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WO2002038350A1 - Procede de transformation de dechets de caoutchouc - Google Patents

Procede de transformation de dechets de caoutchouc Download PDF

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Publication number
WO2002038350A1
WO2002038350A1 PCT/RU2001/000471 RU0100471W WO0238350A1 WO 2002038350 A1 WO2002038350 A1 WO 2002038350A1 RU 0100471 W RU0100471 W RU 0100471W WO 0238350 A1 WO0238350 A1 WO 0238350A1
Authority
WO
WIPO (PCT)
Prior art keywords
products
mixture
gas
activation
steam
Prior art date
Application number
PCT/RU2001/000471
Other languages
English (en)
Russian (ru)
Inventor
Dmitry Viktorovich Aristarkhov
Gennady Ivanovich Zhuravsky
Nikolai Nikolaevich Egorov
Valery Pavlovich Saenko
Original Assignee
Dmitry Viktorovich Aristarkhov
Gennady Ivanovich Zhuravsky
Nikolai Nikolaevich Egorov
Valery Pavlovich Saenko
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dmitry Viktorovich Aristarkhov, Gennady Ivanovich Zhuravsky, Nikolai Nikolaevich Egorov, Valery Pavlovich Saenko filed Critical Dmitry Viktorovich Aristarkhov
Priority to AU2002217640A priority Critical patent/AU2002217640A1/en
Publication of WO2002038350A1 publication Critical patent/WO2002038350A1/fr

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
    • B29B17/04—Disintegrating plastics, e.g. by milling
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/02—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
    • B29B17/04—Disintegrating plastics, e.g. by milling
    • B29B2017/0424—Specific disintegrating techniques; devices therefor
    • B29B2017/0496—Pyrolysing the materials
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2021/00—Use of unspecified rubbers as moulding material
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/62—Plastics recycling; Rubber recycling

Definitions

  • the waste of this method is a high waste of energy for processing, which is caused by a high temperature (up to 1500 ° C), which is more expensive.
  • gaz ⁇ b ⁇ azny ⁇ ⁇ du ⁇ v ⁇ azl ⁇ zheniya che ⁇ ez sl ⁇ y ⁇ d ⁇ v ⁇ i i ⁇ mass ⁇ v ⁇ m s ⁇ n ⁇ shenii (0.05 - 1.62): 1, and ⁇ ve ⁇ dye ⁇ du ⁇ y ⁇ azl ⁇ zheniya smeshivayu ⁇ ⁇ bemnymi with 4-40% oil and ⁇ essuyu ⁇ in b ⁇ i ⁇ e ⁇ y ⁇ i ⁇ dn ⁇ v ⁇ emenn ⁇ m nag ⁇ evanii d ⁇ ⁇ 100-500 ° C ⁇ u ⁇ em gas filtration, resulting from the separation of oil from gaseous products of the disposal of products.
  • ned ⁇ s ⁇ a ⁇ am ⁇ g ⁇ s ⁇ s ⁇ ba sledue ⁇ ⁇ nes ⁇ i b ⁇ lsh ⁇ y specific ⁇ as ⁇ d v ⁇ dyan ⁇ g ⁇ ⁇ a ⁇ a, vys ⁇ y ⁇ as ⁇ d ene ⁇ gii, ⁇ busl ⁇ vlenny ne ⁇ b ⁇ dim ⁇ s ⁇ yu nag ⁇ eva ⁇ a ⁇ a d ⁇ 1600 ° C, and ⁇ a ⁇ zhe b ⁇ lylie vyb ⁇ sy in a ⁇ m ⁇ s ⁇ e ⁇ u ⁇ du ⁇ v sg ⁇ aniya ⁇ liva, ⁇ as ⁇ duem ⁇ g ⁇ on ⁇ izv ⁇ ds ⁇ v ⁇ and ⁇ e ⁇ eg ⁇ ev v ⁇ dyan ⁇ g ⁇ ⁇ a ⁇ a.
  • the objective of the proposed invention is to reduce energy consumption and to reduce the amount of foreign gas by-products in the process environment.
  • reaction (2) for 36 g of steam, 44 g of C 2 and 4 g of 2 are processed and 12 g of carbon are consumed.
  • the process of activating the reaction can be regulated by various factors, for example, by changing the activity and the timing of the activity, and by doing so ⁇ sleds ⁇ vie ⁇ eguli ⁇ vaniya ⁇ e ⁇ aniya ⁇ ea ⁇ tsy a ⁇ ivi ⁇ vaniya ⁇ eguli ⁇ ue ⁇ sya s ⁇ s ⁇ av ⁇ a ⁇ gaz ⁇ v ⁇ y mixture in ⁇ uyu v ⁇ dya ⁇ v ⁇ dyan ⁇ y ⁇ a ⁇ , v ⁇ d ⁇ d, ⁇ sid ugle ⁇ da, di ⁇ sid ugle ⁇ da and neb ⁇ ly ⁇ ie ⁇ liches ⁇ va me ⁇ ana, se ⁇ v ⁇ d ⁇ da and ⁇ a ⁇ zhe gaz ⁇ b ⁇ azny ⁇ ⁇ du ⁇ v ⁇ azl ⁇ zheniya ⁇ ezin ⁇ vy ⁇ ⁇ d ⁇ v, ⁇ ye not been isolated in ⁇ ea ⁇ e ⁇ i ⁇ e ⁇ mic
  • the process uses a gas and vapor medium (mixture), as well as the products of gas combustion in the treatment town.
  • the necessary inactive gas mixture for the heating in the process chamber 1 is divided into the temperature and the temperature of the mixture.
  • the higher the specific heat of the mixture the smaller the quantity of the mixture needed for the specified quantity of heat and the given temperature.
  • the specific gravity of the mixture is divided by its composition, i.e. The components that are included in 4
  • a further increase in the degree of vaporization of the vapor in the mixture leads to a slight increase in the rate of the mixture’s consumption, and the cost (energy) of the vapors of the vapor.
  • the other way round is to keep the steam in the mixture free of heat, that is to say, it doesn’t need to be heated. the excess mixture cannot be burnt in town 12 and should be discharged in the atmosphere (the mixture contains C ⁇ ).
  • the required mass ratio in the mixture should be kept in the range of (3.0 - 0.6): 1 (dry gas vapor).
  • the activation of the product must be carried out in the amount of 0.8 - 1.6 kg of steam per 1 kg of spreading products.
  • P ⁇ dacha ⁇ a ⁇ a in ⁇ liches ⁇ ve b ⁇ lshem 1.6 ⁇ g ⁇ a ⁇ a 1 ⁇ g ⁇ du ⁇ v ⁇ azl ⁇ lseniya ⁇ iv ⁇ di ⁇ ⁇ ⁇ s ⁇ u udeln ⁇ g ⁇ ⁇ as ⁇ da ⁇ a ⁇ a on ⁇ tsess ( ⁇ s ⁇ u ene ⁇ g ⁇ za ⁇ a ⁇ on ⁇ tsess) ⁇ davleniyu ⁇ tsess a ⁇ ivi ⁇ vaniya ⁇ ve ⁇ dy ⁇ ⁇ du ⁇ v ⁇ azl ⁇ lseniya.
  • Rubber discharges in the amount of 0.05-0.20 kg of waste per 1 kg of discharged products Rubber discharges in the amount of 0.05-0.20 kg of waste per 1 kg of discharged products.
  • Fig. 1 the installation diagram is presented, at a short time we will implement methods of processing rubber products.
  • the installation of the appliance is equipped with a steam generator 7 with a control unit for steam 8, a cooler 9 with an engine and a screw 10, a furnace 11 with a heater 12 and 15, 14; carbon 13, condensate 19, with carbon 26, a separator for separating the acid phase 21, carbon 22, 23, 25; a container for oil (liquid food products) 24; ⁇ anom 26; the supply of water to the vapor mixture in a vapor mixture 27; temperature sensors in activation furnace 28; active coal tank 29; active temperature sensors 30; Tank 32 of the dispensing of the vapor-gas mixture in the process chamber; With a good return of rubber products 33 with a screw 34 and an engine 35. 6
  • the processing of rubber products is subject to the following process.
  • the screw 6 is activated, but it starts to move the camera 1.
  • P ⁇ dya che ⁇ ez ⁇ ubash ⁇ u 16 ⁇ du ⁇ y sg ⁇ aniya ⁇ i ⁇ dn ⁇ g ⁇ gas nag ⁇ evayu ⁇ s ⁇ en ⁇ i ⁇ ame ⁇ y 1.
  • E ⁇ ⁇ zv ⁇ lyae ⁇ ⁇ lezn ⁇ is ⁇ lz ⁇ va ⁇ ⁇ e ⁇ l ⁇ ⁇ ab ⁇ avshi ⁇ in ⁇ echi a ⁇ ivatsii ⁇ du ⁇ v sg ⁇ aniya gas.
  • the discharged water vapor through the feed of the gas mixture 17 is fed into the processing chamber 1.
  • the oil from the steam unit 21 through crane 23 is supplied to the generator at all, and the oil is discharged through the tank 25 and the waste oil is drained through the tank 25. 7
  • Condensable gas products from the condensate 19 through valve 26 are delivered to the city 12 and used to provide energy for the activation furnace. With this, with a cover of 13, the gas supply to town 12 is prevented.
  • the vapor-gas mixture in the process chamber 1 is fed at a temperature of 800-1000 ° C, and it is discharged at a temperature of 300-400 ° C.
  • P ⁇ i e ⁇ m ⁇ em ⁇ e ⁇ a ⁇ u ⁇ u vyv ⁇ dim ⁇ y ⁇ a ⁇ gaz ⁇ v ⁇ y mixture ⁇ n ⁇ li ⁇ uyu ⁇ ⁇ ⁇ azaniyam da ⁇ chi ⁇ a ⁇ em ⁇ e ⁇ a ⁇ u ⁇ y 31.
  • Activation ovens by operating high temperature rubber products are suitable for solid and gaseous products. Other products are activated, and gas mixtures are mixed with water and activation gases, and such a gas-oil mixture is generated (oil-containing gas).
  • This quantity of heat is dispensed with a vapor-gas mixture (at the time of restarting the appliance, it must be discharged with a quick food).
  • City 12 of the activation furnace through the gas 13 delivers natural gas with a discharge of 3.28 kg / h and burns it.
  • the furnace 11 is equipped with a speed of 1 rpm.
  • the products of the combustion of natural gas from the furnace 11 in the amount of 47.5 m / h at a temperature of 400 ° C are discharged into the heating chamber 16 of the chamber 1. After using the 16 tank, the combustion gases of the primary gas are heated by the chamber 1. This will reduce the risk of use and the use of the product.
  • the shipments from the steam generator 21 are delivered through steam 23 to the steam generator as fuel.
  • the fuel is disposed of by the waste of the steam.
  • Condensable gas products for the disposal of goods in the amount of 12 kg / h from the condenser 19 through the crane 26 are supplied to the city 12 and are used. At the same time, with the control of 13, the gas supply to the city is 12.
  • pressure 8 changes the flow rate of the steam (decrease by 1). sets the waste water rate of 91.8 kg / h.
  • the gas-vapor mixture has the following capacities:
  • an activated mixture of 130099, 5 kJ / h of heat is required to be activated.
  • a vapor-gas mixture is supplied at a temperature of 1000 ° C, and gaseous process products are discharged from the following by-product
  • the 1 feeds the vapor mixture with 93.4 kg / h and the excess (93 b / h) Activation furnace 12.
  • the specific rate of combustion of a vapor-gas mixture is 4400 cdls / kg.
  • the process in the process chamber 1 emits the gas separation With a speed of 33 with a screw 34 and a motor of 35, activation 11 delivers rubber products in the amount of 11.6 kg / h (0.2 kg of waste for 1 unit).
  • the activation of high temperature products involves the use of rubber products in solid and gaseous products (6.7 kg in the manufacture of gas by-products).
  • EXAMPLE 2 In the chamber, 1 through the bunker with 3 gate locks and 4, 200 kg of ground shredders are supplied with 200-300 mm of loose tire. 14
  • City 12 of the furnace of activation through crane 13 delivers natural gas with a discharge of 6.56 kg / h and uses it.
  • the furnace 11 is equipped with a rotational speed of 2 rpm.
  • the products of the combustion of natural gas from the furnace 11 in the amount of 95 m 3 / h are discharged into the heating chamber 16 of the process chamber 1. After the appliance 16, the products of the combustion of the natural gas are heated by the chamber 1, that is, in the case of a waste of 418
  • the shipments from the steam generator 21 are delivered through steam 23 to the steam generator as fuel.
  • the fuel is disposed of by the waste of the steam. 16
  • Condensable gas products for the disposal of products in the amount of 10 kg / h from the condensate 19 through the crane 26 are fed to the city 12 and burned. At the same time, with the control of 13, the gas supply to the city is 12.
  • volume 8 changes the flow rate of the steam (decrease by
  • the gas-vapor mixture has the following capacities:
  • ⁇ 300 ° ⁇ .
  • the temperature of the coal is observed at the indications of sensor 30.
  • the cooling system is used for heating the steam and the temperature.
  • the heaters are used for the following:
  • the process chamber 1 delivers gas-based rubber products that contain oil in the form of a vapor.
  • the unit receives 11 rubber products in the amount of 5 kg / hour (0.05 kg of output for 1 unit).
  • the activation of high temperature products involves the use of rubber products in solid and gaseous products (2.5 kg of solid products and 2.5 gaseous products).
  • Resetting the device to a dry environment may cause the process to be inactive, and the system may not run out of power.

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Furnace Details (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Processing Of Solid Wastes (AREA)
  • Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)

Abstract

L'invention relève de la transformation des déchets et peut s'utiliser en industrie chimique pour produire des adsorbants, de même que dans l'industrie du caoutchouc pour obtenir des ingrédients de mélanges de caoutchouc et en industrie énergétique à des fins de réutilisation des déchets dans la production de l'énergie. L'invention permet de réduire la consommation d'énergie et les émissions de déchets dans l'atmosphère lors du traitement des déchets. On connaît des procédés de traitement des déchets de caoutchouc qui présentent des inconvénients tels qu'une consommation d'énergie élevée et d'importantes émissions de déchets dans l'atmosphère. L'invention permet de résoudre ces problèmes; selon l'invention, les produits de décomposition solides sont alimentés dans un four d'activation où l'on injecte simultanément de la vapeur d'eau en quantités égales à 0,8 - 1,6 kg de vapeur pour 1 kg de produits de décomposition solides; le mélange gazeux provenant du four d'activation est évacué avec une proportion égale à (3 - 0,6): 1 de la vapeur d'eau et des gaz d'activation. Le tout est réutilisé en tant que milieu gaz-vapeur à des fins de décomposition thermique des déchets. En outre, on alimente dans le four d'activation, conjointement avec les produits de décomposition solides et la vapeur d'eau, des déchets de caoutchouc, en quantités égales à 0,05 - 0,20 kg de déchets pour 1 kg de produits de décomposition solides.
PCT/RU2001/000471 2000-11-09 2001-11-09 Procede de transformation de dechets de caoutchouc WO2002038350A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AU2002217640A AU2002217640A1 (en) 2000-11-09 2001-11-09 Method for reprocessing rubber waste

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
RU2000127875 2000-11-09
RU2000127875A RU2174911C1 (ru) 2000-11-09 2000-11-09 Способ переработки резиновых отходов

Publications (1)

Publication Number Publication Date
WO2002038350A1 true WO2002038350A1 (fr) 2002-05-16

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/RU2001/000471 WO2002038350A1 (fr) 2000-11-09 2001-11-09 Procede de transformation de dechets de caoutchouc

Country Status (3)

Country Link
AU (1) AU2002217640A1 (fr)
RU (1) RU2174911C1 (fr)
WO (1) WO2002038350A1 (fr)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004076595A1 (fr) * 2003-02-25 2004-09-10 Dmitry Viktorovich Aristarkhov Procede de recyclage de dechets de caoutchouc
US10053628B2 (en) 2013-03-08 2018-08-21 Alpha Recyclage Franche Comte Method for treating carbonaceous materials by vapor thermolysis

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2276170C2 (ru) * 2004-04-29 2006-05-10 Закрытое акционерное общество НПФ "ЭКОТЕХ" Способ получения сажи из резиновых отходов
RU2283761C2 (ru) * 2004-11-15 2006-09-20 Закрытое акционерное общество НПФ "ЭКОТЕХ" Устройство для переработки органических отходов
RU2287484C1 (ru) * 2005-06-06 2006-11-20 Открытое акционерное общество "Татнефть" им. В.Д. Шашина Способ получения сорбента органических соединений
RU2296709C1 (ru) * 2005-09-16 2007-04-10 Алексей Викторович Матвеев Установка получения гранулированного углеродного сорбента
RU2305032C1 (ru) * 2005-11-22 2007-08-27 Сергей Владимирович Горбунов Устройство для переработки отходов
RU2299806C1 (ru) * 2005-11-22 2007-05-27 Сергей Владимирович Горбунов Способ переработки отходов
RU2361151C2 (ru) * 2007-07-31 2009-07-10 Владимир Юрьевич Пименов Установка для переработки органического сырья в топливные компоненты
RU2602147C2 (ru) * 2011-04-14 2016-11-10 Альфа Ресиклаж Франш Комте Способ и устройство получения сажи из резиновых отходов
RU2502596C2 (ru) * 2012-03-15 2013-12-27 Закрытое Акционерное Общество "Научно-Производственное Объединение Инноватех" Способ переработки резиновых отходов
RU2659247C1 (ru) * 2017-03-20 2018-06-29 Сергей Павлович Сусеков Способ переработки резиносодержащих отходов

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1504169A (en) * 1974-05-14 1978-03-15 Piovanelli Macch Impianti Method for reclaiming cured rubber scraps
WO1995014562A1 (fr) * 1993-11-25 1995-06-01 Boris Konstantinovich Muslin Procede de retraitement d'enveloppes de pneu use et son equipement de mise en ×uvre
WO1995015840A1 (fr) * 1993-12-09 1995-06-15 Science-Technical And Product-Innovative Center 'tokema' Procede de recyclage de dechets de caoutchouc
RU2076501C1 (ru) * 1995-05-15 1997-03-27 Акционерное общество закрытого типа "РОБЕНТЕХ" Способ переработки резиновых отходов

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1504169A (en) * 1974-05-14 1978-03-15 Piovanelli Macch Impianti Method for reclaiming cured rubber scraps
WO1995014562A1 (fr) * 1993-11-25 1995-06-01 Boris Konstantinovich Muslin Procede de retraitement d'enveloppes de pneu use et son equipement de mise en ×uvre
WO1995015840A1 (fr) * 1993-12-09 1995-06-15 Science-Technical And Product-Innovative Center 'tokema' Procede de recyclage de dechets de caoutchouc
RU2076501C1 (ru) * 1995-05-15 1997-03-27 Акционерное общество закрытого типа "РОБЕНТЕХ" Способ переработки резиновых отходов

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
V.M. MAKAROV ET AL.: "Ispolzovanie amortizovannykh shin I otkhodov proizvodstv rezinovykh izdely", 1986, LENINGRAD, KHIMYA, pages 216 - 218 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004076595A1 (fr) * 2003-02-25 2004-09-10 Dmitry Viktorovich Aristarkhov Procede de recyclage de dechets de caoutchouc
US10053628B2 (en) 2013-03-08 2018-08-21 Alpha Recyclage Franche Comte Method for treating carbonaceous materials by vapor thermolysis

Also Published As

Publication number Publication date
RU2174911C1 (ru) 2001-10-20
AU2002217640A1 (en) 2002-05-21

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