WO2018141791A1 - Procédé amélioré - Google Patents
Procédé amélioré Download PDFInfo
- Publication number
- WO2018141791A1 WO2018141791A1 PCT/EP2018/052393 EP2018052393W WO2018141791A1 WO 2018141791 A1 WO2018141791 A1 WO 2018141791A1 EP 2018052393 W EP2018052393 W EP 2018052393W WO 2018141791 A1 WO2018141791 A1 WO 2018141791A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- vitamin
- alginate
- process according
- gel
- gum
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 39
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims abstract description 82
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims abstract description 43
- 229930003268 Vitamin C Natural products 0.000 claims abstract description 43
- 235000019154 vitamin C Nutrition 0.000 claims abstract description 43
- 239000011718 vitamin C Substances 0.000 claims abstract description 43
- 239000000203 mixture Substances 0.000 claims abstract description 28
- 238000009472 formulation Methods 0.000 claims abstract description 18
- 150000003700 vitamin C derivatives Chemical class 0.000 claims abstract description 17
- 150000001875 compounds Chemical class 0.000 claims description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
- 241000238557 Decapoda Species 0.000 claims description 15
- 241000251468 Actinopterygii Species 0.000 claims description 14
- 239000007921 spray Substances 0.000 claims description 14
- 239000000499 gel Substances 0.000 claims description 12
- 239000000725 suspension Substances 0.000 claims description 12
- 229920001817 Agar Polymers 0.000 claims description 11
- 108010010803 Gelatin Proteins 0.000 claims description 11
- MIJPAVRNWPDMOR-ZAFYKAAXSA-N L-ascorbic acid 2-phosphate Chemical group OC[C@H](O)[C@H]1OC(=O)C(OP(O)(O)=O)=C1O MIJPAVRNWPDMOR-ZAFYKAAXSA-N 0.000 claims description 11
- 235000010419 agar Nutrition 0.000 claims description 11
- 229920000159 gelatin Polymers 0.000 claims description 11
- 239000008273 gelatin Substances 0.000 claims description 11
- 235000019322 gelatine Nutrition 0.000 claims description 11
- 235000011852 gelatine desserts Nutrition 0.000 claims description 11
- 239000001814 pectin Substances 0.000 claims description 11
- 235000010987 pectin Nutrition 0.000 claims description 11
- 229920001277 pectin Polymers 0.000 claims description 11
- 229920002678 cellulose Polymers 0.000 claims description 10
- 239000001913 cellulose Substances 0.000 claims description 10
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 9
- 229920000161 Locust bean gum Polymers 0.000 claims description 9
- 239000008272 agar Substances 0.000 claims description 9
- 235000010443 alginic acid Nutrition 0.000 claims description 9
- 239000000783 alginic acid Substances 0.000 claims description 9
- 229960001126 alginic acid Drugs 0.000 claims description 9
- 229920000615 alginic acid Polymers 0.000 claims description 9
- 150000004781 alginic acids Chemical class 0.000 claims description 9
- 235000010407 ammonium alginate Nutrition 0.000 claims description 9
- 239000000728 ammonium alginate Substances 0.000 claims description 9
- KPGABFJTMYCRHJ-YZOKENDUSA-N ammonium alginate Chemical compound [NH4+].[NH4+].O1[C@@H](C([O-])=O)[C@@H](OC)[C@H](O)[C@H](O)[C@@H]1O[C@@H]1[C@@H](C([O-])=O)O[C@@H](O)[C@@H](O)[C@H]1O KPGABFJTMYCRHJ-YZOKENDUSA-N 0.000 claims description 9
- 235000010410 calcium alginate Nutrition 0.000 claims description 9
- 239000000648 calcium alginate Substances 0.000 claims description 9
- 229960002681 calcium alginate Drugs 0.000 claims description 9
- OKHHGHGGPDJQHR-YMOPUZKJSA-L calcium;(2s,3s,4s,5s,6r)-6-[(2r,3s,4r,5s,6r)-2-carboxy-6-[(2r,3s,4r,5s,6r)-2-carboxylato-4,5,6-trihydroxyoxan-3-yl]oxy-4,5-dihydroxyoxan-3-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylate Chemical compound [Ca+2].O[C@@H]1[C@H](O)[C@H](O)O[C@@H](C([O-])=O)[C@H]1O[C@H]1[C@@H](O)[C@@H](O)[C@H](O[C@H]2[C@H]([C@@H](O)[C@H](O)[C@H](O2)C([O-])=O)O)[C@H](C(O)=O)O1 OKHHGHGGPDJQHR-YMOPUZKJSA-L 0.000 claims description 9
- 235000010418 carrageenan Nutrition 0.000 claims description 9
- 239000000679 carrageenan Substances 0.000 claims description 9
- 229940113118 carrageenan Drugs 0.000 claims description 9
- 235000010420 locust bean gum Nutrition 0.000 claims description 9
- 239000000711 locust bean gum Substances 0.000 claims description 9
- 235000010408 potassium alginate Nutrition 0.000 claims description 9
- 239000000737 potassium alginate Substances 0.000 claims description 9
- MZYRDLHIWXQJCQ-YZOKENDUSA-L potassium alginate Chemical compound [K+].[K+].O1[C@@H](C([O-])=O)[C@@H](OC)[C@H](O)[C@H](O)[C@@H]1O[C@@H]1[C@@H](C([O-])=O)O[C@@H](O)[C@@H](O)[C@H]1O MZYRDLHIWXQJCQ-YZOKENDUSA-L 0.000 claims description 9
- 235000010413 sodium alginate Nutrition 0.000 claims description 9
- 239000000661 sodium alginate Substances 0.000 claims description 9
- 229940005550 sodium alginate Drugs 0.000 claims description 9
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 9
- 229920001525 carrageenan Polymers 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 6
- 229920002907 Guar gum Polymers 0.000 claims description 3
- 235000010417 guar gum Nutrition 0.000 claims description 3
- 239000000665 guar gum Substances 0.000 claims description 3
- 229960002154 guar gum Drugs 0.000 claims description 3
- 238000010907 mechanical stirring Methods 0.000 claims description 3
- 229920001285 xanthan gum Polymers 0.000 claims description 3
- 235000010493 xanthan gum Nutrition 0.000 claims description 3
- 239000000230 xanthan gum Substances 0.000 claims description 3
- 229940082509 xanthan gum Drugs 0.000 claims description 3
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims description 2
- 229920000881 Modified starch Polymers 0.000 claims description 2
- 239000004368 Modified starch Substances 0.000 claims description 2
- 235000019426 modified starch Nutrition 0.000 claims description 2
- 238000001694 spray drying Methods 0.000 claims description 2
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 229920002148 Gellan gum Polymers 0.000 description 9
- 239000001856 Ethyl cellulose Substances 0.000 description 6
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 6
- 235000019325 ethyl cellulose Nutrition 0.000 description 6
- 229920001249 ethyl cellulose Polymers 0.000 description 6
- 229920000609 methyl cellulose Polymers 0.000 description 6
- 235000010981 methylcellulose Nutrition 0.000 description 6
- 239000001923 methylcellulose Substances 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 238000001879 gelation Methods 0.000 description 5
- 150000004347 all-trans-retinol derivatives Chemical class 0.000 description 4
- 239000008367 deionised water Substances 0.000 description 4
- 229910021641 deionized water Inorganic materials 0.000 description 4
- 238000007654 immersion Methods 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- -1 CaC Chemical class 0.000 description 2
- 241000206672 Gelidium Species 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 239000003349 gelling agent Substances 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 229920001206 natural gum Polymers 0.000 description 2
- 239000008188 pellet Substances 0.000 description 2
- 229920001282 polysaccharide Polymers 0.000 description 2
- 239000005017 polysaccharide Substances 0.000 description 2
- 150000004804 polysaccharides Chemical class 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 241000143060 Americamysis bahia Species 0.000 description 1
- 125000002252 acyl group Chemical group 0.000 description 1
- 238000009360 aquaculture Methods 0.000 description 1
- 244000144974 aquaculture Species 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 235000010492 gellan gum Nutrition 0.000 description 1
- 239000000216 gellan gum Substances 0.000 description 1
- 210000000987 immune system Anatomy 0.000 description 1
- 239000001509 sodium citrate Substances 0.000 description 1
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 230000029663 wound healing Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/80—Feeding-stuffs specially adapted for particular animals for aquatic animals, e.g. fish, crustaceans or molluscs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/163—Sugars; Polysaccharides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/174—Vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K40/00—Shaping or working-up of animal feeding-stuffs
- A23K40/30—Shaping or working-up of animal feeding-stuffs by encapsulating; by coating
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/15—Vitamins
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/80—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
- Y02A40/81—Aquaculture, e.g. of fish
- Y02A40/818—Alternative feeds for fish, e.g. in aquacultures
Definitions
- Typical gel-forming compounds include natural gums, starches, pectins, gellan, agar-agar and gelatin. Often, they are based on polysaccharides or proteins.
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Zoology (AREA)
- Animal Husbandry (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Mycology (AREA)
- Insects & Arthropods (AREA)
- Marine Sciences & Fisheries (AREA)
- Birds (AREA)
- Dispersion Chemistry (AREA)
- Fodder In General (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
La présente invention concerne un nouveau procédé de production d'une formulation de vitamine C plus stable (ou de dérivé de vitamine C).
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201880009695.6A CN110234239A (zh) | 2017-02-03 | 2018-01-31 | 改进的方法 |
| PH12019501686A PH12019501686A1 (en) | 2017-02-03 | 2019-07-22 | Improved process |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP17154561 | 2017-02-03 | ||
| EP17154561.9 | 2017-02-03 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| WO2018141791A1 true WO2018141791A1 (fr) | 2018-08-09 |
Family
ID=57963103
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/EP2018/052393 WO2018141791A1 (fr) | 2017-02-03 | 2018-01-31 | Procédé amélioré |
Country Status (3)
| Country | Link |
|---|---|
| CN (1) | CN110234239A (fr) |
| PH (1) | PH12019501686A1 (fr) |
| WO (1) | WO2018141791A1 (fr) |
Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5215767A (en) * | 1991-03-16 | 1993-06-01 | Kabushiki Kaisha Hayashibara Seibutsu Kagaku Kenkyujo | Additive for aquaculture feed for fish and shellfish and aquaculture feed for fish and shellfish which contains same |
| EP1046345A2 (fr) * | 1999-04-23 | 2000-10-25 | Showa Denko Kabushiki Kaisha | Préparation destinée à être administrée aux animaux et procédé d'alimentation correspondant |
| WO2001070044A1 (fr) * | 2000-03-24 | 2001-09-27 | Aventis Animal Nutrition S.A. | Composition liquide de vitamine |
| WO2003086099A1 (fr) * | 2002-04-18 | 2003-10-23 | Showa Denko K.K. | Aliments solides de pisciculture et procede de production correspondant |
| WO2006018119A1 (fr) * | 2004-08-19 | 2006-02-23 | Dsm Ip Assets B.V. | Nouvelles compositions de substances liposolubles |
| US20120039956A1 (en) * | 2010-08-13 | 2012-02-16 | Moti Harel | Dry storage stabilizing composition for biological materials |
| WO2013156543A1 (fr) * | 2012-04-20 | 2013-10-24 | Dsm Ip Assets B.V. | Compositions solides d'acide l-ascorbique de couleur stable |
| WO2014083067A1 (fr) * | 2012-11-27 | 2014-06-05 | Dsm Ip Assets B. V. | Procédé pour la production de particules extrudées solides distinctes |
| WO2015062518A1 (fr) * | 2013-10-30 | 2015-05-07 | 帝斯曼知识产权资产管理有限公司 | Particules de gel contenant une substance nutritive et leur procédé de préparation et d'utilisation |
| WO2015082688A1 (fr) * | 2013-12-06 | 2015-06-11 | Dsm Ip Assets B.V. | Formulation de biomasse |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19739167A1 (de) * | 1997-09-06 | 1999-03-11 | Baensch Tetra Werke | Gelartiges Futter für Wassertiere |
| CN1125638C (zh) * | 1999-05-20 | 2003-10-29 | 杭州阳光文化用品有限公司 | 稳定型缓释维生素c制剂及其生产方法 |
| US6329423B1 (en) * | 2000-06-09 | 2001-12-11 | Aventis Animal Nutrition, S.A. | Stable liquid formulations of high vitamin E content |
| CN103039697B (zh) * | 2012-12-04 | 2014-05-07 | 清远海贝生物技术有限公司 | 一种减少水产膨化饲料中水溶性维生素溶失的方法 |
| CN103783323B (zh) * | 2014-02-05 | 2016-05-18 | 褚旭 | 一种动物用复合维生素预混料制备方法 |
-
2018
- 2018-01-31 WO PCT/EP2018/052393 patent/WO2018141791A1/fr active Application Filing
- 2018-01-31 CN CN201880009695.6A patent/CN110234239A/zh active Pending
-
2019
- 2019-07-22 PH PH12019501686A patent/PH12019501686A1/en unknown
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5215767A (en) * | 1991-03-16 | 1993-06-01 | Kabushiki Kaisha Hayashibara Seibutsu Kagaku Kenkyujo | Additive for aquaculture feed for fish and shellfish and aquaculture feed for fish and shellfish which contains same |
| EP1046345A2 (fr) * | 1999-04-23 | 2000-10-25 | Showa Denko Kabushiki Kaisha | Préparation destinée à être administrée aux animaux et procédé d'alimentation correspondant |
| WO2001070044A1 (fr) * | 2000-03-24 | 2001-09-27 | Aventis Animal Nutrition S.A. | Composition liquide de vitamine |
| WO2003086099A1 (fr) * | 2002-04-18 | 2003-10-23 | Showa Denko K.K. | Aliments solides de pisciculture et procede de production correspondant |
| WO2006018119A1 (fr) * | 2004-08-19 | 2006-02-23 | Dsm Ip Assets B.V. | Nouvelles compositions de substances liposolubles |
| US20120039956A1 (en) * | 2010-08-13 | 2012-02-16 | Moti Harel | Dry storage stabilizing composition for biological materials |
| WO2013156543A1 (fr) * | 2012-04-20 | 2013-10-24 | Dsm Ip Assets B.V. | Compositions solides d'acide l-ascorbique de couleur stable |
| WO2014083067A1 (fr) * | 2012-11-27 | 2014-06-05 | Dsm Ip Assets B. V. | Procédé pour la production de particules extrudées solides distinctes |
| WO2015062518A1 (fr) * | 2013-10-30 | 2015-05-07 | 帝斯曼知识产权资产管理有限公司 | Particules de gel contenant une substance nutritive et leur procédé de préparation et d'utilisation |
| WO2015082688A1 (fr) * | 2013-12-06 | 2015-06-11 | Dsm Ip Assets B.V. | Formulation de biomasse |
Also Published As
| Publication number | Publication date |
|---|---|
| CN110234239A (zh) | 2019-09-13 |
| PH12019501686A1 (en) | 2020-06-01 |
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