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WO2009011225A1 - ４－フルオロ－１，３－ジオキソラン－２－オンの製造方法 - Google Patents

４－フルオロ－１，３－ジオキソラン－２－オンの製造方法 Download PDF

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Publication number
WO2009011225A1
WO2009011225A1 PCT/JP2008/061971 JP2008061971W WO2009011225A1 WO 2009011225 A1 WO2009011225 A1 WO 2009011225A1 JP 2008061971 W JP2008061971 W JP 2008061971W WO 2009011225 A1 WO2009011225 A1 WO 2009011225A1
Authority
WO
WIPO (PCT)
Prior art keywords
dioxolan
fluoro
chloro
chlorine radicals
produced
Prior art date
Application number
PCT/JP2008/061971
Other languages
English (en)
French (fr)
Inventor
Akiyoshi Yamauchi
Michiru Tanaka
Meiten Koh
Original Assignee
Daikin Industries, Ltd.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Daikin Industries, Ltd. filed Critical Daikin Industries, Ltd.
Priority to CN200880024559.0A priority Critical patent/CN101743236B/zh
Publication of WO2009011225A1 publication Critical patent/WO2009011225A1/ja

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
    • C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
    • C07D317/32—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D317/42—Halogen atoms or nitro radicals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

　４－クロロ－１，３－ジオキソラン－２－オンを出発物質とし、これをフッ素化剤でフッ素化する製造方法において、高収率を維持しながら短時間で高純度の４－フルオロ－１，３－ジオキソラン－２－オンを製造できる製造方法を提供する。有機溶媒中にて、４－クロロ－１，３－ジオキソラン－２－オン１モルに対して、１．４モル以上のフッ素化剤を添加して反応させて塩素根を含む４－フルオロ－１，３－ジオキソラン－２－オンを得た後、必要に応じて中間処理工程を施し、さらに、得られた塩素根を含む４－フルオロ－１，３－ジオキソラン－２－オンを蒸留により精製することで、塩素根含有量が低減化された４－フルオロ－１，３－ジオキソラン－２－オンを製造する。
PCT/JP2008/061971 2007-07-13 2008-07-02 ４－フルオロ－１，３－ジオキソラン－２－オンの製造方法 WO2009011225A1 (ja)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN200880024559.0A CN101743236B (zh) 2007-07-13 2008-07-02 4-氟-1,3-二氧戊环-2-酮的制造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007-184442 2007-07-13
JP2007184442A JP5135926B2 (ja) 2007-07-13 2007-07-13 ４−フルオロ−１，３−ジオキソラン−２−オンの製造方法

Publications (1)

Publication Number Publication Date
WO2009011225A1 true WO2009011225A1 (ja) 2009-01-22

Family

ID=40259563

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/061971 WO2009011225A1 (ja) 2007-07-13 2008-07-02 ４－フルオロ－１，３－ジオキソラン－２－オンの製造方法

Country Status (4)

Country Link
JP (1) JP5135926B2 (ja)
KR (1) KR20100031552A (ja)
CN (1) CN101743236B (ja)
WO (1) WO2009011225A1 (ja)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102993160A (zh) * 2012-09-26 2013-03-27 中国海洋石油总公司 一种氟代碳酸乙烯酯的合成方法

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5358974B2 (ja) * 2008-02-28 2013-12-04 ダイキン工業株式会社 フッ素化１，３−ジオキソラン−２−オンの製造方法
TW201121938A (en) * 2009-09-28 2011-07-01 Solvay Fluor Gmbh Manufacture of difluoroethylene carbonate, trifluoroethylene carbonate and tetrafluoroethylene carbonate
CN102060838A (zh) * 2010-12-31 2011-05-18 浙江华晶氟化学科技有限公司 一种氟代碳酸乙烯酯的制备方法
CN106916136B (zh) * 2017-03-01 2019-06-14 山东永浩新材料科技有限公司 一种氟代碳酸乙烯酯的合成方法
CN110637001B (zh) * 2017-06-22 2022-05-27 日本瑞翁株式会社 八氟环戊烯的制造方法
CN110156743A (zh) * 2019-05-24 2019-08-23 泰兴华盛精细化工有限公司 一种氟代碳酸乙烯酯的合成方法
CN113402496B (zh) * 2021-07-07 2022-03-25 山东海科创新研究院有限公司 二甲基乙酰胺在制备氟代碳酸乙烯酯中的应用
CN114621177B (zh) * 2022-02-24 2023-04-07 浙江诺亚氟化工有限公司 一种氟代碳酸乙烯酯的制备方法
CN116425712A (zh) * 2023-03-10 2023-07-14 山东东岳高分子材料有限公司 一种4-氟-1,3-二氧戊环-2-酮的制备方法
CN117624110B (zh) * 2023-12-06 2024-05-03 珠海百川石化工程设计有限公司 一种氟代碳酸乙烯酯的合成方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007008826A (ja) * 2005-06-28 2007-01-18 Central Glass Co Ltd 高純度の４−フルオロ−１，３−ジオキソラン−２−オンの製造方法
JP2007008825A (ja) * 2005-06-28 2007-01-18 Central Glass Co Ltd 高純度の４−フルオロ−１，３−ジオキソラン−２−オンの製造方法
CN101066965A (zh) * 2007-06-01 2007-11-07 张家港市华盛化学有限公司 氟代环状碳酸酯的制备方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2267263A1 (en) * 1996-10-03 1998-04-09 National Research Council Of Canada Electrolyte comprising fluoro-ethylene carbonate and propylene carbonate, for alkali metal-ion secondary battery

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007008826A (ja) * 2005-06-28 2007-01-18 Central Glass Co Ltd 高純度の４−フルオロ−１，３−ジオキソラン−２−オンの製造方法
JP2007008825A (ja) * 2005-06-28 2007-01-18 Central Glass Co Ltd 高純度の４−フルオロ−１，３−ジオキソラン−２−オンの製造方法
CN101066965A (zh) * 2007-06-01 2007-11-07 张家港市华盛化学有限公司 氟代环状碳酸酯的制备方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102993160A (zh) * 2012-09-26 2013-03-27 中国海洋石油总公司 一种氟代碳酸乙烯酯的合成方法

Also Published As

Publication number Publication date
CN101743236B (zh) 2013-04-10
CN101743236A (zh) 2010-06-16
JP2009019019A (ja) 2009-01-29
JP5135926B2 (ja) 2013-02-06
KR20100031552A (ko) 2010-03-22

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