CN106349753A - Novel disperse dye composition - Google Patents
Novel disperse dye composition Download PDFInfo
- Publication number
- CN106349753A CN106349753A CN201610701405.7A CN201610701405A CN106349753A CN 106349753 A CN106349753 A CN 106349753A CN 201610701405 A CN201610701405 A CN 201610701405A CN 106349753 A CN106349753 A CN 106349753A
- Authority
- CN
- China
- Prior art keywords
- dye monomer
- dye
- dyestuff
- monomer
- disperse
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000000203 mixture Substances 0.000 title claims abstract description 6
- 239000000986 disperse dye Substances 0.000 title abstract description 4
- 239000000975 dye Substances 0.000 claims abstract description 110
- 239000000178 monomer Substances 0.000 claims abstract description 66
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 11
- 239000012535 impurity Substances 0.000 claims abstract description 4
- 239000007859 condensation product Substances 0.000 claims description 11
- -1 alkyl naphthalene sulfonic acid formaldehyde Chemical compound 0.000 claims description 6
- NVVZQXQBYZPMLJ-UHFFFAOYSA-N formaldehyde;naphthalene-1-sulfonic acid Chemical compound O=C.C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 NVVZQXQBYZPMLJ-UHFFFAOYSA-N 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 5
- 238000009833 condensation Methods 0.000 claims description 5
- 230000005494 condensation Effects 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- SRDOTWUOTQTGAK-UHFFFAOYSA-N C=O.C1(=CC=CC2=CC=CC=C12)S(=O)(=O)OCC1=CC=CC=C1 Chemical compound C=O.C1(=CC=CC2=CC=CC=C12)S(=O)(=O)OCC1=CC=CC=C1 SRDOTWUOTQTGAK-UHFFFAOYSA-N 0.000 claims description 4
- JSFUMBWFPQSADC-UHFFFAOYSA-N Disperse Blue 1 Chemical compound O=C1C2=C(N)C=CC(N)=C2C(=O)C2=C1C(N)=CC=C2N JSFUMBWFPQSADC-UHFFFAOYSA-N 0.000 claims description 4
- YDEXUEFDPVHGHE-GGMCWBHBSA-L disodium;(2r)-3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Na+].[Na+].COC1=CC=CC(C[C@H](CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O YDEXUEFDPVHGHE-GGMCWBHBSA-L 0.000 claims description 4
- 239000012467 final product Substances 0.000 claims description 4
- WFFKSTRPZWRBEW-UHFFFAOYSA-N n-[2-[(2-bromo-4,6-dinitrophenyl)diazenyl]-5-(diethylamino)phenyl]acetamide Chemical compound CC(=O)NC1=CC(N(CC)CC)=CC=C1N=NC1=C(Br)C=C([N+]([O-])=O)C=C1[N+]([O-])=O WFFKSTRPZWRBEW-UHFFFAOYSA-N 0.000 claims description 4
- 239000000047 product Substances 0.000 claims description 4
- MWMJPPMTXZJLIK-UHFFFAOYSA-N 3-[4-[(2,6-dibromo-4-nitrophenyl)diazenyl]-n-ethylanilino]propanenitrile Chemical compound C1=CC(N(CCC#N)CC)=CC=C1N=NC1=C(Br)C=C([N+]([O-])=O)C=C1Br MWMJPPMTXZJLIK-UHFFFAOYSA-N 0.000 claims description 3
- 229920001732 Lignosulfonate Polymers 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 239000002131 composite material Substances 0.000 claims description 2
- 239000006185 dispersion Substances 0.000 claims 3
- 239000002671 adjuvant Substances 0.000 claims 2
- 238000004043 dyeing Methods 0.000 abstract description 6
- 239000000463 material Substances 0.000 abstract description 5
- 229920000728 polyester Polymers 0.000 abstract description 5
- 238000000859 sublimation Methods 0.000 abstract description 3
- 230000008022 sublimation Effects 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 238000005406 washing Methods 0.000 abstract description 2
- 239000004615 ingredient Substances 0.000 abstract 1
- 230000008018 melting Effects 0.000 abstract 1
- 238000002844 melting Methods 0.000 abstract 1
- 239000004744 fabric Substances 0.000 description 7
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 6
- 239000004753 textile Substances 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- QLRDACXDRLGLOC-UHFFFAOYSA-N 2-[n-(2-cyanoethyl)-4-[(4-nitrophenyl)diazenyl]anilino]ethyl acetate Chemical compound C1=CC(N(CCC#N)CCOC(=O)C)=CC=C1N=NC1=CC=C([N+]([O-])=O)C=C1 QLRDACXDRLGLOC-UHFFFAOYSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- WODGMMJHSAKKNF-UHFFFAOYSA-N 2-methylnaphthalene-1-sulfonic acid Chemical compound C1=CC=CC2=C(S(O)(=O)=O)C(C)=CC=C21 WODGMMJHSAKKNF-UHFFFAOYSA-N 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 239000002270 dispersing agent Substances 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 238000011056 performance test Methods 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 241000158728 Meliaceae Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- NYGZLYXAPMMJTE-UHFFFAOYSA-M metanil yellow Chemical group [Na+].[O-]S(=O)(=O)C1=CC=CC(N=NC=2C=CC(NC=3C=CC=CC=3)=CC=2)=C1 NYGZLYXAPMMJTE-UHFFFAOYSA-M 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 238000009970 yarn dyeing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0046—Mixtures of two or more azo dyes
- C09B67/0051—Mixtures of two or more azo dyes mixture of two or more monoazo dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/008—Preparations of disperse dyes or solvent dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/82—Textiles which contain different kinds of fibres
- D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
- D06P3/8223—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups
- D06P3/8228—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using one kind of dye
- D06P3/8233—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using one kind of dye using dispersed dyes
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Abstract
The invention relates to a novel disperse dye composition, which comprises the following ingredients in percentage by weight: 0.5 to 75 percent of dye monomers A shown as a formula (I), 0.5 to 75 percent of dye monomers B shown as a formula (II), 0.5 to 40 percent of dye monomers C shown as a formula (III), 0.5 to 60 percent of dye monomers D shown as a formula (IV) and the balance of conventional auxiliary agents and unavoidable impurities. The novel scattered dye composition is applicable to the dyeing of polyester materials; the dyeing rate is high; a better environment-friendly effect is achieved; the high-temperature hot melting dyeing performance is very good; the firmness performance is good, for example, the sun-burning resistant firmness, sublimation resistant firmness and the washing resistant firmness are very high.
Description
Technical field
The present invention relates to a kind of Novel disperse dyestuff compositionss, especially a kind of monoazo class dye composite.
Background technology
Since the textile industry of China has added since wto organizes and cancel textile limit, chemical fibre, yarn, cloth, textile etc.
Yield all ranks first in the world, and the yield of wherein fiber accounts for the 50% of the whole world, and textile industry is further to the demand of dyestuff
Increase, along with the different demands to various dyeing fabric effects for the people, the suitable dyestuff of selection to meet the requirement of client is
Put a difficult problem urgently to be resolved hurrily in face of DYE PRODUCTION business.As some medium-to-high grade fabrics both domestic and external, including polyester blended fabric etc.,
The disperse dyes supplied in the market, can't meet the printing and dyeing needs of such textile well.
Content of the invention
For the problems referred to above, the present invention provides a kind of dye-uptake height, washing fastness is good, fastness is excellent, resistance to thermal mobility
Little Novel disperse dyestuff compositionss, are suitable to multifilament fabric, such as polyester blended fabric etc..
For solving above technical problem, the present invention is achieved through the following technical solutions:
A kind of Novel disperse dyestuff compositionss, containing following components in percentage by weight:
0.5～75% dye monomer a, 0.5～75% dye monomer b, 0.5～40% dye monomer c, 0.5～
60% dye monomer d；
Wherein, shown in the molecular structure such as formula (i) of described dye monomer a,
Shown in the molecular structure of described dye monomer b such as formula (),
Shown in the molecular structure of described dye monomer c such as formula (),
Shown in the molecular structure of described dye monomer d such as formula (),
Due to the particularity of dye industry, it is difficult to also there is no need to make sterling, generally typically can make with some
During produce a small amount of impurity.Each component of the present invention can scope is deployed in proportion disperse dyes and coloured light by black
Color is extremely dark blue.
As further, preferably, described Novel disperse dyestuff compositionss are composed of the following components: 5～25% dyestuff list
Body a, 5～25% dye monomer b, 5～20% dye monomer c, 5～25% dye monomer d, and the routine of convention amount helps
Agent.
As alternative preferably, described Novel disperse dyestuff compositionss are composed of the following components: 0.5～25% dyestuff
Monomer a, 0.5～20% dye monomer b, 10～40% dye monomer c, 15～45% dye monomer d, balance of routine helps
Agent and inevitable impurity.
As further preferably, described auxiliary agent is dyestuff used additives, can be such as one of following or two or more any
The mixture of ratio: naphthalene sulfonic acid-formaldehyde condensation product, alkyl naphthalene sulfonic acid formaldehyde condensation products, lignosulfonates, benzyl naphthalene sulfonate
Formaldehyde condensation products；Described naphthalene sulfonic acid-formaldehyde condensation product such as diffusant nno, alkyl naphthalene sulfonic acid formaldehyde condensation products such as diffusant cnf, wood
Mahogany sulfonate such as sodium lignin sulfonate.
As further, preferably, described dye monomer a, dye monomer b, dye monomer c, dye monomer d are respectively adopted
The commercially available prod such as former dyestuff of c.i. disperse orange 31 of Zhejiang Bo Ao dye industry company limited production, the former dye of c.i. disperse orange 61
Material, the former dyestuff of c.i. disperse violet 93, the former dyestuff of c.i. disperse blue 291:1.
Above-mentioned Novel disperse dyestuff compositionss can be made up of following steps: by described dye monomer a, dye monomer b, dye
Material list body c, dye monomer d and auxiliary agent mixing, then be ground disperseing, then it is spray-dried, obtain final product.Or, by described dyestuff
Monomer a, dye monomer b, dye monomer c, dye monomer d are mixed into finished product dyestuff with part of auxiliary respectively, then by finished product dyestuff
Mixing portion auxiliary agent is ground disperseing, and is then spray-dried, obtains final product.
The present invention has a following positive beneficial effect:
Novel disperse dyestuff compositionss of the present invention are highly suitable for contaminating polyester material, yarn dyeing and stamp, high temperature pad-dry-cure dyeing
Performance is good, and dye uptake is high, fastness function admirable, and such as sunlight fastness, fastness to sublimation, wash resistant fastness are all splendid.
Specific embodiment
With reference to specific embodiment, the invention will be further described, but protection scope of the present invention is not limited to this.
Test method in following embodiments, if no special instructions, is conventional method；In following embodiments test material used and
Reagent, if no special instructions, is purchased from conventional chemical reagent shop.
Embodiment 1～8
According to continuous data shown in table 1, by dye monomer a (the former dyestuff of c.i. disperse orange 31), (c.i. divides dye monomer b
Dissipate orange 61 former dyestuffs), dye monomer c (the former dyestuff of c.i. disperse violet 93), dye monomer d (the former dyestuff of c.i. disperse blue 291:1),
Auxiliary agent (dispersant mf (condensation compound of methyl naphthalene sulfonic acid and formaldehyde), diffusant cnf (benzyl naphthalenesulfonate formaldehyde condensation compound), diffusant
Nno (naphthalene sulfonic acid-formaldehyde condensation product), sodium lignin sulfonate) after the blending that adds water, it is ground disperseing with grinder, spray drying is
Can.
Table 1 embodiment 1～8 component is measured
Example 9～16
According to continuous data shown in table 2, by c.i. disperse orange 31, (commercial dye, monomer a content is 50%, and remaining is to help
Agent), c.i. disperse orange 61 (commercial dye, monomer b content is 50%, and remaining is auxiliary agent), c.i. disperse violet 93 (commercial dye,
Monomer c content be 50%, remaining be auxiliary agent), c.i. disperse blue 291:1 (commercial dye, monomer d content be 50%, remaining be help
Agent), auxiliary agent (dispersant mf (condensation compound of methyl naphthalene sulfonic acid and formaldehyde), diffusant cnf (benzyl naphthalenesulfonate formaldehyde condensation compound), expand
Powder nno (naphthalene sulfonic acid-formaldehyde condensation product), sodium lignin sulfonate) after the blending that adds water, it is ground disperseing with grinder, spray dried
Dry.
Table 2 embodiment 9～16 component is measured
Performance test:
The Novel disperse dyestuff compositionss respectively taking 0.5 gram of embodiment 1～16 to be obtained, are dispersed in 500 milliliters of water, draw
Mix with 60 milliliters of water after 20 milliliters.Adjust dye bath ph=5 with acetic acid, be warming up to 70 DEG C and put into 2 grams of polyester cotton cloth simultaneously and contaminated
Color, in 30 minutes, temperature rises to 130 DEG C by 70 DEG C, is incubated 30 minutes, starts to sample when being cooled to 90 DEG C.Using GB gb/
T3921-1997, gb/t3920-1997, gb/t8427-1998, gb/t5718-1997. test that it is water-fastness respectively, rub resistance,
Color fastness to light and sub-limation fastness, test result is shown in Table 3.
Table 3 embodiment 1～16 the performance test results
Claims (7)
1. a kind of Novel disperse dyestuff compositionss are it is characterised in that contain following components in percentage by weight: 0.5～75%
Dye monomer a, 0.5～75% dye monomer b, 0.5～40% dye monomer c, 0.5～60% dye monomer d；
Wherein, shown in the molecular structure such as formula (i) of described dye monomer a,
Shown in the molecular structure of described dye monomer b such as formula (),
Shown in the molecular structure of described dye monomer c such as formula (),
Shown in the molecular structure of described dye monomer d such as formula (),
2. Novel disperse dyestuff compositionss according to claim 1 are it is characterised in that composed of the following components: 5～25%
Dye monomer a, 5～25% dye monomers
B, 5～20% dye monomer c, 5～25% dye monomer d, and conven-tional adjuvants.
3. Novel disperse dyestuff compositionss according to claim 1 are it is characterised in that composed of the following components: 0.5～
25% dye monomer a, 0.5～20% dye monomer
B, 10～40% dye monomer c, 15～45% dye monomer d, balance of conven-tional adjuvants and inevitable impurity.
4. the Novel disperse dyestuff compositionss according to any one of claims 1 to 3 it is characterised in that: under described auxiliary agent is
One of row or the mixture of two or more arbitrary proportion: naphthalene sulfonic acid-formaldehyde condensation product, alkyl naphthalene sulfonic acid formaldehyde condensation products, lignin
Sulfonate, benzyl naphthalenesulfonate formaldehyde condensation compound.
5. Novel disperse dyestuff compositionss according to claim 4 it is characterised in that: described naphthalene sulfonic acid-formaldehyde condensation product is
Diffusant nno, described alkyl naphthalene sulfonic acid formaldehyde condensation products are diffusant cnf, and described lignosulfonates are sodium lignin sulfonate.
6. the Novel disperse dyestuff compositionss according to any one of claims 1 to 3 it is characterised in that: described dye monomer
A, dye monomer b, dye monomer c, dye monomer d are respectively adopted the c.i. dispersion of Zhejiang Bo Ao dye industry company limited production
Orange 31 former dyestuffs, the former dyestuff of c.i. disperse orange 61, the former dyestuff of c.i. disperse violet 93, the former dyestuff of c.i. disperse blue 291:1.
7. the Novel disperse dyestuff compositionss according to any one of claims 1 to 3 it is characterised in that: above-mentioned new dispersion
Dye composite can be made up of following steps: by described dye monomer a, dye monomer b, dye monomer c, dye monomer d and
Auxiliary agent mixes, then is ground disperseing, and is then spray-dried, obtains final product；Or, by described dye monomer a, dye monomer b, dyestuff
Monomer c, dye monomer d are mixed into finished product dyestuff with part of auxiliary respectively, then finished product dyestuff mixing portion auxiliary agent is ground
Dispersion, is then spray-dried, obtains final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610701405.7A CN106349753A (en) | 2016-08-22 | 2016-08-22 | Novel disperse dye composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610701405.7A CN106349753A (en) | 2016-08-22 | 2016-08-22 | Novel disperse dye composition |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106349753A true CN106349753A (en) | 2017-01-25 |
Family
ID=57844403
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610701405.7A Pending CN106349753A (en) | 2016-08-22 | 2016-08-22 | Novel disperse dye composition |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106349753A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112080159A (en) * | 2020-09-03 | 2020-12-15 | 曹云渊 | Environment-friendly disperse black dye composition and mixing device thereof |
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Application publication date: 20170125 |
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