1 (en) * | 1983-12-07 | 1986-01-22 | Henkel Kommanditgesellschaft auf Aktien | Enzyme preparation for use in powder detergents |
| EP0216322A1 (en) * | 1985-09-24 | 1987-04-01 | Heinz Weber | Washing composition and process for cleansing textiles |
-
1990
- 1990-12-24 DE DE4041752A patent/DE4041752A1/en not_active Withdrawn
-
1991
- 1991-12-06 DK DK92900162.6T patent/DK0564476T3/en active
- 1991-12-06 WO PCT/EP1991/002340 patent/WO1992011347A2/en active IP Right Grant
- 1991-12-06 AT AT92900162T patent/ATE121770T1/en not_active IP Right Cessation
- 1991-12-06 EP EP92900162A patent/EP0564476B1/en not_active Expired - Lifetime
- 1991-12-06 DE DE59105338T patent/DE59105338D1/en not_active Expired - Lifetime
- 1991-12-06 ES ES92900162T patent/ES2071478T3/en not_active Expired - Lifetime
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1067711B (en) * | 1957-06-11 | 1959-10-22 | Bancroft Brillotex Internat S | Method of cleaning wool |
| US4176079A (en) * | 1977-04-20 | 1979-11-27 | The Procter & Gamble Company | Water-soluble enzyme-containing article |
| EP0168526A1 (en) * | 1983-12-07 | 1986-01-22 | Henkel Kommanditgesellschaft auf Aktien | Enzyme preparation for use in powder detergents |
| EP0216322A1 (en) * | 1985-09-24 | 1987-04-01 | Heinz Weber | Washing composition and process for cleansing textiles |
Also Published As
| Publication number | Publication date |
|---|---|
| ES2071478T3 (en) | 1995-06-16 |
| DE4041752A1 (en) | 1992-06-25 |
| DK0564476T3 (en) | 1995-09-04 |
| DE59105338D1 (en) | 1995-06-01 |
| EP0564476A1 (en) | 1993-10-13 |
| WO1992011347A2 (en) | 1992-07-09 |
| EP0564476B1 (en) | 1995-04-26 |
| ATE121770T1 (en) | 1995-05-15 |
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