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WO1994022009A3 - A method and equipment for the analysis of volatile organic compounds - Google Patents

A method and equipment for the analysis of volatile organic compounds Download PDF

Info

Publication number
WO1994022009A3
WO1994022009A3 PCT/EP1994/000889 EP9400889W WO9422009A3 WO 1994022009 A3 WO1994022009 A3 WO 1994022009A3 EP 9400889 W EP9400889 W EP 9400889W WO 9422009 A3 WO9422009 A3 WO 9422009A3
Authority
WO
WIPO (PCT)
Prior art keywords
analysis
organic compounds
volatile organic
equipment
sample
Prior art date
Application number
PCT/EP1994/000889
Other languages
French (fr)
Other versions
WO1994022009A2 (en
Inventor
Fausto Munari
Dimitris Kotzias
Matthew Duane
Original Assignee
Fisons Instr Spa
Fausto Munari
Dimitris Kotzias
Matthew Duane
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fisons Instr Spa, Fausto Munari, Dimitris Kotzias, Matthew Duane filed Critical Fisons Instr Spa
Publication of WO1994022009A2 publication Critical patent/WO1994022009A2/en
Publication of WO1994022009A3 publication Critical patent/WO1994022009A3/en

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/04—Preparation or injection of sample to be analysed
    • G01N30/06—Preparation
    • G01N30/12—Preparation by evaporation
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N2030/022—Column chromatography characterised by the kind of separation mechanism
    • G01N2030/025—Gas chromatography
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/04—Preparation or injection of sample to be analysed
    • G01N30/06—Preparation
    • G01N30/12—Preparation by evaporation
    • G01N2030/121—Preparation by evaporation cooling; cold traps
    • G01N2030/122—Preparation by evaporation cooling; cold traps cryogenic focusing
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/28—Control of physical parameters of the fluid carrier
    • G01N30/32—Control of physical parameters of the fluid carrier of pressure or speed
    • G01N2030/324—Control of physical parameters of the fluid carrier of pressure or speed speed, flow rate

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)

Abstract

The analysis of volatile organic compounds at low concentrations (ppb or ppt) is performed by making a sample flow to pass through a cold trap containing few mg of packing, at a sample feeding speed ranging between 50 and 1000 cm/sec; the sample thus concentrated is then desorbed by heating of the trap and conveyed for the analysis.
PCT/EP1994/000889 1993-03-25 1994-03-22 A method and equipment for the analysis of volatile organic compounds WO1994022009A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
ITMI930571A IT1270972B (en) 1993-03-25 1993-03-25 PROCEDURE AND EQUIPMENT FOR THE ANALYSIS OF ORGANIC VOLATILE COMPOUNDS.
ITMI93A000571 1993-03-25

Publications (2)

Publication Number Publication Date
WO1994022009A2 WO1994022009A2 (en) 1994-09-29
WO1994022009A3 true WO1994022009A3 (en) 1995-02-02

Family

ID=11365490

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP1994/000889 WO1994022009A2 (en) 1993-03-25 1994-03-22 A method and equipment for the analysis of volatile organic compounds

Country Status (2)

Country Link
IT (1) IT1270972B (en)
WO (1) WO1994022009A2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109799302B (en) * 2019-03-20 2021-08-31 上海市环境科学研究院 Near-online detection method for medium-volatility organic compounds

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8257951B2 (en) * 2002-10-28 2012-09-04 Little Sioux Corn Processors, LLC. Ethanol production process
DE602004011795T2 (en) 2003-10-17 2009-02-05 PerkinElmer LAS, Inc., Boston METHOD FOR INTRODUCING STANDARD GAS INTO A SAMPLING VESSEL
CN102375041B (en) * 2011-09-16 2015-03-04 武汉市天虹仪表有限责任公司 Online volatile organic matter analyzer and using method thereof
CN103499662B (en) * 2013-09-12 2015-01-28 苏州威阳环保科技有限公司 Sampling analysis device and sampling analysis method for atmosphere volatile organic compounds
KR101818841B1 (en) * 2016-03-09 2018-01-16 포항공과대학교 산학협력단 Portable system for analyzing sulfur hexafluoride
CN108627369B (en) * 2017-03-20 2023-11-07 广州禾信仪器股份有限公司 Atmospheric volatile organic compound double-stage cryogenic online enrichment concentration sampling system and method
CN112816644A (en) * 2020-12-31 2021-05-18 杭州谱育科技发展有限公司 Device and method for detecting VOCs in water

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3592064A (en) * 1969-02-18 1971-07-13 Bryggeriindustriens Forsknings Method for transferring a sample to be analyzed into the column of a gas chromatograph, and system for carrying out the method
US4998433A (en) * 1989-06-19 1991-03-12 Stumpf David K Method and means for condensing trace air contaminates from gases
US5168746A (en) * 1991-06-03 1992-12-08 Hughes Aircraft Company Ambient ether vapor testing apparatus and method
EP0519614A2 (en) * 1991-06-18 1992-12-23 The Regents Of The University Of Michigan Sample collection and inlet systems for gas chromatography apparatus

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3592064A (en) * 1969-02-18 1971-07-13 Bryggeriindustriens Forsknings Method for transferring a sample to be analyzed into the column of a gas chromatograph, and system for carrying out the method
US4998433A (en) * 1989-06-19 1991-03-12 Stumpf David K Method and means for condensing trace air contaminates from gases
US5168746A (en) * 1991-06-03 1992-12-08 Hughes Aircraft Company Ambient ether vapor testing apparatus and method
EP0519614A2 (en) * 1991-06-18 1992-12-23 The Regents Of The University Of Michigan Sample collection and inlet systems for gas chromatography apparatus

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
B.A. EWELS ET AL.: "electrically heated cold trap inlet system for high-speed gas chromatography", ANALYTICAL CHEMISTRY, vol. 57, no. 14, December 1985 (1985-12-01), COLUMBUS US, pages 2774 - 2779 *
L.A.LANNING ET AL.: "electrically heated cold trap inlet system for computer-controlled high-speed gas chromatography", ANALYTICAL CHEMISTRY, vol. 60, no. 18, December 1988 (1988-12-01), COLUMBUS US, pages 1994 - 1996, XP000021331 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109799302B (en) * 2019-03-20 2021-08-31 上海市环境科学研究院 Near-online detection method for medium-volatility organic compounds

Also Published As

Publication number Publication date
WO1994022009A2 (en) 1994-09-29
IT1270972B (en) 1997-05-26
ITMI930571A0 (en) 1993-03-25
ITMI930571A1 (en) 1994-09-25

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