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WO2007032810A3 - Procédé de mise en contact multiphase à l’aide d’un dispositif de microcanal - Google Patents

Procédé de mise en contact multiphase à l’aide d’un dispositif de microcanal Download PDF

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Publication number
WO2007032810A3
WO2007032810A3 PCT/US2006/026682 US2006026682W WO2007032810A3 WO 2007032810 A3 WO2007032810 A3 WO 2007032810A3 US 2006026682 W US2006026682 W US 2006026682W WO 2007032810 A3 WO2007032810 A3 WO 2007032810A3
Authority
WO
WIPO (PCT)
Prior art keywords
phase
liquid phase
microchannel
fluid
phase contacting
Prior art date
Application number
PCT/US2006/026682
Other languages
English (en)
Other versions
WO2007032810A2 (fr
Inventor
Anna Lee Tonkovich
Maddalena Fanelli
Ravi Arora
Timothy J Sullivan
Steven T Perry
David J Kuhlmann
Original Assignee
Velocys Inc
Anna Lee Tonkovich
Maddalena Fanelli
Ravi Arora
Timothy J Sullivan
Steven T Perry
David J Kuhlmann
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US11/177,941 external-priority patent/US7610775B2/en
Application filed by Velocys Inc, Anna Lee Tonkovich, Maddalena Fanelli, Ravi Arora, Timothy J Sullivan, Steven T Perry, David J Kuhlmann filed Critical Velocys Inc
Priority to EP06836085A priority Critical patent/EP1917099A2/fr
Priority to CA002613674A priority patent/CA2613674A1/fr
Publication of WO2007032810A2 publication Critical patent/WO2007032810A2/fr
Publication of WO2007032810A3 publication Critical patent/WO2007032810A3/fr

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
    • B01F25/431—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor
    • B01F25/4317—Profiled elements, e.g. profiled blades, bars, pillars, columns or chevrons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/14—Evaporating with heated gases or vapours or liquids in contact with the liquid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D19/00—Degasification of liquids
    • B01D19/0031—Degasification of liquids by filtration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20—Mixing gases with liquids
    • B01F23/23—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/232—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using flow-mixing means for introducing the gases, e.g. baffles
    • B01F23/2321—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using flow-mixing means for introducing the gases, e.g. baffles by moving liquid and gas in counter current
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
    • B01F25/431—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40—Static mixers
    • B01F25/42—Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/43—Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
    • B01F25/431—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor
    • B01F25/43197—Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor characterised by the mounting of the baffles or obstructions
    • B01F25/431971—Mounted on the wall
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00—Other mixers; Mixing plants; Combinations of mixers
    • B01F33/30—Micromixers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00783—Laminate assemblies, i.e. the reactor comprising a stack of plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00822—Metal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00824—Ceramic
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00824—Ceramic
    • B01J2219/00826—Quartz
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00824—Ceramic
    • B01J2219/00828—Silicon wafers or plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00831—Glass
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00833—Plastic
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00835—Comprising catalytically active material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00844—Comprising porous material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00858—Aspects relating to the size of the reactor
    • B01J2219/0086—Dimensions of the flow channels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00873—Heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00889—Mixing

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

Cette invention concerne un procédé de mise en contact d’une phase liquide et d’une seconde phase fluide, comprenant les étapes suivantes : amenée de la phase liquide et/ou de la seconde phase fluide dans un microcanal de procédé en contact avec des dispositifs de surface du microcanal, le contact des dispositifs de surface avec la phase liquide et/ou la seconde phase fluide perturbant l’écoulement de la phase ; mise en contact de la phase liquide avec la seconde phase fluide dans le microcanal ; et transfert de masse de la phase liquide à la seconde phase fluide et/ou de la seconde phase fluide à la phase liquide.
PCT/US2006/026682 2005-07-08 2006-07-07 Procédé de mise en contact multiphase à l’aide d’un dispositif de microcanal WO2007032810A2 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
EP06836085A EP1917099A2 (fr) 2005-07-08 2006-07-07 Procédé de mise en contact multiphase à l aide d un dispositif de microcanal
CA002613674A CA2613674A1 (fr) 2005-07-08 2006-07-07 Procede de mise en contact multiphase a l'aide d'un dispositif de microcanal

Applications Claiming Priority (8)

Application Number Priority Date Filing Date Title
US11/177,941 US7610775B2 (en) 2004-07-23 2005-07-08 Distillation process using microchannel technology
US11/177,941 2005-07-08
US72712605P 2005-10-13 2005-10-13
US60/727,126 2005-10-13
US73159605P 2005-10-27 2005-10-27
US60/731,596 2005-10-27
US78573206P 2006-03-23 2006-03-23
US60/785,732 2006-03-23

Publications (2)

Publication Number Publication Date
WO2007032810A2 WO2007032810A2 (fr) 2007-03-22
WO2007032810A3 true WO2007032810A3 (fr) 2007-06-21

Family

ID=37865416

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2006/026682 WO2007032810A2 (fr) 2005-07-08 2006-07-07 Procédé de mise en contact multiphase à l’aide d’un dispositif de microcanal

Country Status (3)

Country Link
EP (1) EP1917099A2 (fr)
CA (1) CA2613674A1 (fr)
WO (1) WO2007032810A2 (fr)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070246106A1 (en) * 2006-04-25 2007-10-25 Velocys Inc. Flow Distribution Channels To Control Flow in Process Channels
US8101048B2 (en) 2007-07-20 2012-01-24 Rohm And Haas Company Purification process using microchannel devices
EP2184103A1 (fr) * 2008-11-11 2010-05-12 Onea Engineering Austria GmbH Réacteur modulaire
US8435387B2 (en) 2008-11-14 2013-05-07 Massachusetts Institute Of Technology Small-scale method and apparatus for separating mixtures
WO2013074551A1 (fr) * 2011-11-14 2013-05-23 Biocee, Inc. Réacteurs continus à milieux poreux multiphases et leurs procédés d'utilisation
EP3034159B1 (fr) * 2014-12-18 2020-11-04 The Procter and Gamble Company Mélangeur statique et procédé pour mélanger des fluides
US10729600B2 (en) 2015-06-30 2020-08-04 The Procter & Gamble Company Absorbent structure
WO2017079599A1 (fr) 2015-11-04 2017-05-11 The Procter & Gamble Company Structure absorbante
BR112018009094A2 (pt) 2015-11-04 2018-11-06 Procter & Gamble estrutura absorvente
RU2018128214A (ru) 2016-01-27 2020-02-27 Кох-Глич, Лп Лопастное устройство ввода с внутренней балкой для обеспечения жесткости и содержащий его сосуд
CN109069946B (zh) 2016-04-28 2021-05-11 株式会社Ihi 分离装置
DE102021208923A1 (de) * 2021-08-13 2023-02-16 Ineratec Gmbh Plattenelement für reaktionsmodule oder -systeme
CN115031556A (zh) * 2022-08-11 2022-09-09 杭州沈氏节能科技股份有限公司 微通道换热器及微通道换热器的加工方法
CN117550670A (zh) * 2023-11-15 2024-02-13 中国计量大学 基于超疏水跨轨道阵列的高效气泡运输器、装置及制作方法

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0007106A1 (fr) * 1978-07-19 1980-01-23 BASF Aktiengesellschaft Procédé de préparation de polycondensats de cétones et d'aldéhydes à l'aide de catalyseurs de transfert de phase
US5800595A (en) * 1994-08-30 1998-09-01 William Allen Trusts Pty Ltd Spaced evaporative wicks within an air cooler
WO2001093976A2 (fr) * 2000-06-06 2001-12-13 Battelle Memorial Institute Separations capillaires de microsystemes
US20020144600A1 (en) * 2000-06-06 2002-10-10 Tegrotenhuis Ward E. Conditions for fluid separations in microchannels, capillary-driven fluid separations, and laminated devices capable of separating fluids
WO2003011443A2 (fr) * 2001-07-27 2003-02-13 President And Fellows Of Harvard College Appareil et procedes de melange de flux laminaires
US20030226806A1 (en) * 2002-06-11 2003-12-11 Young Lincoln C. Methods and devices for liquid extraction
EP1380337A2 (fr) * 2002-07-12 2004-01-14 Tosoh Corporation Dispositif à canaux minces et procédé chimique permettant son utilisation du dispositif avec des fluides
US20050082351A1 (en) * 2003-10-17 2005-04-21 Jmp Industries, Inc., An Ohio Corporation Micro-reactor fabrication
WO2006039568A1 (fr) * 2004-10-01 2006-04-13 Velocys Inc. Procede de melange multiphase par technologie de traitement a micro-canaux
WO2006053345A1 (fr) * 2004-11-12 2006-05-18 Velocys Inc. Procede utilisant la technologie de microcanal pour conduire une reaction d'alkylation ou d'acylation
WO2006102675A1 (fr) * 2005-03-23 2006-09-28 Velocys, Inc. Elements de surface dans la technologie microfluidique
WO2006110458A1 (fr) * 2005-04-08 2006-10-19 Velocys, Inc. Regulation de flux a travers des conduits de raccordement paralleles vers / en provenance d'un collecteur

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Publication number Priority date Publication date Assignee Title
US7250151B2 (en) 2002-08-15 2007-07-31 Velocys Methods of conducting simultaneous endothermic and exothermic reactions

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0007106A1 (fr) * 1978-07-19 1980-01-23 BASF Aktiengesellschaft Procédé de préparation de polycondensats de cétones et d'aldéhydes à l'aide de catalyseurs de transfert de phase
US5800595A (en) * 1994-08-30 1998-09-01 William Allen Trusts Pty Ltd Spaced evaporative wicks within an air cooler
WO2001093976A2 (fr) * 2000-06-06 2001-12-13 Battelle Memorial Institute Separations capillaires de microsystemes
US20020144600A1 (en) * 2000-06-06 2002-10-10 Tegrotenhuis Ward E. Conditions for fluid separations in microchannels, capillary-driven fluid separations, and laminated devices capable of separating fluids
WO2003011443A2 (fr) * 2001-07-27 2003-02-13 President And Fellows Of Harvard College Appareil et procedes de melange de flux laminaires
US20030226806A1 (en) * 2002-06-11 2003-12-11 Young Lincoln C. Methods and devices for liquid extraction
EP1380337A2 (fr) * 2002-07-12 2004-01-14 Tosoh Corporation Dispositif à canaux minces et procédé chimique permettant son utilisation du dispositif avec des fluides
US20050082351A1 (en) * 2003-10-17 2005-04-21 Jmp Industries, Inc., An Ohio Corporation Micro-reactor fabrication
WO2006039568A1 (fr) * 2004-10-01 2006-04-13 Velocys Inc. Procede de melange multiphase par technologie de traitement a micro-canaux
WO2006053345A1 (fr) * 2004-11-12 2006-05-18 Velocys Inc. Procede utilisant la technologie de microcanal pour conduire une reaction d'alkylation ou d'acylation
WO2006102675A1 (fr) * 2005-03-23 2006-09-28 Velocys, Inc. Elements de surface dans la technologie microfluidique
WO2006110458A1 (fr) * 2005-04-08 2006-10-19 Velocys, Inc. Regulation de flux a travers des conduits de raccordement paralleles vers / en provenance d'un collecteur

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
JOHNSON T J ET AL: "RAPID MICROFLUIDIC MIXING", 1 January 2002, ANALYTICAL CHEMISTRY, AMERICAN CHEMICAL SOCIETY. COLUMBUS, US, PAGE(S) 45-51, ISSN: 0003-2700, XP001108780 *

Also Published As

Publication number Publication date
EP1917099A2 (fr) 2008-05-07
WO2007032810A2 (fr) 2007-03-22
CA2613674A1 (fr) 2007-03-22

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